Abstract
The present investigation reports, the novel synthesis of nanoparticles Ni and NiO using thermal decomposition and their physicochemical characterization. The nanoparticles Ni powder have been prepared using [bis(2-hydroxyacetophenato)nickel(II)] as precursor. Transmission electron microscopy (TEM) analysis was demonstrated nanoparticles Ni with an average diameter of about 14–22 nm. The products were characterized by X-ray diffraction (XRD), TEM, high-resolution transmission electron microscopy (HRTEM) and Fourier transform infrared (FT-IR) spectroscopy. The magnetic property of Ni and NiO was studied with vibrating sample magnetometer (VSM).
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