Agricultural Biomass Research Articles

Chemical Hydrolysis-Gamma Irradiation Processes for Cellulose Nanofibers Isolation from Rice Straw

Utilization of agriculture biomass waste into high value product is still potential to develop. In this study, cellulose nanofibers (CNF) as valuable materials were isolated from rice straw. Sodium hydroxide pulping and hydrogen peroxide bleaching were conducted as cellulose pretreatment. The CNF was prepared using 1 M hydrochloric acid hydrolysis followed gamma irradiation with various radiation doses, i.e. 40, 60, 80, 100 and 120 kGy. Compositions of α–cellulose and water retention of each stage processes increased inversely with hemicellulose, lignin and degrees of polymerization which had been strengthened by Fourier transform infrared spectroscopy (FTIR) spectra. X-ray Diffraction (XRD) analysis revealed that crystallinity index was more intense than rice straw, i.e. 80.85 %. Particle Size Analyzer (PSA) studies described the isolation process of CNF succeed with the smallest size 77.8 nm. The CNF functional groups of hydrophilic both hydroxyl and carboxylate slightly diminished with increasing of radiation doses followed water retention reducing, however the crystallinity had not changed significantly. Increasing radiation doses also could improve the thermal stability with the highest Tg 153.1 0C therefore the obtained CNF could be used as suitable nanocomposite.

Particle size-dependent anti-corrosion and mechanical behavior of green-graphene composite

In this study, Green graphene (GG) was synthesized from residual agricultural biomass through pyrolysis and prepared various sizes (2D, 37 μm, 45 μm, 53 μm, and 100 μm) via mechanical and liquid phase exfoliation. These GG samples were incorporated into an EP matrix, forming GG/EP composite coatings for carbon steel. Corrosion resistance was assessed via PDP and EIS techniques. The 37 μm-GG/EP composite coating also showed uniform distribution and compact surfaces. The 37 μm-GG/EP composite coating displayed higher corrosion inhibition (99 %) owing to the even distribution of GG within the EP matrix than the uncoated, along with enhanced hydrophobicity, tensile strength (61.3 %), fracture strain (77.2 %), and toughness (90.5 %) than pure EP coating. Improved corrosion resistance, which was found related to three main factors: first, GGs enhance the coating integrity by obstructing pores and flaws, to stop corrosive media from penetrating. Second, the well-dispersed GG sheet lengthens the diffusion pathways for corrosive agents to the carbon steel substrate, consequently lenghtening the corrosion process. Third, at 37 μm size the resititve forcefields of the GG/EP structure become the most effecitve agaisnt the corrosive media. The study also establishes GG as an eco-friendly sustainable alternative of non-renewable resource based mined compounds of Zn, etc. that are universally and traditionally used, for protective coatings.

Adsorption Isotherms and Thermodynamics of <i>Thymol Blue</i> Removal from Aqueous Solution Using Native Pear (<i>Dacryodes edulis</i>) Seed Biomass

The release of dyes into watercourses not only upsets their beautiful nature but also hinders the transmission of sunlight into streams, reducing photosynthesis and resulting in the loss of aquatic life and reduction of water quality. Therefore, there is need to remove such colored substances. One of such dyes is thymol blue. This study was conducted with a view to removing thymol blue (TB) dye from an aqueous solution using a low-cost agricultural biomass, the African native pear (Dacryodes edulis), as the adsorbent. Batch experiments showed that the process was affected by pH, temperature, contact time, and initial thymol blue concentration. Optimum dye adsorption was achieved at pH 12. The data was analyzed using Langmuir and Freundlich isotherm models. The latter isotherm better described this process than the former. The thermodynamic quantities like free energy change (∆G°), enthalpy change (∆H°), and entropy change (∆S°) were also evaluated. It was inferred from the results that the adsorption process was spontaneous, feasible, endothermic in nature, and occured by a physisorption mechanism. These findings indicate that the native peer seed is an efficient biosorbent for thymol blue removal from an aqueous environment.

Efficient and low-cost mesoporous magnetic carbon composites derived from date palm stones for environmental remediation of hexavalent chromium

This study was performed to achieve two important scientifically challenging goals, environmental remediation of toxic heavy metals and utilization of agricultural lignocellulosic wastes. In this work, a series of mesoporous magnetic carbon (MMC) adsorbents were synthesized by carbothermic reduction at different temperatures employing date palm (Phoenix dactylifera L.) stones as the carbon source. The synthesized adsorbents were characterized by different technquies and the results confirmed the presence of zero-valent iron (ZVI) nanoparticles and other iron oxides as products of the carbothermal reduction. The nature of phases present, crystallite size and the surface properties were found to be dependent on the calcination temperature. The adsorbent MMC700 exhibited the smallest (ZVI) crystallite size 36 nm and the largest SBET 341 m2/g. All adsorbents showed mesoporous structure with mesopore average diameter lower than 6 nm. The performance was evaluated in the removal process of toxic Cr(VI) in an aqueous medium, and the optimum conditions of the process were reported. The removal process was dependant of solution pH where best results was achieved at pH = 2. Complete removal of chromium was achieved in less than 5 min by MMC700. The results were better fitted with pseudo-second-order kinetics and followed the Freundlich model isotherm. The maximum adsorption capacity was found to be 265.25 mg/g for MMC700, suggesting its application as an efficient, low-cost, and easily separable adsorbent for the toxic Cr(VI) removal process. The prepared adsorbents exhibited superior performance in the removal process compared to other agricultural wastes or biomass - derived adsorbents reported in literature.

Investigation of regeneration cycles with different catalysts on steam gasification of biomass

In this work, agricultural biomass waste was gasified in a two-zone tubular reactor in the presence of steam. Firstly, during preliminary experiments the effect of temperature in the 1st and 2nd reactor zone, as well as the influence of catalysts and steam/raw material ratio was investigated, then the reusability of catalysts was also studied during ten regeneration cycles. Based on the preliminary results, in the 1st reactor zone a lower temperature was used (400 °C), where the yield of carbon dioxide was ∼55 %, which has a positive effect on numerous reactions, also it can be converted to carbon monoxide with proper catalysts with in-situ process. Regarding the temperature, it is important to be mentioned that a significant difference was observed in the yield of synthesis gas at 700 °C thus, the experiments were carried out using 700 °C in the 2nd reactor zone. A natural (Clinoptilolite) and a synthetic zeolite (ZSM-5), a mesoporous alumina (Al2O3) and a carbon dioxide capturing carrier (CaO) were selected and impregnated with nickel for further use and for enhancing the yield of synthesis gas and hydrogen during the gasification process. The utilization of catalysts helped the in-situ reduction of carbon dioxide while their performance in the gasification process during the regeneration cycles was also investigated. Henceforward, the tested Ni/ZSM-5, Ni/Al2O3 and Ni/Clinoptilolite, reduced the amount of carbon monoxide from the 5th regeneration cycles, while the amount carbon dioxide with the four mentioned catalysts was decreased by 15–35 mmol/g raw material, compared to the results obtained during thermal degradation.

A wastes-based hierarchically structured cellulose membrane: Adsorption performance and adsorption mechanism

It was imperative to expeditiously investigate novel avenues for the valorization of agricultural waste biomass crop straws. The straws represented promising substrates to design eco-friendly adsorbents for the effective treatment of complex dyeing wastewater owing to their widespread availability, low cost, easy production, and environmental friendliness. Despite the advantages, developing adsorbents with versatile uses, antibacterial properties, and strong mechanical qualities remained a challenge. Herein, a sustainable waste treatment strategy is put forward by developing multifunctional adsorbents derived from agricultural waste. The adsorbents are designed to synchronously adsorb the typical contaminants such as organic molecule (methylene blue, MB) and heavy metal ions (cadmium ion, Cd2+) in dyeing wastewater. Through the assembly of cellulose fibers, multiscale cellulose membrane (MCM) substrates with enhanced two-dimensional (2D) structure were simply fabricated from biomass crop straws. Coating functional copper phosphate (CP) nanoflakes on the MCM substrate effectively constructed the hierarchical structure to achieve the synchronous adsorption. The synergistic effects of electrostatic attraction, hydrogen bonding and coordination greatly prompted the adsorption process. Furthermore, the multifunctional adsorbents were imparted with satisfactory antibacterial properties, thereby expected to solve the problem of membrane fouling in wastewater. Hierarchically structured copper phosphate @ cellulose antibacterial adsorbents (CP@MCM) exhibit huge application potential in the resource utilization of agricultural waste and effective treatments for dyeing wastewater.

Expression of Concern: Agricultural waste biomass for sustainable bioenergy production: Feedstock, characterization and pre-treatment methodologies

Expression of Concern: Agricultural waste biomass for sustainable bioenergy production: Feedstock, characterization and pre-treatment methodologies

Eco-friendly aqueous binder derived from waste ramie for high-performance Li-S battery

Even the sulfur cathode in lithium-sulfur (Li-S) battery has the advantages of high theoretical energy density, wide source of raw materials, no pollution to the environment, and so on. It still suffers the sore points of easy electrode collapse due to large volume expansion during charge and discharge and low active materials utilization caused by the severe shuttle effect of lithium polysulfides (LiPSs). Therefore, in this work, ramie gum (RG) was extracted from ramie fiber degumming liquid and used as the functional binder to address the above problems and improve the Li-S battery's performance for the first time. Surprisingly, the sulfur cathode using RG binder illustrates a high initial capacity of 1152.2 mAh/g, and a reversible capacity of 644.6 mAh/g after 500 cycles at 0.5 C, far better than the sulfur cathode using polyvinylidene fluoride (PVDF) and sodium carboxymethyl cellulose (CMC) binder. More importantly, even if the active materials loading increased to as high as 4.30 mg/cm2, the area capacity is still around 3.1 mAh/cm2 after 200 cycles. Such excellent performances could be attributed to the abundant oxygen- and nitrogen-containing functional groups of RG that can effectively inhibit the shuttle effect of LiPSs, as well as the excellent viscosity and mechanical properties that can maintain electrode integrity during long-term charging/discharging. This work verifies the feasibility of RG as an eco-friendly and high-performance Li-S battery binder and provides a new idea for the utilization of agricultural biomass resources.

Research on environment and sustainable development education under the background of green ecology

Abstract The implementation of environmental and sustainable development goal (SDG) education helps to cultivate people's awareness of environmental protection and the concept of SDG, and is conducive to the protection and management of the environment. However, due to the weak awareness of education and lack of environmental protection knowledge in the environment and SDG education, environmental protection work has been affected. Therefore, this article proposed the implementation strategy of environment and SDG education from the perspective of green ecology. This research utilized datasets agricultural biomass accumulated from five cities of Guandong (i.e., Foshan [F], Heshan [H], Nanxiong [N], and Shantou [S]) province, China. Through experimental research, the utilization rate of agricultural waste and utilization ratio of straw was explored by using data envelopment analysis, and then, the environmental awareness of students and the environmental education level of teachers under the environmental and SDG education strategies of green ecological concept were combined. The results showed that the proportion of straw waste biomass utilization in S city was the highest among the four cities; the implementation strategy of environment and SDG education proposed in this article can enhance students’ awareness of environmental protection by 5.21% and improve environmental education level of teachers by 9.51%.

Enhancement of hydrophobic, resistive barrier and anticorrosion performance of epoxy coating with addition of Clay-Modified Green Silico-Graphitic Carbon

Under this study, a straightforward method for producing clay-modified silico-graphitic carbon (CGSGC) was developed and applied to create CGSGC/epoxy coatings for carbon steel (CS). The CGSGC was synthesized using a mixture of 25 % pond clay, and 75 % remnant agricultural biomass by mass via pyrolysis route. The aim was to evaluate the barrier and anti-corrosion properties of these coatings. The results demonstrated that adding 0.1 wt.% of CGSGC in the epoxy (EP) matrix enhanced its anti-corrosion inhibition capabilities by 99.8 % when compared with standard EP coating. The 0.1 wt.% CGSGC/EP mixed coating also exhibited robust hydrophobicity with WCA of 142.2° and thermal stability up to 250 °C with 2–3 % coating weight reduction. The microhardness of the optimized sample shows a 59.18 % improvement compared to standard EP coating. SEM images revealed improved EP compactness and reduction in microstructural defects (holes and cracks), with the incorporation of 0.1 wt.% CGSGC. 3D profilometry showed a smoother surface for the 0.1 wt.% CGSGC/EP coating. Similar such materials, while being abundantrly and renewably available, can be a safer alternative to conventional hazardous chemicals for protecting carbon steel from corrosion; not to mention the carbon credit benefits they entail.

Detailed analysis of Türkiye's agricultural biomass-based energy potential with machine learning algorithms based on environmental and climatic conditions

AbstractIn the study, the biomass and energy potential of each province of Türkiye was calculated for the years 2010–2021, using data from 15 different fields and 16 different horticultural crops. The total theoretical energy potential obtained from field and garden products was calculated as 222,620 Terajoule (TJ) and 61,737 TJ for 2010 and 308,888 TJ and 77,002 TJ for 2021, respectively. The agricultural biomass potential for 2021 was estimated using machine learning algorithms, depending on the environmental and climate data covering 2010–2020, which has not been studied in the literature. In this study, agricultural biomass potential for Türkiye was tried to be modeled by using Random Forest, K-Nearest Neighbors (KNN), Gradient Boosting, and eXtreme Gradient Boosting Regressor (XGBR) from machine learning methods. Agricultural biomass potential was tested in a tenfold cross-validation analysis and prediction for 2021 using only climatic and agricultural area data. In addition, by applying feature selection, it has been tried to reduce the features to be used and increase the success rate. Accordingly, when the results of the Random Forest algorithm were generalized, it achieved an R2 value of 0.9328 using all features for the tenfold cross-validation analysis. At the same time, it reached an R2 value of 0.9434 using four features in the prediction of 2021 and was found to be successful. Considering only the 2021 forecast, the KNN algorithm reached the highest result with an R2 value of 0.9560 using only four features. Also, the Wilcoxon rank-sum test result at p = 0.05 shows no significant difference between the predictions and the actual values. Graphical abstract

Quantitative structural elucidation of original lignins in different varieties of waste Gleditsia sinensis Lam. pods

Obtaining new materials, industrial chemicals, and energy from the conversion of agricultural and forestry biomass to fill the gap of non-renewable fossil energy has become a growing trend. As a waste biomass, the G. sinensis pods (GSP) after saponin extraction are always discarded due to lack of industrial/high value-added utilization. Herein, in order to lay a foundation for the selection of pretreatment strategies of GSP and the valorization of GSP lignin, the lignins from the different varieties of GSP were isolated by double enzymatic method and quantitatively characterized. Results indicated that GSP lignin was of the GS-type (S/G, 1.1–1.4) and the interunit linkages were mainly β-O-4′ linkage, along with a certain amount of carbon-carbon linkages (≈35/Ar). L1 showed higher β-O-4′ linkage content (61.3/100 Ar) and relative molar mass (12190 mol/g). Some atypical lignin units, such as cinnamyl aldehyde end-group, cinnamyl alcohol end-groups, and ferulates, were also revealed in GSP lignins. Finally, the potential molecular structure graphs of the GSP lignin were depicted on the basis of the quantitative results. Overall, comprehensive research of the structural characteristics of GSP lignin is essential for efficiently deconstructing GSP and transforming the utilization of the cell wall components.

Decoding the quantitative relationship of algistatic activity and chemodiversity of plant-derived allelochemicals in optimized straw decomposition

The allelopathic effect of agricultural waste pretreated with Trametes versicolor for controlling the toxic alga Amphidinium carterae was investigated in this study. Response surface methodology revealed that the optimized physical factors displayed a substantial contribution to the potentiality of agricultural by-products in inhibiting A. carterae. The optimal inhibition property was achieved at a pH of 5.1, a temperature of 28.6 °C, a water content of 68 mL, and a straw particle size of 23.6 mm. Quantitative relationship analysis showed that total phenolic content, degradation rate, and β-glucanase greatly contributed to the algistatic activity of the straw extracts. Moreover, the extracts of straw were found to contain a diverse range of allelochemicals, with 63 compounds exhibiting allelopathic effects identified based on historical reports. Our analysis indicated that the allelochemicals responsible for the inhibition of A. carterae are mostly polyphenolics and their derivatives, as well as fatty acids. Therefore, these results provide a new strategy for the intensive and value-added utilization of agricultural biomass, contributing to the sustainable development of plant-derived algaecides.

Avocado Pruning Residues for the Formulation of Bio‐Based Polyethylene/Fiber‐Based Biocomposites for Sustainable Food Packaging

AbstractThe extensive use of non‐biodegradable bioplastics and fossil‐based plastics in food packaging presents a significant environmental challenge. Consequently, there has been a growing interest in exploring agricultural biomass as a potential source for formulating biocomposites for packaging due to the substantial amount of lignocellulosic residue generated. This study explores the utilization of avocado pruning residue (APR) for isolating lignocellulose fibers and their application as replacement and reinforcement material for bio‐based polyethylene (BioPE) composites. The results obtained reveal that a concentration of 9% (w/w) of maleic anhydride‐grafted‐polyethylene (MAPE) shows the most effective fiber–polymer interaction, resulting in a significant improvement of 25.47% in the mechanical properties. Biocomposites with varying fiber concentrations, ranging from 10% to 40% (w/w), are prepared and assessed for their macro‐ and micromechanical properties. The results demonstrate a substantial 49% increase in tensile strength and a remarkable 325% enhancement in Young's modulus for biocomposites containing 40% (w/w) fiber content. Furthermore, micromechanical analysis provides insights into the intrinsic strength and modulus of avocado fibers, with values of ≈437 MPa and 33 GPa, respectively. This research contributes to the development of sustainable and eco‐friendly alternatives for food packaging, reducing the reliance on fossil‐based plastics, and promoting the utilization of agricultural waste.

Surface modification of Luffa and Maize fibers by using alkali medium

Agricultural biomass is a well-known renewable resource that has a high rate of recycling. Two of them are luffa sponge and corn husk/maize fibers. Luffa sponge may be effectively used to reinforce lightweight composite constructions because of its polypore structure. For this race, maize fiber is also appropriate. Surface modifications for both of the fibers are needed for increasing mechanical strength with higher interfacial bonding with the matrix materials of composite manufacturing. This investigation involved treating both materials with 5 g/L, 10 g/L, and 15 g/L of NaOH in order to describe the alterations occurring on their physio-chemical characteristics. The therapy lasted 60 min and was administered at 90 °C. Following that, acetic acid was used to neutralize the samples. The ASTM D1445 technique was used to measure the bundle fibers' breaking force and elongation, and the ASTM D570 procedures were used in order to determine the water absorption variation % in the treated samples. The FTIR test and SEM examination revealed the contaminants that were eliminated from the surface of Luffa and Maize fibers. The test findings demonstrated improved modification behaviors for the 15 g m/L treated fibers, which had an elongation percentage of 3.02% and an equivalent breaking force of 5.12 kg for the Luffa fiber and 5.72 kg for the maize fiber. Natural contaminants were eliminated as a result of variations in functional group intensity shown in the FTIR pictures. However, SEM pictures showed that the surface smoothed out for samples treated with 15 g per liter of NaOH, which may be the cause of the fiber's brittle interlocking with the matrix components. Moreover, water absorbency rose by over 300% compared to the untreated fibers. In summary, samples treated with 10 g/L NaOH might serve as superior reinforced materials of composite for both types of fibers.

Efficient removal of sulfamethoxazole by activated peroxodisulphates using Fe/N co-doped biochar: The minimal role of high-valent iron species

The harmful effects of the widespread presence of sulfamethoxazole (SMX) in water on ecosystems have become an increasingly pressing concern, necessitating the urgent development of an effective decontamination strategy. In this work, iron and nitrogen co-doped biochar (Fe-N-BC) samples were synthesized using peanut shells as a precursor to activate peroxydisulfate for SMX degradation. The most effective Fe-N-BC had a 12 times higher SMX removal rate of 97.00% within 90 min compared to the pristine biochar. The excellent catalytic performance was achieved by the synergistic effect of the Fe and N active sites, and the system contained not only typical free radicals (SO4− and OH) but also high-valent iron species (Fe(IV)). Further quantitative experiments with active species revealed that the free radical reaction pathway played a predominant role, while the relative contribution of Fe(IV) was only 8.01%. Furthermore, the degradation pathways of SMX in the system were proposed, and toxicity assessment revealed that all intermediate products exhibited lower toxicity levels than SMX. This study clarifies the structure–activity relationships of Fe-N-BC for PDS activation and offers an innovative strategy for the treatment and utilization of agricultural waste biomass as the catalyst.

Biodegradable films from the lignocellulosic fibers of wheat straw biomass and the effect of calcium ions

Plastics are hazardous to human health, and plastic waste results in environmental pollution and ecological catastrophe. Biobased polymers from renewable sources have recently become promising for developing biodegradable packaging films. Among them, lignocellulosic residue from agricultural biomass is inexpensive, renewable, and biodegradable. This study aims to develop biodegradable films using lignocellulosic residue from wheat straw biomass. The methodology is a green process that solubilizes lignocellulosic chains using Zn2+ ions and crosslinks with Ca2+ ions of different concentrations (200–800 mM). The results reveal that the increase of Ca2+ ions significantly decreases moisture content, water solubility, water vapor permeability, transparency, and elongation of films. The tensile strength is recorded as 6.61 ± 0.07 MPa with the addition of 800 mM of CaCl2, which is approximately 2.5 times higher than commercial polyethylene films. Around 90 % of films biodegrade within a month in soil containing 20 % moisture content. Overall, lignocellulosic residue from wheat straw biomass could be an excellent replacement for synthetic polymer to fabricate strong, transparent, and biodegradable plastic films.

Efficient crop straws biotreatment using the fungus Cerrena Unicolor GC.u01

Lignin is main composition of agricultural biomass which can be decomposed through enzymatic hydrolysis by fungi. However, there are still needs to identify more efficient and effective fungal stain for biomass valorization. In this study, lignin degrading fungi from birch forest were screened for sustainable degradation of waste agricultural straws. The most effective strain was identified as Cerrena unicolor GC.u01 using 18 S rDNA gene-sequencing technology. Three different crop straws (corn stalk, rice and wheat straws) were used for the biotreatment studies. The activities of lignin degrading enzymes, laccase (Lac), cellulase and xylanase, secreted by C. unicolor were also determined. Scanning electron microscopy (SEM), fourier transform infrared spectroscopy (FTIR) and thermal gravimetric analyzer (TGA) were further used to monitor the effects of the biotreatment process. The results showed that C. unicolor degraded 34.3% rice straw lignin, a percentage which was higher than other isolated strains after 15 d straw liquid fermentation. The highest Lac activity (8.396 U•mL− 1) was observed with corn stalk on the 7 d. Cellulase and xylanase activities, in the same biomass, were higher than those of wheat and rice straws after 15 d. Furthermore, SEM, FTIR and TGA analyses showed that C. unicolor pretreatment process had significant effects on corn stalk, rice and wheat straws’ structures. The newly isolated stain of C. unicolor demonstrated high lignin degradation potential that can provide effective, ecofriendly means of valorizing biomass to industrial useable raw-material.

Mechanical pretreatment of typical agricultural biomass on shape characterization and NO emissions during combustion

The impact of mechanical pretreatment of corn straw (CS), pea straw (PS), and wheat straw (WS), on shape characterization and NO emissions during combustion were investigated in this research. Particle size ranges were obtained and characterized their shape factors using Image J correction. The thermal properties and NO emissions of the different-sized particles were investigated by TG-MS and fixed-bed reactor. Compared with CS and PS, WS is more likely to break into smaller particles due to its moderate strength. Amine-N completely disappeared after pyrolysis, whereas pyrrolic-N and pyridinic-N were the main N functionalities in char-N. During the volatile burning stage, the maximum peak of NO concentration was 270, 354 and 311 ppm for CS, PS and WS, respectively. NO was detected at a steady level during the semicoke combustion stage, and the duration increased with particle size. The NO concentration decreased sharply in a short duration during the fixed carbon combustion stage.

Preparation of Samples for the Study of Rheological Parameters of Digested Pulps in a Bioreactor of an Agricultural Biogas Plant

The studies of the rheology of digested pulp from agricultural biogas plants have often been fragmentary and non-standardised due to their complexity and time-consuming nature. As a result of measurements, it was possible to develop a procedure and range of measurements for the correct determination of the parameters of the carrier substance. The applicability of the coaxial cylinder measurement system was demonstrated for assessing the rheological parameters of digested pulp from a fermenter that utilises agricultural biomass. To determine the characteristics of solid particles, the Zingg diagram was used, inter alia, allowing the comparison of particles from each fraction. The analysis of the shape and size of solid particles may help to describe the onset of motion of this phase, flow type, or sedimentation type. The authors propose a completely new research approach to obtain an appropriate, repeatable test conditions of medium, which is the carrier liquid from the biogas plant reactor. The proposed methodology and the scenario of the entire study make it possible to achieve scalable and comparable test results in any laboratory. The proposed solution eliminates the influence of most external factors on the sample and rheological measurements, and the effectiveness of the presented procedure was confirmed in tests.