Abstract
Carbon-13 n.m.r. spectroscopy is shown to be a valuable analytical tool—offering considerable advantages over other physical methods—for investigating the site, and in some cases the degree, of deuterium incorporation in several simple alkenes and also in various tertiary phosphine complexes of platinum(II). 13C N.m.r. data are presented for the alkenes, CH2CHC(CH3)2R (R = Et, Pr, and Bu) together with their partially deuteriated analogues and also for the complexes [M2Cl4L2](M = Pd or Pt; and L = PEt3, PPr3, PBu3, or PBut2Pr) together with the partially deuteriated analogues [M = Pt and L = PPr3(D), PBu3(D), or PBut2Pr(D)].
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