Beam Technology Research Articles

Enhanced DNA damage induced by ultrashort electron beams in the presence of a Cu-containing porphyrin

This article presents an investigation into the interaction between ultrashort electron beams and DNA molecules. With the advent of advanced electron beam technology, the potential applications in various fields, including medicine and genetic engineering, have garnered significant attention. However, the intricate mechanisms underlying the interaction between ultrashort electron beams and DNA molecules remain largely unexplored. This study aims to bridge this gap in knowledge by obtaining experimental data. We used Cu containing water-soluble cationic 4-N meso-tetra-oxyethyl-pyridyl porphyrin. The electron beam irradiated the samples with different relative concentrations of porphyrin per base pair. It was shown that the presence of porphyrin enhances DNA stability, making it more resistant to radiation-induced damage, with the effect varying based on porphyrin concentration and irradiation dose.

Research progress of ultracold ion source

<sec>Nanobeam is an advanced technology for preparing charged ion beams with spot diameters on a nanometer scale, and mainly used for high-resolution and high-precision ion beam analysis, ion beam fabrication and ion beam material modification research. The nanobeam devices play an important role in realizing material analysis, micro/nano fabrication, microelectronic device manufacturing and quantum computing. The high-quality ion source is one of the key components of nanobeam device, the performance of which directly affects the resolution and precision of the nanobeam system. However, the traditional ion source used in this system is limited to available ionic species, large energy spread and complex structure. These issues hinder their ability to meet emerging application scenarios that require multi-ion types and high resolution. This emphasizes the importance of creating newion sources as soon as possible.</sec><sec>With the development of laser cooling technology, ultracold ions with temperatures in the range of mK or even μK can be obtained based on photoionization of cold atoms and laser cooling of ions. The typical characteristics of low temperature and easy operation greatly promote the emergence of ultracold ion sources. The ultracold ions exhibit extremely small transverse velocity divergence, which can significantly enhance the brightness and emittance quality parameters of the ion source, bringing great opportunities for innovating nano-ion beam technology. Therefore, the research on ultracold ion sources is of great significance for achieving high-quality ion sources with higher brightness, smaller size, lower energy dispersion, more diverse ion species, and simplified structure. Here, we introduce the important achievements in basic research and application technology development of magneto-optical trap ion sources, cold atomic beam ion sources, and ultracold single ion sources from the aspects of preparation principles, generation methods, and typical applications, and review the recent research progress of ultracold ion sources. Finally, we provide an outlook on the future development and application prospects of ultracold ion sources.</sec>

Exploring Magnetic Tractor Beam Technology for Enhanced Catheter Steering: Insights From Simulation and Experimentation

Exploring Magnetic Tractor Beam Technology for Enhanced Catheter Steering: Insights From Simulation and Experimentation

Modeling of technological parameters of electron beam weldingfor rocket and space technology products

The article contains the results of scientific research on modeling the technological parameters of electron beam welding. The modeling used a material VT-14 with a thickness of 0.16 cm. The purpose of the simulation is to improve the quality of the weld due to the optimal shape and the absence of defects in the form of pores and cracks. A concentrated energy source equivalent to an electron beam is used in the calculations. During the study of the thermal process of heating the material, the authors developed and tested criteria that allow optimizing welding parameters such as welding speed and the position of the focal spot relative to the surface of the heated part. In their calculations, the authors applied an original method of finding the welding speed and the coordinates of the focal spot according to the functionals of the thermal model. The algorithm developed by the authors was successfully tested on AMG-6 material with a thickness of 10 cm. In the process of modeling welding for large thicknesses, results have been obtained that must be taken into account when optimizing the welding parameters of products with large thickness. The relevance of the presented material is confirmed by the demand for the quality of the technology of welding structures with an electron beam. Research by the authors of this direction will significantly expand the possibilities in the application of electron beam technology for rocket and space technology.

Microstructure and properties of a multilayered laser cladding Al0.2NbTiV0.1W0.5Zr0.3 high-entropy alloy coating on a zirconium alloy

The corrosion and wear requirements of Zr alloys for application as fuel cladding materials are becoming increasingly stringent. Accordingly, developing surface engineering techniques and high-performance coating materials is crucial for achieving improved surface properties of these alloys. Herein, we propose a strategy for preparing high-performance coatings on Zr alloys using the multilayer cladding technique to prevent the high dilution of Zr alloy substrates because of high-energy beams. A novel Al0.2NbTiV0.1W0.5Zr0.3 high-entropy alloy (HEA) coating with a multilayer structure was prepared on a Zr alloy using multiple laser claddings. The top-layer and interlayer were composed of two body-centered cubic (BCC) phases and a Zr-rich phase. Owing to the multilayer cladding, the top-layer was almost unaffected by matrix dilution and substrate evaporation, leading to a significantly reduced precipitation of the Zr-rich phase in the top-layer. The high hardness and excellent wear resistance of the coating were attributed to the two BCC phases; moreover, both, the Zr-containing HEA and substrate, exhibited adhesive wear. The top-layer exhibited superior pitting corrosion properties, whereas the microstructural inhomogeneity in the interlayer led to intergranular corrosion, dominating the corrosion process. Thus, this study presents a coating material system suitable for Zr alloys with excellent wear and corrosion resistances. The findings can potentially contribute to expanding the application of the high-energy beam technology to Zr alloys.

Significance of radiographic temporomandibular degenerative joint disease findings

The field of orthodontics has seen a recent increase in the number of patients over the age of 50 seeking treatment and also an increase in the use of cone beam technology. Similar to other joints in the body, the temporomandibular joint (TMJ) is associated with age-related degeneration. However, unlike other joints, degeneration of the TMJ is rarely symptomatic and when there is pain, it is usually self-limiting. In this article, we will review: (a) the incidence and prevalence of TMJ degenerative diseases, (b) similarities and differences of TMJ vs knee degenerative diseases, and (c) current treatment recommendations for TMJ degenerative diseases. In the vast majority of people, radiographic evidence of TMJ degeneration is an incidental finding. Future longitudinal research is needed to follow the natural course of TMJ degenerative patients.

Roadmap for focused ion beam technologies

The focused ion beam (FIB) is a powerful tool for fabrication, modification, and characterization of materials down to the nanoscale. Starting with the gallium FIB, which was originally intended for photomask repair in the semiconductor industry, there are now many different types of FIB that are commercially available. These instruments use a range of ion species and are applied broadly in materials science, physics, chemistry, biology, medicine, and even archaeology. The goal of this roadmap is to provide an overview of FIB instrumentation, theory, techniques, and applications. By viewing FIB developments through the lens of various research communities, we aim to identify future pathways for ion source and instrumentation development, as well as emerging applications and opportunities for improved understanding of the complex interplay of ion–solid interactions. We intend to provide a guide for all scientists in the field that identifies common research interest and will support future fruitful interactions connecting tool development, experiment, and theory. While a comprehensive overview of the field is sought, it is not possible to cover all research related to FIB technologies in detail. We give examples of specific projects within the broader context, referencing original works and previous review articles throughout.

From molecular beam technologies to virtual experiments and communities

In the last 50 years, the impressive results on chemical kinetics from crossed molecular beam experiments have been assisted by theoretical and particularly computational progress, among which are: (1) the design and implementation of the SIMBEX (SImulation of Molecular Beam EXperiments) procedure on parallel and distributed computers aimed at rationalizing the dynamical behavior of the investigated systems on the ab initio computed molecular interactions; (2) the establishing of theoretical and computational research and educational networks (like the Quantum Reactive Scattering and European Chemistry Thematic Network), the assembling of virtual research communities (like the meta- and the grid-chemistry ones within the Collaboration in Science and Technology (COST) initiatives to enhance synergic and cooperative work levering on highly productive platforms; (3) the participation in the management of both the Italian and the European grid infrastructures initiatives; (4) the development of molecular open science-enabled cloud services within the European Open Science Cloud (EOSC). Levering on the mentioned collaborative efforts, important open science initiatives have been implemented. The present paper illustrates a prototype model apparatus for the production of methane out of CO2 using renewable energy sources and a prosumer (producer–consumer) model for delivering online chemistry competence tests. Finally, a suggestion is made to establish networked local services of the academy for high school education.

Modeling and algorithm of three-dimensional metrology with critical dimension scanning electron microscope

To address the challenges of accurate metrology of height and sidewall angle (SWA) of three-dimensional structures with critical dimension scanning electron microscopy, general modeling and algorithms based on tilted electron beam technology and the corresponding application skills are proposed, and the validity and error accuracy are evaluated as well. Three typical structures, the trapezoid, inverted trapezoid, and step, are investigated with Monte Carlo simulation. The maximum derivative method is used to extract key parameters from the secondary electron linescan. The efficiency of the proposed modeling, algorithms, and the accuracy of the calculated height and SWA are improved further with the application of wavelet transform.

Influence of vacuum annealing on mechanical characteristics of focused ion beam fabricated silicon nanowires

This paper describes the influence of vacuum annealing on the mechanical characteristics of silicon (Si) nanowires (NWs) fabricated using focused ion beam (FIB) technologies. Two types of Si NWs having a cross-sectional one-side length or diameter ranging from 19 to 447 nm are prepared using the direct milling and Ga ion doping functions of FIB. The Si NWs prepared are annealed at 400–700 °C in high vacuum for 10 min, followed by quasi-static uniaxial tensile testing using a microelectromechanical system based tensile test system in a scanning electron microscope. All the Si NWs fracture in a brittle manner. Young's modulus of submicrometer-sized Si NWs shows both annealing and specimen size influences in the range from 120 to 170 GPa, whereas that of nano-sized Si NWs shows only annealing influence in the range from 60 to 110 GPa. Tensile strength scatters greatly, ranging from 1.0 to 7.2 GPa, which increases with increasing the NW size. A transmission electron microscope and an atomic force microscope suggest that, by annealing, recrystallization happens in the damaged layer introduced by FIB milling and the NW surface morphology changes due to its recrystallization and gallium (Ga) ion evaporation. Fracture origin is discussed through the comparison between surface roughness and crack length estimated by the Griffith theory of brittle fracture.

Optimization of Hoisting Attitude in Non-standard Steel Structures via Adjustable Counterweight Balance Beam Technology

Optimization of Hoisting Attitude in Non-standard Steel Structures via Adjustable Counterweight Balance Beam Technology

Nano Hotplate Fabrication for Metal Oxide-Based Gas Sensors by Combining Electron Beam and Focused Ion Beam Lithography.

Metal oxide semiconductor (MOS) gas sensors are widely used for gas detection. Typically, the hotplate element is the key component in MOS gas sensors which provide a proper and tunable operation temperature. However, the low power efficiency of the standard hotplates greatly limits the portable application of MOS gas sensors. The miniaturization of the hotplate geometry is one of the most effective methods used to reduce its power consumption. In this work, a new method is presented, combining electron beam lithography (EBL) and focused ion beam (FIB) technologies to obtain low power consumption. EBL is used to define the low-resolution section of the electrode, and FIB technology is utilized to pattern the high-resolution part. Different Au++ ion fluences in FIBs are tested in different milling strategies. The resulting devices are characterized by scanning electron microscopy (SEM), atomic force microscopy (AFM), and secondary ion mass spectrometry (SIMS). Furthermore, the electrical resistance of the hotplate is measured at different voltages, and the operational temperature is calculated based on the Pt temperature coefficient of resistance value. In addition, the thermal heater and electrical stability is studied at different temperatures for 110 h. Finally, the implementation of the fabricated hotplate in ZnO gas sensors is investigated using ethanol at 250 °C.

Germanium-based nearly hyperuniform nanoarchitectures by ion beam impact

We address the fabrication of nano-architectures by impacting thin layers of amorphous Ge deposited on SiO2 with a Ga+ ion beam and investigate the structural and optical properties of the resulting patterns. By adjusting beam current and scanning parameters, different classes of nano-architectures can be formed, from elongated and periodic structures to disordered ones with a footprint of a few tens of nm. The latter disordered case features a significant suppression of large length scale fluctuations that are conventionally observed in ordered systems and exhibits a nearly hyperuniform character, as shown by the analysis of the spectral density at small wave vectors. It deviates from conventional random fields as accounted for by the analysis of Minkowski functionals. A proof of concept for potential applications is given by showing peculiar reflection properties of the resulting nano-structured films that exhibit colorization and enhanced light absorption with respect to the flat Ge layer counterpart (up to one order of magnitude at some wavelength). This fabrication method for disordered hyperuniform structures does not depend on the beam size. Being ion beam technology widely adopted in semiconductor foundries over 200 mm wafers, our work provides a viable pathway for obtaining disordered, nearly-hyperuniform materials by self-assembly with a footprint of tens of nanometers for electronic and photonic devices, energy storage and sensing.

Cracking mechanisms in additively manufactured pure tungsten from printing single tracks, thin walls and cubes

Cracking is a critical issue in the additive manufacturing of pure tungsten (W). To eliminate crack formation, it is imperative to gain an in-depth understanding of the underlying mechanisms behind this process. In this study, we systematically investigated the crack behaviors of single tracks, thin walls, and cubes fabricated using powder bed fusion–laser beam (PBF–LB) technology with nonrotational parallel-hatching scanning. The energy framework was employed to elucidate the mechanism of crack formation. The longitudinal cracks appearing in the microstructures of single tracks and the through cracks existing in thin walls and cubes were characterized. Notably, periodic through cracks extended upward across the sample, appearing at every single hatch in unidirectional samples and at every other hatch in bidirectional samples. The horizontal, longitudinal, and transverse cross sections of cubes were studied to clarify the correlation between through crack arrangement and solidification microstructure. Based on a comprehensive analysis of grain boundaries, we proposed a deformation-cracking competition mechanism in PBF–LB tungsten. Geometric effects in the crack and microstructure were also revealed. This study could provide valuable insights into the formation of cracks in PBF–LB tungsten and serve as a foundation for future investigations aimed at eliminating cracks.

Degradation of polyacrylamide (PAM) in aqueous solution by electron beam technology: Efficiency, viscosity reduction and correlation with microstructure of polymer molecules

In this paper, we present a systematic evaluation about degradation of partially hydrolyzed polyacrylamide (HPAM) in aqueous solution by ionizing radiation to find relationship between HPAM decomposition, viscosity reduction and microstructure of polymer molecules. The viscosity of the two HPAM solution declined rapidly from 5.2 to 3.0 mPa s to 1.4–1.2 mPa s with the adsorbed dose of 0.1 kGy, and then reached the level of pure water at 0.5 kGy. The molecular weight declined remarkably from 1.6 × 107 Da to 1.4 × 105 Da (HPAM1) and from 1.2 × 107 Da to 1.1 × 106 Da (HPAM2) at 0.1 kGy. The HPAM solution changed from pseudoplastic fluid behavior to Newtonian fluid after irradiation. Following ionizing radiation, the presence of anion Na+, Ca2+, Mg2+, anions HCO3- and SO42-(1000–5000 mg/L) and surfactant sodium dodecyl sulfate (SDS) (50–100 mg/L) respectively has slight effect on the rate and extent of viscosity reduction, while CO32- and surfactant petroleum sulfonate exhibit a great negative effect on reducing HPAM viscosity. Ionizing radiation is able to destroy the molecular structure and spatial structure of HPAM. Both the C-C backbones and pendant are attacked. It is proposed that the degradation products include ammonium, aliphatic hydrocarbon, small molecular acids and compounds with double-bond. With the absorbed dose of 0.1 kGy, the micelles-like aggregates are broken into small particles by direct microscope observation, while the stretched and coiled molecular strands shrink and curl to form an irregular network from AFM and SEM observation. The chains break into fragment scattered randomly as increasing dose to 1.0 kGy. Both the diameter size and dispersity of HPAM molecules decreased remarkably after irradiation.·OH is the major active species responsible for HPAM degradation and viscosity reduction. This study contributes to a multiscale understanding the mechanism of ionizing radiation-induced degradation of HPAM in aqueous solution.

Applied research of high-strength steel utilization for a track of demining machine in terms of mechanical properties

The aim of this paper is to investigate welded joints of high-strength steel S960 QL manufactured by using three different welding technologies, namely the electron beam, the laser beam, and the metal active gas (MAG) technologies. The experimental part included tensile strength evaluation, microstructural analysis of welded joints, and hardness measurement. Welded joints (WJ) have consisted of the identical steels and the identical thickness (10 mm). Destructive tests confirmed that welded joints are characterized by the tensile strength similar to the base material. Upon further observation, we can conclude that microhardness was characterized by the lowest value in the softening zone (SZ) and the highest value in the hardening zone (HZ). The degree of softening was 11% for the electron welding, 13% for the laser welding, and up to 27% for the conventional MAG welding. This also corresponds with the size of the SZ, which was the widest in welds made with the MAG technology. The laser beam weld produced up to 50% lower heat-affected zone (HAZ) compared to the conventional MAG technology. In case of the electron beam, this number is even higher. On the contrary, highest hardness was observed for the electron beam technology, where the hardness in the hardening zone increased by up to 40% when compared with the base material. Tests show the possibility of production of reliable welded joints, which meet the complex requirements for lifetime and quality (according to the standard EN 6520–1 focusing on defects categorization and EN 5817 dealing with defects tolerance).

Hot corrosion behavior of NiCoCrAlY laser cladding coating on 17-4PH stainless steel before and after high-current pulsed electron beam irradiation

In this study, we employed high-current pulsed electron beam technology (HCPEB) to modify NiCoCrAlY coatings that were created via laser cladding on 17-4PH stainless steel. We compared and analyzed the hot corrosion behavior of the coatings before and after HCPEB irradiation using a molten salt of 75 wt. %Na2SO4 + 25 wt. %NaCl at 700 °C. We also elucidated the mechanism by which irradiation affects the hot corrosion performance of the coatings. Our findings demonstrate that the irradiated coating surface exhibited a dense remelting layer, which effectively prevented erosion by oxygen and molten salt, without any internal oxidation corrosion. Moreover, irradiation refined the grains on the coating surface and increased the diffusion rate of grain boundaries. Consequently, the irradiated coating formed laminated thermal growth oxides (TGO) during the hot corrosion process, with the interface between the TGO and the coating always covered by an Al2O3 layer. This TGO structure provided excellent protection, reduced the corrosion weight gain, and corrosion rate of the coating, and significantly improved the hot corrosion performance of the coating.

Microstructure and phase correlation of DySZ-Polyester abradable seal coating after thermal exposure

Advanced gas turbine blade/shroud clearance control system requires abradable seal coatings with a high-temperature capacity above 1000 ℃ to accommodate the increasing turbine inlet temperature requirements. Dysprosia-stabilized-zirconia (DySZ) based abradable seal Coatings were fabricated on the Ni-based single-crystal superalloy via the atmospheric plasma spraying technique. The microstructure of the DySZ-based coating before and after thermal ageing was characterized using high-contrast SEM. The phase composition and distribution of the coatings were measured by XRD and Raman spectroscopy, respectively. Focused ion beam (FIB) and Scanning transmission electron microscope (STEM) technologies were employed for the phase confirmation. The results indicated that phase transformation from tetragonal to monoclinic ZrO2 was observed in the DySZ-Polyester after 300 h thermal exposure. Based on the different concentrations of Dy element in the monoclinic and tetragonal phases, the morphology and distribution of the monoclinic phase in the coating were observed intuitively using high-contrast BSE images and further corroborated by the Raman spectra mapping results. During heat treatment, the polyester added to the feedstock was oxidized to form amorphous carbon, which is mainly distributed in the gaps of interlamellar cracks and big pores. In addition, numerous Dy2O3 precipitates added to the feedstock were detected in the as-sprayed coating, and some reacted with ZrO2 to form the Dy2Zr2O7 phase during thermal spraying and thermal ageing. The correlation between Dy concentration and phase structure was then discussed.

Engineering of niobium surfaces through accelerated neutral atom beam technology for quantum applications

A major roadblock to scalable quantum computing is phase decoherence and energy relaxation caused by qubits interacting with defect-related two-level systems (TLSs). Native oxides present on the surfaces of superconducting metals used in quantum devices are acknowledged to be a source of TLS that decrease qubit coherence times. Reducing microwave loss by “surface engineering” (i.e., replacing the uncontrolled native oxide of superconducting metals with a thin, stable surface with predictable characteristics) can be a key enabler for pushing performance forward with devices of higher intrinsic quality factor. In this work, we present a novel approach to replace the native oxide of niobium (typically formed in an uncontrolled fashion when its pristine surface is exposed to air) with an engineered oxide, using a room-temperature process that leverages accelerated neutral atom beam (ANAB) technology at 300 mm wafer scale. This ANAB is composed of a mixture of argon and oxygen, with tunable energy per atom, which is rastered across the wafer surface. The ANAB-engineered Nb-oxide thickness was found to vary from 2 to 6 nm depending on ANAB process parameters. The modeling of variable-energy x-ray photoelectron spectroscopy data confirms the thickness and compositional control of Nb surface oxide by the ANAB process. These results correlate well with those from transmission electron microscopy and x-ray reflectometry. Since ANAB is broadly applicable to material surfaces, the present study indicates its promise for modification of the surfaces of superconducting quantum circuits to achieve longer coherence times.

Fabrication of triangular pits in barium fluoride single crystals by localized electronic excitations

Ion beam technology is considered as one of the most effective and unique techniques for materials engineering. Here, we show that the selective chemical etching is used successfully for the fabrication of pyramidal etch pits by revealing the ion-induced damage in the surface and below surface regions of barium fluoride single crystals. The size of ion-induced pits is increasing by etching the ion impacted zones for longer time. Moreover, the types of the induced defects are probed using optical absorption spectroscopy. The presented findings are discussed in terms of the peculiarities of ion energy deposition as well as the comparison with the induced structures using different type of ions, namely slow highly charged ions. Furthermore, they might be of importance in today’s nano and microelectronics applications, where the fabrication of size-controlled surface structures is of high necessity.