Abstract
An electron-capture gas-liquid chromatographic assay was developed for the determination of clonazepam (as its methyl derivative) and of flunitrazepam and its N-desmethyl metabolite in blood. The method was used to measure blood levels in man following single oral 2-mg doses of clonazepam and flunitrazepam, and has a sensitivity limit of 0.5 to 1.0 ng of compound per milliliter of blood.
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