Abstract
AbstractSynthesis of dihydrochloride of (−)‐cis‐2,8‐dimethyl‐6‐[3H]‐2,3,4,4a,5,9b‐hexahydro‐1H‐pyrido[4,3b]indole by catalytic reductive dehalogenation of dihydrochloride of (−)‐cis‐2,8‐dimethyl‐6‐bromo‐2,3,4,4a,5,9b‐hexahydro‐1H‐pyrido[4,3b]indole is described together with the reaction conditions of the tritiation using 5% Pd/BaSO4 (UVVVR) in 0.1 M phosphate buffer pH 7.4. Specific activity of the product was 0.9 TBq.mmol−1, its radiochemical purity 96%.
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More From: Journal of Labelled Compounds and Radiopharmaceuticals
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