The technology on separation of the solid wastes at the municipal waste landfills obtaining solid waste and soil, which is sanitized with the use of natural sorbent "Agroionit" is suggested. It showed that sorbent "Agrionite" application in the amount of 16 % in absolutely dry matter could reduce the content of mobile forms of heavy metals up to MPC. To reduce the amount of sorbent up to 12 % pre-treatment of soil with lime in the amount of 0,4 % for the detoxification of zinc, which is slowly absorbed by Agrionite is required. Appropriate changes to the developed technology have been added, including the regulation of temperature and humidity of soil.