Abstract

Cryogenic high energy ball milling was used to synthesize nanocrystalline Cu and Cu99.5Zr0.5 alloys by mechanical alloying and consolidation by hot pressing at 550°C temperature. The grain size stability of nanocrystalline Cu is improved by the Zr addition. Microstructural characterization using X-ray diffraction and transmission electron microscopy provided evidence for the formation of a Cu–Zr alloy solid solution with nanocrystalline size after hot pressing. The alloy exhibited a higher hardness (3.31GPa), and shear strength (550MPa) than nano-crystalline pure Cu however, the electrical resistivity is increased in the alloy.

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