X-ray Tube Radiation Research Articles

Static X-ray differential phase contrast imaging via bidirectional-misalignment grating

Grating-based X-ray differential phase contrast imaging (GB-DPCI) offers excellent imaging contrast for soft tissues. Limited by the phase stepping of gratings, the conventional GB-DPCI leads to a high radiation dose. This study presents a static GB-DPCI method employing an analyzer grating with a misaligned structure in both vertical and horizontal directions. A signal retrieval algorithm is developed for this method to permit the use of neighboring pixels on the detector to approximate multiple phase stepping positions, thereby obtaining the phase contrast signal in a single exposure. This study reduces high radiation doses and time-consumption caused by phase stepping. The presented method is validated with datasets from a laboratory X-ray tube and synchrotron radiation. Considering synchrotron results as example, minimal improvements in Feature Similarity Index Measure are 2.48%, 6.31%, and 7.06% for absorption, dark field, and phase contrasts, and in Information-Weight Structure Similarity Index Measure are 3.24%, 16.07%, and 8.61%.

X-ray Fluorescence Analysis of the Elemental Composition of Tungsten, Nickel and Copper

The purpose of this work was to conduct an X-ray fluorescence analysis of the elemental composition of tungsten, nickel and copper metal waste using an Olympus Delta portable spectrometer.Methods. To determine the chemical composition of raw materials, samples of metal waste in the form of copper rods, tungsten rods of various diameters and scraps of nickel plates intended for recycling were examined. To determine the elemental composition of metal waste, the method of X-ray fluorescence analysis (XFA) was chosen. The X-ray fluorescence method is based on the ratio of the intensity of X-ray fluorescence to the concentration of elements in the sample. Samples irradiated with powerful X-ray tube radiation, in response, emit characteristic fluorescent radiation of atoms proportional to their concentration in the sample. This method allows us to qualitatively assess the elemental composition of complex samples without violating their physico-chemical properties with minimal time costs. The Olympus Delta spectrometer was used as an express analyzer of metals and alloys, with the help of which experimental data on the composition of metal waste of tungsten, nickel and copper were obtained.Results. Based on the conducted studies aimed at X-ray fluorescence analysis of the elemental composition of tungsten, nickel and copper metal waste using the Olympus Delta portable spectrometer, it was found that the samples of the studied metal waste correspond to the following grades of alloys: tungsten rod made of tungsten grade VA; nickel plate made of nickel grade PNK-0T1; copper rod made of copper grade M3r.Conclusion. The results obtained will allow further research on their processing by the method of electroerosive dispersion and reuse in the production of heavy tungsten alloys. Renovation of metal waste, including tungsten, nickel and copper metal waste, will contribute to resource conservation, import substitution and ensuring the technological sovereignty of the Russian Federation.

Pavlinsky Geliy Veniaminovich (1935–2023)

Pavlinsky Geliy Veniaminovich (1935–2023)

The Evaluation of Complementary Metal-Oxide Semiconductor (CMOS) in Smartphone to Test X-Ray Tube Radiation Leakage

Radiation detection method has been developed through years. It started from the complex module tools to simple handheld instrument. Recently, the more ease method has been developed with the help of smartphone application. To detect radiation using smartphone usually required the external tools connected to the phone as detector, but there is one application that did not. This application only required complementary metal-oxide semiconductor (CMOS) part of camera. The application is a game changer in radiation protection because nowadays smartphone is in everyone’s pocket. The application needs to be tested to ensure its effectiveness to detect radiation. The application has been tested by the previous research and it is effective to detect radiation. In this research, CMOS will be tested to detect radiation leakage of x-ray tube. The aim of this research is to find the effectiveness of CMOS in smartphone for radiation leakage detection of x-ray tube. The finding will help the radiation worker detect leakage radiation of x-ray tube using smartphone in case of the absences of surveymeter in the facility. The radiation from x-ray machine were detected and measured three times by Iphone 6s, Xs, and 11 using RadioactivityCounter. To ensure there was a leakage, surveymeter is used as a comparative modul. The data obtained from the experiment was analyzed using t-test. The result show that percentage error of Iphone 6s, Xs, and 11 Consecutively were 93.4%, 98.2%, and 98.9%. which mean CMOS in these said phone could detect and measured radiation ineffectively. This due to the low leaked intensity x-ray that came from x-ray machine. From the T-test anaysis found that only Iphone 11 had linear comparison to surveymeter

Microfocus X-ray Tubes

Introduction. X-ray inspection plays a unique role among all nondestructive testing methods for products and materials due to sufficiently high resolution and high penetrability. The present study is designed to consider the key features of microfocus X-ray sources, their areas of application, and main technical characteristics.Aim. The paper aims to systematize information and review modern X-ray radiation sources for the implementation of microfocus radiography.Materials and methods. The main designs of microfocus X-ray tubes (soldered and demountable) were considered relying on the experience of the St Petersburg State Electrotechnical University in developing and operating such equipment, as well as the experience and open-access publications of foreign researchers and developers. Data collected by leading research teams over the last ten years were analyzed.Results. The paper presents design features for each main type of microfocus X-ray tubes – soldered and demountable. All key structural elements are considered: an anode assembly, a cathode assembly, and a focusing system. The influence of anode target material on the X-ray tube radiation spectrum is shown. An original design of a liquid-anode microfocus X-ray tube is described to demonstrate its key features and advantages. In addition, the paper gives an overview of cathodes used in microfocus X-ray tubes (tungsten cathode and lanthanum hexaboride cathode), as well as providing a detailed description of calculations performed for focusing systems. Finally, the designs of modern X-ray tubes are presented.Conclusion. Modern X-ray tubes are high-tech products that allow for high-resolution research of various objects. The main advantage of testing performed with the use of X-ray tubes consists in high resolution (micron and submicron). The X-ray images of test objects used to determine their spatial resolution are given, which clearly illustrate the vast possibilities of this technology. In addition, ways to improve microfocus X-ray tubes are briefly discussed. The considered materials can be useful in selecting a nondestructive testing tool, as well as in developing and creating X-ray systems on the basis of microfocus X-ray tubes.

An Enumeration Survey on Diagnostic X-Ray Generators and Essential Safety Parameters in Mizoram, India

Introduction: Best radiography practice involves operational optimal machine performance, delivering cost-effective healthcare services under appropriate safety conditions for workers and the public. The present study aimed to investigate the safety status of diagnostic X-ray installations in Mizoram, India. Material and Methods: Linearity of time (sec), linearity of current (mA), output reproducibility, table dose (μGy/mAs), peak voltage (kVp) accuracy, and 16 essential safety parameters of 135 X-ray machines were considered in this study. A battery-operated dosimeter and wide-range digital kVp meter were used to measure output radiation and effective peak potential of X-ray tube. Data analysis was performed using SPSS software to obtain the mean, standard deviation, and coefficient of variation. Results: Among different electronic parameters, 59.2% linearity of time, 82.6% linearity of current, 89.7% kVp accuracy, 35.1% output reproducibility, and 92.8% table dose were beyond the acceptable limits. Based on 16 essential safety parameters, it was observed that 98.7% of X-ray machines did not receive proper quality assurance test, 1.9% of the installations employed lead-line patient entrance doors, 46.8% of the machines were operated without any protective barriers and 83.1% of the units were operated without personnel monitoring service. Conclusion: The present study had concluded with more problems than the previous studies in different parts of the world in this regard. Due to the absence of proper quality control (QC) programs, many installations did not follow standard installation guidelines. The authors recommended that proper QC should be implemented by the frequent monitoring of each and every diagnostic X-ray installation.

On the possibility of PhotoEmission Electron Microscopy for E. coli advanced studies

The novel approach was proposed for detailed high-resolution studies of morphology and physico-chemical properties concomitantly at one measurement spot of E. coli bacterial cells culture immobilized onto silicon wafer surface in UHV conditions applying PhotoEmission Electron Microscopy under Hg lamp irradiation. For the E. coli characterization scanning electron microscopy (electron beam) and X-ray photoelectron spectroscopy (X-ray tube radiation) were applied prior to PhotoEmission Electron Microscopy measurements. In spite of irradiation doses collected for the cell arrays we were successful in detection of high-resolution images even of single E. coli bacterium by PhotoEmission Electron Microscopy technique followed by detailed high-resolution morphology studies by scanning electron microscopy. These results revealed widespread stability of the E. coli membranes shape after the significant number of applied characterization techniques.

Calculation of air kerma inside the radiation field of X-ray tube

The air kinetic energy released per unit of mass (air kerma) quantity is of importance in both medicine and industry for evaluating the radiation field of X-ray tubes and also for calibrating the reference instruments. The air kerma spatial distribution inside the X-ray tube's radiation field is not uniform because of the heel effect phenomenon. In this paper, a combination of Monte Carlo N Particle eXtended (MCNPX) simulation code and artificial neural network (ANN) has been utilized to estimate the air kerma inside the radiation field of X-ray tube for a wide range of tube voltages (50–600 kV) which covers both medical and industrial applications. At first, an X-ray tube with an anode angle of 20° was simulated using MCNPX code. Next, in order to provide the required data for training the network, 1375 point detectors were placed in different positions inside the conical radiation field of the simulated X-ray tube and then the air kerma was calculated for tube voltages in the range of 50–600 kV with a step of 50 kV. The tube voltage and point detector's spherical coordinates including distance from target, tangential angle and polar angle were utilized as the 4 inputs and the air kerma was used as the output of the ANN. After training the ANN, the proposed ANN model could estimate the air kerma in every position inside the radiation field of X-ray tube for a wide range of voltages (50–600 kV) with a mean relative error (MRE) of less than 0.67%.

Spectral structure of a polycapillary lens shaped X-ray beam

Polycapillary X-ray optics is widely used in X-ray analysis techniques to create a small secondary source, for instance, or to deliver X-rays to the point of interest with minimum intensity losses [1]. The main characteristics of the analytical devices on its base are the size and divergence of the focused or translated beam. In this work, we used the photon-counting pixel detector ModuPIX to study the parameters for polycapillary focused X-ray tube radiation as well as the energy and spatial dependences of radiation at the focus. We have characterized the high-speed spectral camera ModuPIX, which is a single Timepix device with a fast parallel readout allowing up to 850 frames per second with 256 × 256 pixels and a 55 μm pitch defined by the frame frequency. By means of the silicon monochromator the energy response function is measured in clustering mode by the energy scan over total X-ray tube spectrum.

Determination of mass absorption coefficient in two-layer thin-film Cr/V and V/Cr systems by X-ray fluorescence spectrometry

A method is proposed for the determination of mass absorption coefficient in the analysis of two-layer thin-film V/Cr and Cr/V systems on Polikor substrates by X-ray fluorescence spectrometry. Simply fabricated and unified film layers formed by applying vanadium and chromium on polymer film substrates are used. Correction coefficients taking into account the attenuation of primary radiation of X-ray tube and analytical line of an element from the lower layer in the upper layer are calculated.

Computed Tomography Experiments on a Laboratory Multipurpose Diffractometer

Applications of soft (Co and Cu X-ray tube) and hard (Ag X-ray tube) radiation in computed tomography experiments on a laboratory X-ray diffractometer are presented. Using low energy (<10 keV) X-ray sources provide the possibility to investigate objects made of light (organic) materials in more detail compared to the high energy application. In case of metal or heavy element containing composites high energy (~20 keV) X-ray sources allow to obtain full 3D information on the samples without destroying them. These measurements allow both qualitative and quantitative analysis of porous materials, samples with oriented components, and solid compounds.

Optical properties of X-ray irradiated Cu<sub>6</sub>PS<sub>5</sub>I-based thin films deposited by magnetron sputtering

Introduction . Cu 6 PS 5 I crystals belong to a big family of compounds with argyrodite structure. They are characterized by high ionic conductivity. That’s why these materials are promising for creation of different type of modern devices such as batteries, supercapacitors, electrochemical sensors, etc. Studies of the influence of external factors on physical properties of Cu 6 PS 5 I materials are important to predict endurance, wear resistance and safety of devices made on their basis. Purpose . The purpose of the paper is to investigate the influence of X-ray irradiation on the optical properties of Cu 6 PS 5 I-based thin films as well as to perform the quantative and qualitative evaluation of the changes that have taken place in the structure “film-substrate” as a result of X-ray irradiation. Methods . Cu 6 PS 5 I-based thin films were deposited onto silicate glass substrates by non-reactive radio frequency magnetron sputtering. The film chemical composition was investigated by energy-dispersive X-ray spectroscopy. X-ray irradiation was performed at different exposition times (30, 60 and 120 min) using wideband radiation of Cu-anode X-ray tube with approx 400 W of power applied (33 kV, 13 mA). Optical transmission spectra of Cu 6 PS 5 I-based thin films were studied using MDR-3 grating monochromator. Results . Optical transmission spectra of X-ray irradiated Cu 5.6 P 1.7 S 4.9 I 0.8 , Cu 6.4 P 1.1 S 4.6 I 0.9 and Cu 8.0 P 0.7 S 3.6 I 0.7 thin films were studied at various irradiation times at room temperature. With irradiation time increase the red shift of the short-wavelength part of transmission spectra and interference maxima is revealed. In the X-ray irradiated thin films the Uhrbach behavior of the optical absorption edge is observed. Optical absorption edge for X-ray irradiated thin films is shifted to the long-wavelength region with irradiation time increase. It leads to the energy pseudogap decrease and Uhrbach energy increase. Dispersion dependences of the refractive index for the X-ray irradiated thin films have shown a slight dispersion of the refractive indices in the transparency region, increasing with approaching the optical absorption edge. With irradiation time increase the nonlinear increase of the refractive indices in the X-ray irradiated thin films is revealed. Conclusions. The influence of X-ray irradiation on optical properties of Cu 6 PS 5 I-based thin films was studied. Changes in optical parameters of the thin films were investigated and described. With irradiation time increase the decrease of energy pseudogap as well as increase of Uhrbach energy and refractive index values was observed. It was determined that with irradiation time increase the darkening and densitification of the thin films occur. The increase of Uhrbach energy indicates on increase of structural disordering induced by the influence of X-ray irradiation.

A comparative study on the total reflection X-ray fluorescence determination of lowZelements using X-ray tube and synchrotron radiation as excitation sources

Detailed total reflection X-ray fluorescence (TXRF) studies for the detection and quantification of low atomic number elements were carried out by using a laboratory dual source TXRF spectrometer equipped with a vacuum chamber and at the International Atomic Energy Agency multi-purpose end-station facility, operated at the XRF beamline of Elettra Sincrotrone Trieste, Italy. Multi-elemental standard aqueous solutions of low Z elements (F, Na, Al, S, K, Sc, and Ti) with different elemental concentrations of 2, 10, 20, and 30 µg/ml were prepared and measured in both setups. The measurements at the synchrotron setup were performed in a scanning mode across the sample residue and perpendicular to the incident beam in order to account properly for a possible non-uniform deposition of certain elements. The accuracy and the detection limits obtained from the TXRF measurements in both setups were determined and comparatively evaluated and assessed. Significant improvement in the TXRF detection limits at the synchrotron beamline end-station was obtained for the elements with Z ≤ 13 (Al). Copyright © 2017 John Wiley & Sons, Ltd.

뇌혈관 중재적시술에 있어 측방향 차폐체를 이용한 시술자 피폭 선량 저감화 방법 연구

The bi-plane cerebrovascular angiography radiation is done the radiation exposure at the forward and lateral direction as opposed to the one of the source. So, the exposure dose of radiation workers increases further. Therefore, the medical diagnostic radiation workers as well as patients is interested to ways to reduce the dose. The exposure dose of cerebral angiography and interventional radiology must be considered the primary radiation of X-ray tube directly, scattered primary radiation between lateral tube and lateral detector and relatively small secondary scatter radiation in the walls of room. The aim of study is that the exposure dose of primary and scatter radiation reduce as much as possible to install protection device of lateral protection than common shielding of table and ceiling. As a result, the dose of fluoroscopy was reduced approximately 3.64 times the gonads, thyroid approximately 3.13 times, 4.42 times around eyes. And the dose of DSA was reduced approximately 4.98 times the gonads, thyroid approximately 3.00 times, 1.67 times around eyes. Consequently, medical practitioners can be helpful for radiation dose-exposure for the lateral protection of bi-plane cerebrovascular angiography more than the common shield method in cerebrovascular angiography and interventional radiological procedures. Key Word: bi-plane cerebrovascular, radiation workers, interventional angiology procedures, lateral protection

3D analysis of micro-deformation in VHCF-loaded nodular cast iron by [formula omitted

The impact of very high cycle fatigue (VHCF) load conditions on the microstructure of specimens consisting of nodular cast iron is analyzed by means of micro-computed tomography (μCT) utilizing both monochromatic synchrotron radiation and polychromatic X-ray tube radiation. Using 3D μCT, the microstructure in the region of the smallest cross-sections of shouldered round specimens is imaged in different stages of the VHCF loading. By digital image correlation (DIC) of these tomograms strain fields are analyzed three-dimensionally. Strain levels in the range of a few percent were detected. It is proven that a localization of strain allows to predict the site of the crack which precedes and induces the macroscopic failure of the specimens.

An X-ray fluorescence method for determining the mass absorption coefficient in thin-film V/Ge and Cr/Ge bilayer systems

A new approach has been proposed for determining the mass absorption coefficient in the X-ray fluorescence characterization of V/Ge and Cr/Ge thin bilayer structures using simple-to-prepare unified layers grown by depositing vanadium or chromium on a polymer film. We have calculated correction coefficients that take into account the absorption of the primary X-ray tube radiation and that of the analytical line of an element from the lower layer in the upper layer.

Mutual influence of elements in x-ray fluorescence analysis of thin bilayer Ni/Ge-systems

A new approach to the determination of the layer thickness in x-ray fluorescence analysis of bilayer Ni/Ge-systems was proposed. The approach was based on accounting for the degree of attenuation in the upper layer of both the primary x-ray tube radiation and the analytical line of the lower-layer element and the fluorescence intensity amplification of the upper layer by radiation from lower-layer atoms.

Effect of Processing of the Focal Track of a Composite Anode on X-Ray Tube Characteristics

The impact of different methods of composite anode tungsten layer processing on X-ray tube radiation intensity is discussed. The results of the analysis of tungsten layer surface samples studied by various methods are reported. The results of the X-ray tube radiation intensity measurement are discussed for each sample.

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Compact pnCCD-Based X-ray Camera with High Spatial and Energy Resolution: A Color X-ray Camera

For many applications there is a requirement for nondestructive analytical investigation of the elemental distribution in a sample. With the improvement of X-ray optics and spectroscopic X-ray imagers, full field X-ray fluorescence (FF-XRF) methods are feasible. A new device for high-resolution X-ray imaging, an energy and spatial resolving X-ray camera, is presented. The basic idea behind this so-called "color X-ray camera" (CXC) is to combine an energy dispersive array detector for X-rays, in this case a pnCCD, with polycapillary optics. Imaging is achieved using multiframe recording of the energy and the point of impact of single photons. The camera was tested using a laboratory 30 μm microfocus X-ray tube and synchrotron radiation from BESSY II at the BAMline facility. These experiments demonstrate the suitability of the camera for X-ray fluorescence analytics. The camera simultaneously records 69,696 spectra with an energy resolution of 152 eV for manganese K(α) with a spatial resolution of 50 μm over an imaging area of 12.7 × 12.7 mm(2). It is sensitive to photons in the energy region between 3 and 40 keV, limited by a 50 μm beryllium window, and the sensitive thickness of 450 μm of the chip. Online preview of the sample is possible as the software updates the sums of the counts for certain energy channel ranges during the measurement and displays 2-D false-color maps as well as spectra of selected regions. The complete data cube of 264 × 264 spectra is saved for further qualitative and quantitative processing.