Abstract
Copper catalysed azide-alkyne cycloaddition have been undertaken involving as azide 1,12diazido-dodecane and 1,5-dibenzyl-3-propargyl-1,5-benzodiazepine-2,4-dione 1 and 7-chloro-1,5-dipropargyl-1,5-benzodiazepine-2,4-dione 2 as dipolarophiles. The reactions studied led exclusively in each case to 3-(1-azidododecyl-1,2,3-triazol-4-ylmethyl)-1,5- benzodiazepine-2,4-dione 3 and a di-1,2,3-triazolyl macrocyclic ligand 4. The structures of compounds isolated 3 and 4 have been elucidated on the basis of 1H NMR, 13C NMR and comfirmed by a single crystal X-ray diffraction studies.
Published Version
Talk to us
Join us for a 30 min session where you can share your feedback and ask us any queries you have
Schedule a callDisclaimer: All third-party content on this website/platform is and will remain the property of their respective owners and is provided on "as is" basis without any warranties, express or implied. Use of third-party content does not indicate any affiliation, sponsorship with or endorsement by them. Any references to third-party content is to identify the corresponding services and shall be considered fair use under The CopyrightLaw.
