Abstract
ABSTRACT In the present work, hydroxyapatite (HA)-50 wt.% TiO2 composite coating has been developed on Mg-alloy by laser cladding process using 400 W continuous wave fibre laser. A detailed microstructural characterisation has been done by using optical profilometry, field emission scanning electron microscopy (FESEM), energy-dispersive X-ray spectroscopy (EDS) and X-ray diffraction techniques. The wettability analysis has been done by the sessile method using hank’s solution. The average roughness is 0.5 μm for the Mg-1% Ca alloy and 1.45 μm for laser-cladded surface. The microstructure analysis shows uniform deposition with the presence of porosities, particles and few cracks on the top surface of laser-cladded surface. The composition analysis shows the uniform and homogeneous distribution of Ca, Ti, P, and O on the laser-cladded surface. The phase analysis shows the presence α, β phase in Mg-1% Ca alloy and the presence of Ca2P2O7, Ca3(PO4)2, CaTiO3 and TiO2 (rutile) phases in the laser-cladded surface. There is an improvement in wettability of the laser-cladded surface as compared to as-received Mg alloy.
Published Version
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