Stainless Steel Alloy Research Articles

Characteristics of 3D Printed Functionally Graded Material for Replacement of Dissimilar Metal Weld in Nuclear Reactor

The dissimilar metal welds in the most of the reactors are connections between low alloy steel parts and stainless steel piping. There is a high possibility of primary water stress corrosion cracking (PWSCC) damage attributed to residual stress caused by the difference in material properties in the dissimilar metal weld joints. A number of accidents such as leakage of radioactive coolant due to PWSCC have been reported around the world, posing a great threat to nuclear safety. The objective of this study is to develop a technology that can fundamentally remove dissimilar metal welds by replacing the existing dissimilar metal parts with the functionally graded material (FGM) manufactured by metal 3D printing consisting of low alloy steel and austenitic stainless steel. A powder production, mixing ratio calculation, and metal 3D printing were performed to fabricate the low alloy steel-stainless steel FGM, and microstructure analysis, mechanical properties, and coefficient of thermal expansion (CTE) measurement of the FGM were performed. As a result, it is observed that CTE tended to increase as the austenite content increased in FGM. The gradual change of coefficient of thermal expansion in a FGM showed that the additive manufacturing using 3D printing was effective for preventing an abrupt change in thermal expansion properties throughout their layers.

سباكة الصلب عالي السبائكية AISI321 باستخدام السباكة الرملية

In this work, sand casting was used to obtain high-strength steel AISI-321 by melting alloy AISI304 using sand casting. This is in addition to titanium using an induction furnace, which is considered one of the metal forming processes that originated from the principle of casting in sand molds. In general, Ti will oxidize quickly in the melt if it is exposed to air in typical sand/investment casting processes; Titanium element provides greater resistance to inter granular corrosion. Stainless steel alloy 321, which differs from 304 in that it contains a percentage of titanium, which has given it the property of being used at high temperatures, which has increased the need or demand for stainless steel casting in some industries and due to the difficulty and complexity of producing some pieces or parts using SS304 (wrought) forging alloy by Machines, so that it became necessary to search for a way to improve quality and reduce time and cost, using plumbing technology, although information about this technology is not available in open references. The ability to cast stainless steel is affected by a variety of factors, such as the time and degree of melting, the types of additives, and the time of total solidification. In addition, there are some other casting factors that have a direct impact on the quality of casting stainless steel, such as the sand mold materials, their type, preparation of the sand mold, and the heat treatment steps. This research includes two parts, a theoretical part that includes the steps of sand casting, and the second part related to the practical side, where the effect of some casting factors was studied, which includes the weight and quantity of addition of titanium (300 to 1000 grams), the time of addition and pouring from (3 to 15 minutes), as well as a study of heat treatment and its effect. This is due to the quality of the stainless steel alloy under study. In each experiment, 100 kilograms were used on stainless steel 321 and 304. The practical experiments were completed in several experimental stages, and in each stage, some modifications were made so that they were based on previous results. The results of the chemical analysis of the last five samples showed a gradual increase in the amount of Ti% until it reached about 0.4%. The tensile strength and yield strength were at acceptable values compared to the Wrought SS321 and cast SS (CF) alloys, an austenitic stainless steel, where the lowest value was (200 and 198) MPa and the highest value was (559 and 315) MPa, respectively. The hardness values were between (145 to 149). Key words: sandcasting, Austenitic SS321, SS304, FeTi.

Titanium versus stainless steel alloy bridge plates for distal femur fractures: Does callus form earlier with titanium?

Distal femur fractures account for 3-6% of all femur fractures. Internal fixation of most distal femur fractures with an anatomic lateral locking plate should permit some motion at the metaphyseal portion of the fracture when secondary bone healing is planned by the operating surgeon. While several studies have been performed evaluating union rates for distal femur fractures with stainless steel and titanium plates, the timing of callus formation between stainless steel and titanium implants used as bridge plates for distal femur fractures (AO/OTA 33-A and -C) has been investigated to a lesser extent. We hypothesize that callus will be visualized earlier with post-operative radiographs with titanium versus stainless steel bridge plates. We retrospectively reviewed a consecutive cohort of patients over 18 years of age with acute AO/OTA 33-A and 33-C fracture patterns treated with an isolated stainless steel or titanium lateral bridge plate within 4 weeks of injury by a single fellowship-trained orthopedic trauma surgeon from 2011 to 2020 at one academic Level 1 trauma center. An independent, fellowship-trained orthopedic trauma attending surgeon reviewed anterior-posterior (AP) and lateral radiographs from every available post-operative clinic visit and graded them using the Modified Radiographic Score for Tibia (mRUST). Twenty-five subjects were included in the study with 10 with stainless steel and 15 with titanium plates. There were no significant differences in demographics between both groups, including age, sex, BMI, injury classification, open versus closed, mechanism, and laterality. Statistically significant increased mRUST scores, indicating increased callus formation, were seen on 12-week radiographs (8.4 vs. 11.9, p = 0.02) when titanium bridge plates were used. There were no statistically significant differences in mRUST scores at 6 or 24-weeks, but scores in the titanium group were higher in at every timepoint. In conclusion, we observed greater callus formation at 12 weeks after internal fixation of 33-A and 33-C distal femur fractures treated with titanium locked lateral distal femoral bridge plates compared to stainless steel plates. Our data suggest that titanium metallurgy may have quicker callus formation compared to stainless steel if an isolated, lateral locked bridge plate is chosen for distal femur fracture fixation.

Optimizing LPBF-parameters by Box-Behnken design for printing crack-free and dense high-boron alloyed stainless steel parts

Boron has almost null solubility in iron, and its addition to stainless steels leads to the formation of hard borides, beneficial for increasing the wear resistance. However, these boron-containing steels have poor printability, with the occurrence of pronounced cracking, high porosity and risk of delamination. In this work, Box-Behnken design coupled with analysis of variance (ANOVA) was used to optimize the LPBF (Laser Powder Bed Fusion) processing parameters of a highly boron-alloyed stainless steel reinforced with a boride network. The proposed models demonstrated to be accurate in determine the porosity percentage for the studied alloys, in which the laser power and scanning speed play the main role in the alloys’ densification, and absence of extensive defects. These results indicate that the use of design of experiments tools is essential to produce defect-free boron-modified stainless steel specimens with a relatively low number of experiments, identifying a narrow optimized processing window to build bulk composite materials.

Evaluation of the Corrosion Resistance of Watch Links from 316L and 904L Austenitic Stainless Steels Obtained by the Metal Injection Molding (MIM) Technique Intended to Be in Contact with Human Skin

Watchmaking manufacturers obtain their bracelet links from machining drawn metal profiles. But, today, there is another process that represents an alternative to manufacture them: metal injection molding using metal powders (MIM technology). This process is less expensive than the machining of drawn metal profiles. The aim of this study was to evaluate the corrosion behavior and the nickel cation release of two stainless steel alloys: 316L MIM and 904L MIM. The general corrosion behavior was evaluated by the rotating electrode technique; the galvanic corrosion measurements were conducted with a 316L AISI bulk coupling partner. The pitting corrosion behavior was evaluated in FeCl3 0.5 M media (according to ASTM G48-11). For comparison, a complementary study was conducted on 316L and 904L bulk alloys. The Ni cation release tests were conducted on 316L and 904L MIM and bulk samples according to EN 1811. Different electrochemical parameters were measured and calculated (open circuit potential, polarization resistance, corrosion current and Tafel slopes, coulometric analysis). Generally, if MIM steels are compared with conventional steels, their corrosion resistance behavior is inferior. In the couplings studied, the galvanic currents generated are very important. The shape of the curves also reveals the presence of localized corrosion phenomena. According to tests in ferric chloride, MIM steels were noted to have inferior behavior compared to conventional steels. MIM type 904L steels are comparable in behavior to conventional type 316L steels. The quantities of nickel released according to EN 1811 were very significant (2 mg cm−2 week−1 up to 24 mg cm−2 week−1) and did not meet the requirements of the European directive (0.5 µg cm−2 week−1). In conclusion, conventional steels studied under the same experimental conditions revealed a better behavior compared to MIM steels independently of the phenomenological parameters chosen.

Experimental Investigation into the Dry Reciprocating Wear Behavior of Additively Manufactured Austenitic Stainless Steel (316L) Alloys

Experimental Investigation into the Dry Reciprocating Wear Behavior of Additively Manufactured Austenitic Stainless Steel (316L) Alloys

Enhancing Machining performance in Stainless Steel Machining using MXene Coolant: A Detailed Examination

Metal cutting, a complex process in manufacturing, involves various factors that significantly affect the quality of the final product. Notably, the turning process is crucial, with outcomes that heavily depend on multiple machining parameters. These parameters encompass speed, depth of cut, feed rate, the type of coolant used (specifically, high heat transfer MXene coolant), and insert types, among others. The material of the workpiece is also a critical factor in the metal-cutting operation. This study focuses on achieving optimal surface quality and minimizing cutting forces in the turning process. It recognizes the substantial impact of numerous process parameters, directly or indirectly affecting the product's surface roughness and cutting forces. Understanding these optimal parameters can lower machining costs and improve product quality. Our research concentrates on turning a stainless-steel alloy workpiece using a carbide insert tool. We employ the Response Surface Method (RSM) to optimize cutting parameters within a set range of cutting speed (100, 125, 150 m/min), feed rate (0.1, 0.2, 0.3 mm/rev), and depth of cut (0.4, 0.8, 1.2 mm). Additionally, we use various tool geometries and the RSM design of experiments to enhance and analyze the multi-response parameters of surface roughness and tool life. Optimal machining parameters for MXene-NFC involve a cutting speed of 140 m/min, a feed rate of 0.05 mm/rev, and a depth of cut of 0.5 mm. These settings ensure minimal surface roughness, maximum tool life, and the greatest total length of cut, achieving a composite desirability of 0.695.

Correction to “Dynamic and localized microelectrochemical approaches to evaluate the corrosion resistance of newly developed lean duplex stainless steel alloys”

Correction to “Dynamic and localized microelectrochemical approaches to evaluate the corrosion resistance of newly developed lean duplex stainless steel alloys”

Efficient design of composite honeycomb sandwich panels under blast loading

Hybrid composite honeycomb sandwich structures (HCHSS) were employed due to high specific strength and stiffness and higher impact resistance property required for the aerospace and defence fields. The numerical modelling of the efficient HCHSS was developed for the core, front and back face plate using the C3D8R elements to determine the realistic failure behaviour for the honeycomb sandwich structure. The ConWep blast simulation loading was applied for the HCHSS. Advanced composite materials were used for the blast analysis of the HCHSS (carbon/epoxy, graphite/epoxy, woven basalt fibres/polypropylene and woven Kevlar fibres/polypropylene). The damage initiation and damage propagation based progressive damage modelling was developed and implemented in the VUMAT code for composite materials to determine the actual failure behaviour of the HCHSS. The face sheets used in this model were of a stainless-steel alloy AL-6XN. The sandwich structure was subjected to blast loads of 1, 2 and 3 kg of TNT and their performance was compared w.r.t both front and back-face deflection. The effectiveness of sandwich panels was further examined by altering the thickness of the core. Fibre-metal laminates (FML) were used in place of the steel face sheets in the panel in order to minimise its mass, and a thorough analysis of the panel’s mass in relation to its peak deflection was carried out. Upon analysing the results, it was noted that the panel with the basalt fibre reinforced polymer (BFRP) core gave the best results compared to other composite materials. For a blast load of 3 kg TNT, the peak back face deflection (PBFD) of HCHSS with a BFRP core decreased by 10.64%, 7.61% and 4.75%, respectively, compared to panels with CFRP, GFRP, and KFRP cores. The peak deflection of the panel decreased as the BFRP core thickness increased. The energy absorption capacity of the panel also increased with increasing thickness. Additionally, it was found that panels with BFRP cores and KFRP-steel laminate face sheets provided the optimum balance of strong blast resistant performance and light weight. Compared to the metallic (steel) sandwich panel, the mass of the sandwich panel with KFRP-steel laminate face sheets and BFRP core was reduced by 33%, but at the same time, its PBFD increased by almost 50%.

Experimental periprosthetic fractures with collarless polished tapered cemented stems.

After cemented total hip arthroplasty, the risk of periprosthetic fracture (PPF) of taper-slip stems is higher than that of composite-beam stems. We aimed to assess the conditions resulting in PPFs of taper-slip stems using a falling weight. Taper-slip stems were fixed to five types of simulated bone models using bone cement, and the fractures were evaluated by dropping stainless-steel weights from a predetermined height onto the heads. The periprosthetic fracture height in 50% of the bone models (PPFH50) was calculated using the staircase method. For the fixation with 0° of flexion, the values for PPFH50 were 61 ± 11, 60 ± 13, above 110, 108 ± 49, and 78 ± 12cm for the cobalt-chromium-molybdenum alloy, stainless steel alloy (SUS), titanium alloy (Ti), smooth surface, and thick cement mantle models, respectively; for the fixation with 10° of flexion (considering flexure), the PPFH50 values were 77 ± 5, 85 ± 9, 90 ± 2, 89 ± 5, and 81 ± 11cm, respectively. The fracture rates of the polished-surface stems were 78.6 and 35.7% at the proximal and distal sites, respectively (p < 0.05); the fracture rates of the smooth-surface stems were 14.2 and 100%, respectively (p < 0.05). The impact tests demonstrated that the conditions that were less likely to cause PPFs were use of Ti, a smooth surface, a thick cement mantle, and probably, use of SUS.

Microstructure and tribological properties of laser directed energy deposited 316-NiTi heterogeneous bionic sandwich structure coatings

In this study, inspired by multilayer structures in nature, an equal weight ratio Ni/Cu composite sandwich specimen was introduced for joining 316 and NiTi alloys to improve the wear resistance of 316. The microstructural evolution process as well as the wear resistance mechanism is clarified by a series of material characterization methods and mechanical property tests. The microstructure of the Ni/Cu interlayer exhibits a dendritic morphology, and the NiTi layer shows both coarse and fine characteristics. The crystallography of 316-Ni/Cu–NiTi composite sandwich specimens was investigated by electron backscatter diffraction. Three types of friction balls (316, 440C, 100Cr6) were used to perform dry reciprocating sliding ball-on-plate wear testing on 316-Ni/Cu–NiTi composite sandwich specimens and 316 substrates under varying normal loads from 10 N to 30 N. The 316-Ni/Cu–NiTi specimens showed better wear resistance compared to the 316 substrate under different wear conditions, when the normal load is 30 N and the friction ball is 100Cr6, the specific wear rate of the coating is only 44% of the substrate. This study not only provides insights to enhance the wear resistance of 316, but also develops a novel approach to broaden the connection between austenitic stainless steel and NiTi alloys.

Long-lasting low fluorinated stainless steel hierarchical surfaces for omniphobic, anti-fouling and anti-icing applications

Stainless steel (SS) alloys are prevalent in many industries, household appliances or other commodities, where a strict control of surface properties is required to tailor their interaction with the environment. In this work we report a new procedure of stainless steel surface processing that provides a multifunctional response including superhydrophobicity, omniphobicity, self-cleaning, anti-fouling and effective anti-icing capacity, while still preserving a corrosion resistance similar to that of this material in compact form. The method consists of a first nanostructuration step followed by a low fluorination. The nanostructured surfaces presented a dual scale roughness of hierarchical character. The liquid free approach developed in this work to get this singular surface nanostructuration entails a first laser treatment of stainless steel flat substrates, followed by the deposition of a nanostructured thin layer of this material by electron beam evaporation in an oblique angle configuration. The resulting hierarchical surfaces were subjected to fluorination by: (i) the plasma-assisted deposition of a thin Teflon-like coating or (ii) the grafting of fluorinated molecules. The self-cleanable, anti-adherent and ice repellent character of the resulting low fluorinated surfaces outperformed the behaviour of classical slippery surfaces obtained by the infusion of high amounts of fluorinated liquids. These hierarchical SS surfaces withstood mild abrasion tests and the effect of water jets. Moreover, the corrosion behaviour of the fluorinated surfaces determined through their potentiodynamic analysis revealed a similar corrosion resistance than the flat SS substrates. Outstandingly, after these corrosion tests, the fluorinated samples obtained by grafting preserved their surface functionalities without significant degradation. The high mechanical and chemical stability of these low fluorinated samples support their usage for a large variety of applications.

Manufacturing process encoding through natural language processing for prediction of material properties

Knowledge of manufacturing processes is crucial to determine the final properties of a material, thus this work focuses on analyzing the relationship between final properties, chemical composition, and manufacturing process through data analysis. Furthermore, techniques of natural language processing are used to encode the manufacturing process as input in the neural network. The work consisted of two main parts: firstly, the relevant data was gathered, cleaned-up, and analyzed using statistical and probabilistic methods, K-means, and Principal Components Analysis (PCA), and secondly, a model was developed to predict elongation, yield, and tensile strength. Fully Connected Neural Network (FCNN) algorithms were used to build the aforementioned model. In addition, in order to avoid overfitting and evaluate the model dropout function and K-fold cross-validation are incorporated. Results demonstrated reasonable accuracy in elongation, yield, and tensile strength. Two cases of mechanical properties prediction of stainless steel alloy were presented, first, an existing alloy that was not in the training and test set, and second a suggestion of a new stainless steel alloy, which combines good YS, UTS, and Pitting resistance equivalent number (PREN). Additionally, it was considered an example from the TRIP family to showcase the tool’s versatility across various steel types.

Using spherical indentation to determine creep behavior with considering empirical friction coefficient

Indentation testing is a common technique for characterizing the mechanical properties of materials. When it comes to assessing the yield behavior of metals, conical indentation is often favored due to its ability to induce significant plastic deformation at relatively shallow indentation depths. On the other hand, spherical indentation is typically chosen for evaluating metal creep behavior, as it helps minimize the influence of plastic deformation on creep measurements. In spherical indentation tests, the friction at the contact interface is particularly crucial, given the larger contact area and more pronounced slip zones. However, accurately determining the friction coefficient at the contact interface is a complex multi-scale challenge, with the exact coefficient varying based on specific testing conditions and surface treatments. Consequently, empirical friction coefficients are frequently employed, often without thorough justification. In this work, we proposed Bayesian inference method for obtaining the creep constitutive behavior of alloys through spherical indentation tests. Our model considers not only the complexity of creep law, but also the indentation friction, which is unable to consider in most spherical indentation tests with traditional treatment. By using experimental data of spherical indentation tests on 310S stainless steel and pure nickel alloy from literature, present study demonstrates the effectiveness of the Bayesian inference approach, with the inferred constitutive models exhibiting well agreement with uniaxial creep behavior. Furthermore, the method considers the friction coefficient as an extra factor in inferring creep constitutive behavior from indentation tests.

Characterization of Fiber Metal Laminates for the Development of Subsea Housing

Fiber Metal Laminates (FML) are hybrid composites comprising metals and Fiber Reinforced Plastics (FRP). FMLs are the most widely used in aerospace, defence and automotive sectors due to their superior qualities like light weight, tensile, compression, flexural, excellent fatigue and impact resistance. The properties like strength-to-weight ratio, susceptibility to corrosion and good heat conduction of FML make it suitable for subsea applications. Commonly, FML with a combination of aluminium (Al), titanium (Ti), stainless steel (SS) alloys and FRP are widely used for ocean applications. Compared to other FML, the SS alloy-based FML is typically used in subsea applications as it has more creep and excellent corrosion resistance. In India, under the Ocean Acoustics programme of the National Institute of Ocean Technology (NIOT), an autonomous underwater Ambient Noise Measurement System (ANMS) has been developed and deployed in the shallow waters of Indian seas for the past 12 years to study the background noise prevailing in the sea. To accommodate electronics and power packs for the measurement of ambient noise at an ocean depth of 100 m, subsea housing with stainless steel 316L (SS316L) material for a pressure rating of 1 MPa has been developed. The objective of this study is to develop the FML with SS316L and FRP for reducing the weight of the housing. Based on the literature studies and Classical Laminate Theory (CLT), the FML has been fabricated as a 0.45 m (450 mm) panel with a sequence of SS316L as outer layers and E-glass fibre and carbon as the inner layers. The total thickness of the laminates is 0.006 m (6 mm). The developed FMLs are processed with water jet cutting machines to carry out various testing such as tensile, compression and flexural, which are relevant to the characterization of FML and the experimental results are described in the paper.

Corrosion-induced changes in surface properties and roughness of orthodontic wires

This study aimed to investigate the surface free energy and surface roughness (SR) of metallic alloys under the influence of acid solutions. The experiment involved the use of 270 rectangular wire samples measuring 0.019 × 0.025-in. These samples were sourced from 3 different commercial brands: Dentsply GAC, American Orthodontics, and Orthoclassic. This invitro study categorized the samples into 3 groups based on the solutions employed: deionized water, citric acid, and phosphoric acid. Each group consisted of 90 samples, with 30 samples representing each type of alloy-stainless steel, nickel-titanium, and titanium molybdenum alloy (TMA). The wire segments were immersed in their respective solutions for 72 hours at a controlled temperature of 37°C, with continuous orbital agitation at 130 rpm. After the immersion period, the study analyzed both surface free energy and SR. The mean values obtained were subjected to an analysis of variance at a significance level of 5%. All alloys displayed hydrophobic behavior, as indicated by interaction free energy values<0. In acidic environments (phosphoric acid and citric acid), significant differences were observed among different brands and alloys, affecting surface energy and interaction free energy. Variations in SR among metallic alloys included steel with the lowest SR variations, followed by nickel-titanium and TMA. Notably, the TMA alloy stood out with significantly higher surface energy compared with that of the other alloys (P<0.001). In this study, all examined alloys demonstrated a hydrophobic nature, suggesting a limited attraction to water. Notably, TMA exhibited the least hydrophobic behavior among the alloys studied. However, when exposed to citric acid, TMA displayed the most substantial alterations in its surface properties. These results underscored the significance of accounting for the distinctive properties of each alloy and their responses to diverse challenges, such as exposure to acidic solutions, during the selection of orthodontic wires for orthodontics treatment.

Comparing the Corrosion Behavior of CoCrNi Medium-Entropy Alloy and Duplex Stainless Steel in Ammonium Chloride Solution

Comparing the Corrosion Behavior of CoCrNi Medium-Entropy Alloy and Duplex Stainless Steel in Ammonium Chloride Solution

Exploring the mechanisms of calcium carbonate deposition on various substrates with implications for effective anti-scaling material selection

The unexpected scaling phenomena have resulted in significant damages to the oil and gas industries, leading to issues such as heat exchanger failures and pipeline clogging. It is of practical and fundamental importance to understand the scaling mechanisms and develop efficient anti-scaling strategies. However, the underlying surface interaction mechanisms of scalants (e.g., calcite) with various substrates are still not fully understood. In this work, the colloidal probe atomic force microscopy (AFM) technique has been applied to directly quantify the surface forces between calcite particles and different metallic substrates, including carbon steel (CR1018), low alloy steel (4140), stainless steel (SS304) and tungsten carbide, under different water chemistries (i.e., salinity and pH). Measured force profiles revealed that the attractive van der Waals (VDW) interaction contributed to the attachment of the calcium carbonate particles on substrate surfaces, while the repulsive electric double layer (EDL) interactions could inhibit the attachment behaviors. High salinity and acidic pH conditions of aqueous solutions could weaken the EDL repulsion and promote the attachment behavior. The adhesion of calcite particles with CR1018 and 4140 substrates was much stronger than that with SS304 and tungsten carbide substrates. The bulk scaling tests in aqueous solutions from an industrial oil production process showed that much more severe scaling behaviors of calcite was detected on CR1018 and 4140 than those on SS304 and tungsten carbide, which agreed with surface force measurement results. Besides, high salinity and acidic pH can significantly enhance the scaling phenomena. This work provides fundamental insights into the scaling mechanisms of calcite at the nanoscale with practical implications for the selection of suitable anti-scaling materials in petroleum industries.

Characterisation of TCP precipitation sequences of superaustenitic stainless steel and correlation with electrochemical and mechanical properties

This study investigates the influence of precipitation sequences formed at critical high-temperature range for various ageing time of super austenitic stainless steel 654SMO against the evolution of its corrosive resistance performance through the microstructural characterization, hardness and electrochemical corrosion testing. The specific type of stainless-steel alloy is one of the most corrosion resistant along with exceptional mechanical properties, tailor-made for pressurized and erosive systems handling chlorinated sea water, plate heat exchangers, and fuel gas cleaning applications and an excellent case study of in-depth phase transformations-electrochemical properties characterization phenomena. The microstructure evolution is characterized by scanning electron microscopy (SEM) coupled with energy-dispersive spectroscopy (EDS), hardness testing and potentiodynamic polarization curves. The corresponding precipitation characteristics and sequences of secondary phases are discussed and correlated with electrochemical properties. The results demonstrate σ phase with various morphologies formed during isothermal aging and the formation of three more secondary topologically close pack (TCP) phases, such as chi phase (χ), laves phase (A2B), and Cr2N against corrosive resistance and mechanical performance, which are of primary importance for understanding electrochemical phenomena of different phases and useful for optimizing such alloys for various applications.

Preparation, characterization and composition optimization design of laser powder bed fusion continuously graded Invar36/316L stainless steel alloys

It is of great significance for designing different material compositions and batch experimental research via using additive manufacturing. In this work, Invar36 and 316L stainless steel (SS) are used as raw materials, and a specially designed powder distribution system in a laser powder bed fusion (LPBF) equipment is used to prepare continuous gradient alloys (CGAs) of Invar36/316L SS. The effects of microstructure and properties variations when the ratio of two compositions of Invar36 and 316L SS are systematically studied. It is found that the grain size and morphology of the melt pool would vary with the composition, but there is no significant difference in the phase distribution. In addition, localized areas of CGAs show similar or even better mechanical properties, thermal expansion properties, or corrosion resistance than the two materials themselves. When the percentage of Invar36 content is 70% - 80%, the microstructure and grain distribution of the samples are relatively uniform, and the tensile strength and corrosion resistance of the material are greatly improved, while the coefficient of thermal expansion does not increase significantly. The results of this work provide a practical path for the composition design and high throughput experiments of multiple materials.