Abstract

This study investigates the effect of the α/C14 interface on the creep strength of α-Mg/C14–Mg2Ca eutectic alloy at 473 K under a stress of 40 MPa. The α/C14 interface is composed of terraces and steps, with terraces parallel to the (1101)α pyramidal plane of the α-Mg lamellae and to the (1120)C14 columnar plane of the C14–Mg2Ca lamellae. The creep curves of the alloy exhibit three stages: a normal transient creep stage, a minimum creep rate stage, and an accelerating stage. The minimum creep rate is proportional to the lamellar spacing, indicating that the α/C14 lamellar interface plays a creep-strengthening role. In the high-resolution transmission electron microscopy image captured of the specimen after the creep test, <a> dislocations can be mainly seen within the soft α-Mg lamellae, and they are randomly distributed at the α/C14 interface. In contrast, dislocations are rarely introduced in the hard C14–Mg2Ca lamellae. It is deduced that the α/C14 interface presents a barrier to dislocation gliding within the α-Mg lamellae and does not help rearrange the dislocations.

Highlights

  • Magnesium alloys are gaining interest as lightweight structural materials in the aerospace and automotive industries to achieve high fuel efficiency and reduce the emission of carbon dioxide [1]

  • The intermetallic phases with high thermal stability, which are available as covering phases [7,8] and/or precipitation phases [9,10], are essential for enhancing the high-temperature strength of heat-resistant magnesium alloys [11,12]

  • The2 Ca objective lamellae through a detailed observation; second, to quantitatively clarify the study were to elucidate the following three points by using a Mg–Ca alloy with interrelation between creep strength and λ, where λ was controlled by aging at 673 K; finethird, lamellar microstructure: first, to clarifyonthe orientation relationship and to clarify the role of the lamellar interface dislocation gliding, through the betwee and C14–Mg

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Summary

Introduction

Magnesium alloys are gaining interest as lightweight structural materials in the aerospace and automotive industries to achieve high fuel efficiency and reduce the emission of carbon dioxide [1]. The intermetallic phases with high thermal stability, which are available as covering phases [7,8] and/or precipitation phases [9,10], are essential for enhancing the high-temperature strength of heat-resistant magnesium alloys [11,12]. In the effec elucidate the following three points by using a Mg–Ca alloy with a α/C14 contrast, fine lamellar microstructure: first, to clarify the orientation relationship between α-Mg alloys. HRTEM observation; second, to quantitatively clarify the study were to elucidate the following three points by using a Mg–Ca alloy with interrelation between creep strength and λ, where λ was controlled by aging at 673 K; finethird, lamellar microstructure: first, to clarifyonthe orientation relationship and to clarify the role of the lamellar interface dislocation gliding, through the betwee and C14–Mg. HRTEM observation; second, to q observation of dislocation substructure of the creep specimens. A binary alloy of composition Mg–13.8 mass% Ca was cast at Mitsui Mining & Smelting ing, through the observation of dislocation substructure of the creep specimens

Experimental Section
Results and Discussion
Strain
Dislocation Analysis
Ca eutectic
Conclusions
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