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Cite Journal: RSC advances |  Publication Date: Jan 1, 2021 |
 Citations: 5 |  License type: CC BY-NC 3.0 |
Fast (60 kHz) magic angle spinning solid-state NMR allows very sensitive proton detection in highly paramagnetic organometallic powders. We showcase this technique with the complete assignment of 1H and 13C resonances in a high-spin Fe(ii) polymerisation catalyst with less than 2 mg of sample at natural abundance.
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