Abstract
It was found that fluorosulfonic acid is a very convenient source of deuterium fluoride by the simple deuterolysis reaction: FSO/sub 3/H + D/sub 2/O yields DF + DHSO/sub 4/. Although only half of the deuterium used is converted to DF, the reaction takes place at moderate temperatures and is practically quantitative at 100 deg C. (W.L.H.)
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