Abstract
The temperature dependence of the intensities of the (00l) X-ray reflections from a binary paraffin (C23H48-25 % C 24H50) was determined, in order to obtain structural parameters related to the molecular disorder and intramolecular defects. The long lattice spacing was also determined as a function of temperature. All these results are compared with the temperature dependence of the ratio of the two short lattice parameters. The clear correlation of all of these experimental results provides a close characterization of the molecular structures and their changes at the various solid state phase transitions.
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