Abstract
In situ/operando characterization techniques are widely used for studying dynamic processes and electrochemical, thermal, and mechanical properties of energy storage materials. It has become an essential tool to provide fundamental understanding of the material properties, reaction kinetics, and failure mechanisms, contributing to the advancement of the energy storage technologies. In this review, variety of in situ/operando techniques are compiled, and the experimental setups, attainable information, and limitations/requirements are explained in detail by introducing representative studies using the techniques Finally, challenges and future opportunities for the development of the advanced in situ/operando characterization techniques are discussed.
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