Wide Angle Research Articles

A wide angle beam scanning CRLH leaky-wave antenna with non-identical elements per unit-cells

In this research article, a wide-angle scanning leaky-wave antenna (LWA) based on the composite right/left-handed (CRLH) metamaterial (MTM) operating over the C-band spectrum for mobile applications is proposed, investigated, and realized. The proposed LWA includes nine CRLH-MTM-based unit-cells. The properties of CRLH-MTM have been applied using series slots and shunt metallic via-holes. Each unit cell consists of three patches, two external patches, and one smaller middle patch implemented between them. One slot has been etched on each external patch; the width of these two slots is unequal. Moreover, the distance of the middle patch with each side patch is different. The results show that using this method of realizing non-identical elements caused the achievement of proper return-loss at the transition frequency and provided the balanced CRLH metamaterial condition. Additionally, using CRLH-MTM properties by realizing series capacitance (slot) and shunt inductance (via-holes) made the wide-angle scant from backward to forward radiation pattern. The results demonstrate that the LW antenna with small dimensions of 251.5 × 30 × 1.575 mm3 operates over a frequency range of 4.8–6.13 GHz covering a wide beam scanning range from −63° to +65° with broadside radiation at the center frequency of 5.46 GHz. The radiation gain of the proposed antenna varies from 6.2–13.1 dB. The achievements confirm the effectiveness of the proposed methods to realize a high-performance LW-antenna with the advantages of simple design, low profile, low cost, and easy of manufacture for mobile applications.

The high-Q THz stereo metasurface sensor based on double toroidal dipole with wide operating angle bandwidth

A highly sensitive terahertz stereo metasurface sensor, characterized by a high quality factor (Q-factor) and based on dual toroidal dipole (TD) resonance, has been proposed. The optimal structural parameters are ascertained by comparing the pertinent parameters of the stereo and planar structures in relation to TD modal excitation. The effective excitation of the TD mode is demonstrated using the calculations of multipole scattered power, reflection spectra, surface currents, electric fields, and magnetic field distributions. It is crucial that the stereo metasurface exhibits simplicity and that the dual TD resonance can be readily excited through simple adjustments in the distance and height of the intermediate gap. It also demonstrates exceptionally high sensitivity and Q-factor, both of which are essential for sensing applications. Moreover, the proposed stereo terahertz metasurface sensor still shows excellent sensing performance in a wide range of incidence angles (±40°), which is of great significance for practical applications. In conclusion, this structure offers a novel design framework for high-performance terahertz sensors based on the TD mode.

GdWN3 is a nitride perovskite

Nitride perovskites ABN3 are an emerging and highly underexplored class of materials that are of interest due to their intriguing calculated ferroelectric, optoelectronic, and other functional properties. Incorporating novel A-site cations is one strategy to tune and expand such properties; for example, Gd3+ is compelling due to its large magnetic moment, potentially leading to multiferroic behavior. However, the theoretically predicted ground state of GdWN3 was a non-perovskite monoclinic structure. Here, we experimentally show that GdWN3−y crystallizes in a perovskite structure. High-throughput combinatorial sputtering with activated nitrogen is employed to synthesize thin films of Gd2−xWxN3−yOy with oxygen content y < 0.05. Ex situ annealing crystallizes a polycrystalline perovskite phase in a narrow composition window near x = 1. LeBail fits of synchrotron grazing incidence wide angle x-ray scattering data are consistent with a perovskite ground-state structure. Refined density functional theory calculations that included antiferromagnetic configurations confirm that the ground-state structure of GdWN3 is a distorted Pnma perovskite with antiferromagnetic ordering, in contrast to prior predictions. Initial property measurements find that GdWN3−y is paramagnetic down to T = 2 K with antiferromagnetic correlations and that the absorption onset depends on cation stoichiometry. This work provides an important path toward both the rapid expansion of the emerging family of nitride perovskites and understanding their potential multiferroic properties.

Investigation of the effect of elbow pipes of Ti6Al4V, 304 stainless steel, AZ91 materials on erosion corrosion by finite element analysis

Corrosion is the degradation of metals caused by chemical or electrochemical reactions with their environment. As a result of these reactions, undesirable conditions occur in the physical, chemical, mechanical and electrical properties of metals. These conditions cause parts made of metallic materials to become unusable. Erosion corrosion is one of the most common types of corrosion in fluid transfer. There are several methods for preventing erosion corrosion. First of all, some precautions should be taken to prevent wear. Intervention is very important in terms of cost, especially at the design stage. Measures such as wide angle bends, wall thickness of wear-resistant material and corrosion allowance can be taken, especially in applications where the flow direction needs to be changed. The aim of this study was to determine the effect of liquid fluid on erosion corrosion in Ti6Al4V, 304 stainless steel and MgAz91 elbow pipes by using the computer aided and finite element based AnsysWorkbench Explicit Dynamics module. For the design of the elbow pipe, SolidWorks was used for 3D studies. In the analysis of the pipe, the suitability of the pipe for the 3D model was examined. The effect of fluid rotation on the pipe walls and the effect of the pipe material on the flow along the pipe were determined. The standard k-e model based on the velocity-pressure relationship in continuous and steady flow was used for the flow calculations. The flow simulation showed that for all models the flow accumulation after rotation was more concentrated on the opposite walls of the pipe, as expected. The results obtained showed that the deformation in MgAZ91 material had the highest value at 9.14 × 10−8 mm. This situation has been interpreted to mean that it may vary depending on the flow rate automation. Designs on the old designs in the erosion structure of the liquid that occurs in the pipes with a new product design in the analysis design.

Assessing the effect of offline topography on electrical resistivity measurements: insights from flood embankments

Summary Electrical resistivity tomography (ERT), a geophysical imaging method, is commonly used on flood embankments (dykes or levees) to characterise their internal structure and look for defects. These surveys often use a single line of electrodes to enable 2D imaging through the embankment crest, an approach that enables rapid and efficient surveying compared to 3D surveys. However, offline variations in topography can introduce artefacts into these 2D images, by affecting the measured resistivity data. Such topographic effects have only been explored on a site-specific basis. If the topographic effects can be assessed for a distribution of embankment geometries (e.g. slope angle and crest width) and resistivity variations, it would allow for targeted correction procedures and improved survey design. To investigate topographic effects on ERT measurements, we forward-modelled embankments with different trapezoidal cross-sections sat atop a flat foundation layer with contrasting resistivity values. Each was compared to a corresponding flat model with the same vertical resistivity distribution. The modelling workflow was designed to minimise the effect of forward modelling errors on the calculation of topographic effect. We ran 1872 unique embankment forward models, representing 144 geometries, each with 13 different resistivity contrasts. Modelling results show that offline topography affects the tested array types (Wenner-Schlumberger, Dipole-Dipole, and Multiple-Gradient) in slightly different ways, but the magnitudes are similar, so all are equally suitable for embankment surveys. Three separate mechanisms are found to cause topographic effects. The dominant mechanism is caused by the offline topography confining the electrical current flow, increasing the measured transfer resistance from the embankment model. The two other mechanisms, previously unidentified, decrease the measured transfer resistances from the embankment model compared to a layered half-space but only affect embankments with specific geometries and resistivity distributions. Overall, we found that for typical embankment geometries and resistivity distributions, the resistivity distribution has a greater control on the magnitude of the topographic effect than the exact embankment geometry: the subsurface resistivity distribution cannot be neglected. 2D inversions are suitable when both the embankment is more resistive than the foundations and when the embankment's cross-sectional area is greater than 4 m2/m2 (area scaled to an embankment with a height of 1 m). Topographic corrections, 3D data acquisition or 3D forward models are required when these conditions are not met. These are demonstrated using field data from an embankment at Hexham, Northumberland, UK. Improving the accuracy of the resistivity values in ERT models will enable more accurate ground models, better integration of resistivity data with geotechnical datasets, and will improve the translation of resistivity values into geotechnical properties. Such developments will contribute to a better characterised and safer flood defence network.

The nano-organization structure of triple fluorocopolymer

Three nanostructures with size 37–130 nm discovered in the triple fluorocopolymer with different temperature past by X-ray pattern at small and wide angles. Two level of order nano-organization are determined which change with phase transitions above glass transition. The conformation TGTG′ of vinyledenfluoride microblockes passage in conformation zigzag at the ρ3′–ρ5′ transitions in triple fluorocopolymer different from polyvinyldifluoride.

Do anomalously dense hot Jupiters orbit stealth binary stars?

ABSTRACT The Wide Angle Search for Planets (WASP) survey used transit photometry to discover nearly 200 gas-giant exoplanets and derive their planetary and stellar parameters. Reliable determination of the planetary density depends on accurate measurement of the planet’s radius, obtained from the transit depth and photodynamical determination of the stellar radius. The stellar density and hence the stellar radius are typically determined in a model-independent way from the star’s reflex orbital acceleration and the transit profile. Additional flux coming from the system due to a bright, undetected stellar binary companion can, however, potentially dilute the transit curve and radial velocity signal, leading to underestimation of the planet’s mass and radius, and to overestimation of the planet’s density. In this study, we cross-check the published radii of all the WASP planet-host stars, determined from their transit profiles and radial velocity curves, against radiometric measurements of stellar radii derived from their angular diameters (via the infrared flux method) and trigonometric parallaxes. We identify eight systems showing radiometric stellar radii significantly greater than their published photodynamical values: WASPs 20, 85, 86, 103, 105, 129, 144, and 171. We investigate these systems in more detail to establish plausible ranges of angular and radial velocity separations within which such ‘stealth binaries’ could evade detection, and deduce their likely orbital periods, mass ratios, and flux ratios. After accounting for the dilution of transit depth and radial velocity amplitude, we find that, on average, the planetary densities for the identified stealth binary systems should be reduced by a factor of 1.3.

A comprehensive study on active mixer performance using liquid metal droplets: an experimental approach

In this experimental study, we delve into the performance of an active mixer that utilizes liquid metal droplets. Our mixer configuration follows an innovative Y-type design, where two liquid metal-based pumping mechanisms operate within the minichannel inlet branches. By applying alternating current voltage to both sides of the liquid metal, we induce a surface tension gradient, propelling the fluid from the reservoirs toward the minichannel. Notably, the two entering liquids are distinctly colored, allowing us to quantify mixing using a Mixing Index (MI) definition and image processing techniques. Our investigation centers on four key variables governing mixer performance: applied voltage, liquid metal droplet diameter, input angle between the branches, and minichannel width. Given the experimental nature of our research, we employ a central composite design method within the framework of design of experiments (DoE). From our obtained experimental results, we establish correlations between MI and the other variables. Our examination of the four mentioned parameters revealed that liquid metal droplet diameter exerts the most significant influence on the mixing index. Following this, in descending order of impact, we find applied voltage, input angle, and channel width. In the optimal dimensions of our mixer, we achieve a remarkable maximum MI of 0.867.

Wheel path planning for flute grinding of non-cylindrical solid end-mills based on circular arc projection

Flute grinding is a crucial process in solid end-mill manufacturing, because the generated flute parameters, i.e. helix angle, rake angle, core radius, and flute width, have significant effects on the cutting performance of end-mills. However, the flute grinding of non-cylindrical solid end-mills is still challenging due to the variation of the flute parameters along the tool axis. This paper proposes an accurate and efficient method of wheel path planning for flute grinding of non-cylindrical solid end-mills based on circular arc projection. The wheel path determined by the new method can accurately generate the designed helix angle, rake angle, core radius, and flute width, even if all of these parameters vary along the tool axis. The helix angle and rake angle are ensured by the conjugate condition between the wheel surface and the cutting-edge curve. Based on circular arc projection, equivalent errors of the core radius and flute width are introduced to quantify the machining errors of the two parameters, without the need to predict the flute profile. Simulations and experiments are conducted to validate the proposed method. Three types of non-cylindrical end-mills i.e. tapered end-mill, tapered barrel end-mill, and barrel end-mill, are considered in the validation. The measured results indicate that the generated flute parameters coincide well with the designed ones at different axial positions of the end-mills.

Experimental study on the mechanical behavior of laminates made by fiber steering: influence of fiber angle and tow width

Abstract This work considers the effects of fiber trajectory and prepreg width on the material strength and failure behavior of variable stiffness composites. The test matrix was designed according to commonly used fiber placement trajectory and width of prepreg in engineering. Different trajectories were compared for tensile, compressive, bending, shear and CAI strengths. For tensile and compressive performance, curved ply specimens have varying degrees of decrease compared to straight ply specimens; For shear and bending performance, the optimal layup sequence is [±45/〈30|45〉]. For impact toughness, curved ply is significantly higher than straight ply, and the CAI strength of straight ply exceeds that of curved ply. For variable stiffness laminate with different fiber angles and tow widths, the maximum tensile, compressive and CAI strengths were reduced by up to 66%, 56%, and 27%, and the maximum bending strength, shear strength and impact toughness were increased by up to 53%, 23%, and 10.3%, respectively. The increase in width of prepreg leads to an increase in defects between fiber bundles which weakens the tensile/compressive performance but enhances the shear/bending performance.

The effect of polylactic acid ordering on the long-term corrosion protection capacity of biodegradable magnesium alloys

The polylactic acid (PLA) coatings of different crystallinity were prepared on biodegradable Mg-2.2Zn-0.3Ca alloy wires to improve the long-term anti-corrosion properties. The composition characteristics and microstructure of the samples were investigated by differential scanning calorimetry (DSC), Fourier transform infrared spectroscope (FTIR), wide angle X-ray diffraction (WAXD) and scanning electron microscope (SEM). The corrosion resistance of all samples was investigated by immersion tests and electrochemical techniques in vitro simulated body fluid (SBF). The results indicated heat treatment improved the crystallinity of PLA coating and heated-coating performed protective behaviors in the short and long-term immersion. The corrosion rate of heated samples was lower than that of unheated samples and exhibited superior long term protective effect for Mg alloy wires. The lifetime of heated sample (H2) increased significantly from 33 to 55 days. The initial electrochemical performance of unheated coating was better than heated coating, but it declined more rapidly during the long-term immersion. These results indicated that PLA coating could not ignore the effect of its crystallinity to anti-corrosion ability, and only the suit heat treatment makes PLA coating more ordering and achieves higher corrosion resistance in vitro immersion. Therefore, it has promising potential by controlling effectively the PLA ordering for surgical implant applications.

Angle-insensitive perfect light transmission and absorption in one-dimensional photonic crystal heterostructures

Abstract Prefect light transmission in metamaterials typically suffers a frequency shift as the incident angle of wave increase, limiting their applicability across wide angles. One-dimensional photonic crystal heterostructures, with elliptic-shaped equi-frequency contours, exhibit angle-insensitive properties. However, there remains an inevitable blue shift in the optical response as the incident angle increases. In this work, we present two photonic crystal heterostructures, one of which is composed of the optical phase-change material Sb2S3. By combining two heterostructures with distinct Zak phases, we achieve perfect light transmission. Specifically, as incident angle of wave increases, the transmission peak can be strictly maintained without a frequency shift by tuning the phase (refractive index) of Sb2S3. Moreover, by jointing the heterostructures with a thin silver film, we demonstrate a Tamm plasma polariton mode with angle-insensitive property. This mode can facilitate angle-tolerant light absorption. Our work provides an alternative way to designing high angle-tolerant and tunable devices.

Experimental demonstration of a silicon nanophotonic antenna for far-field broadened optical phased arrays

Optical antennas play a pivotal role in interfacing integrated photonic circuits with free-space systems. Designing antennas for optical phased arrays ideally requires achieving compact antenna apertures, wide radiation angles, and high radiation efficiency all at once, which presents a significant challenge. Here, we experimentally demonstrate a novel ultra-compact silicon grating antenna, utilizing subwavelength grating nanostructures arranged in a transversally interleaved topology to control the antenna radiation pattern. Through near-field phase engineering, we increase the antenna’s far-field beam width beyond the Fraunhofer limit for a given aperture size. The antenna incorporates a single-etch grating and a Bragg reflector implemented on a 300-nm-thick silicon-on-insulator (SOI) platform. Experimental characterizations demonstrate a beam width of 44°×52° with −3.22 dB diffraction efficiency, for an aperture size of 3.4 μm×1.78 μm. Furthermore, to the best of our knowledge, a novel topology of a 2D antenna array is demonstrated for the first time, leveraging evanescently coupled architecture to yield a very compact antenna array. We validated the functionality of our antenna design through its integration into this new 2D array topology. Specifically, we demonstrate a small proof-of-concept two-dimensional optical phased array with 2×4 elements and a wide beam steering range of 19.3º × 39.7º. A path towards scalability and larger-scale integration is also demonstrated on the antenna array of 8×20 elements with a transverse beam steering of 31.4º.

Deep neural network-enabled multifunctional switchable terahertz metamaterial devices

Under the support of deep neural networks (DNN), a multifunctional switchable terahertz metamaterial (THz MMs) device is designed and optimized. This device not only achieves ideal ultra-wideband (UWB) absorption in the THz frequency range but enables dual-functional polarization transformation over UWB. When vanadium dioxide (VO2) is in the metallic state, the device as a UWB absorber with an absorption rate exceeding 90% in the 2.43–10 THz range, with a relative bandwidth (RBW) of 145.2%, and its wideband absorption performance is insensitive to polarization. When VO2 is in the insulating state, the device can switch to a polarization converter, achieving conversions from linear to cross polarization and from linear to circular polarization in the ranges of 4.58–10 THz and 4.16–4.43 THz, respectively. Within the 4.58–10 THz range, the polarization conversion ratio approaches 100% with an RBW of 74.3%, the polarization rotation angle is near 90°. Within the 4.16–4.43 THz range, the RBW is 6.29% and the ellipticity ratio approaches 1, Moreover, the effects of incident angle and polarization angle on the operational characteristics are studied. This THz MMs due to its advantages of wide angle, broad bandwidth, and high efficiency, provides valuable references for the research of new multifunctional THz devices. It has great application potential in short-range wireless THz communication, ultrafast optical switches, high-temperature resistant switches, transient spectroscopy, and optical polarization control devices.

Supraspinal Activation Induced by Visual Kinesthetic Illusion Modulates Spinal Excitability.

Repetitive passive movement (RPM) enhances reciprocal inhibition. RPM is more effective when performed rapidly and at wide joint angles. However, patients with limited joint range of motion may not receive the most effective RPM. Therefore, having an alternative method for performing RPM in patients who cannot perform actual exercise due to limited joint motion is necessary. This study investigated the effects of RPM on spinal excitability using a visual kinesthetic illusion. Participants included 17 healthy adults (7 women). Measurements were taken before, during, and immediately after the intervention. We established two intervention conditions: the control condition, in which participants focused their attention forward, and the illusion condition, in which participants watched a video about RPM. F-waves from the tibialis anterior and soleus muscles were measured, and F-wave persistence and F/M amplitude ratios were analyzed. Under the illusion condition, compared with the preintervention condition, the F/M amplitude ratio of the tibialis anterior increased by approximately 44% during the intervention (p < 0.05), whereas the F-wave persistence of the soleus decreased by approximately 23% from the immediate start of the intervention (p < 0.05). This study suggests that a visual kinesthetic illusion can increase the spinal excitability of the tibialis anterior, whereas reciprocal inhibition can decrease the spinal excitability of the soleus.

RSM-BASED STATISTICAL APPROACH TO ENHANCE THE COMPRESSIVE PERFORMANCE OF ABS P400 PARTS FABRICATED VIA FDM TECHNOLOGY

This research investigates the performance of ABS P400 parts under compressive loading. These ABS P400 parts are fabricated by fused deposition modeling (FDM) process using omnidirectional printing. The effects of three critical parameters, raster angle (A), air gap (B), and raster width (C), each at three different levels, were analyzed on three different performance measures, i.e. total deformation up to failure ([Formula: see text]) measured in %, maximum energy ([Formula: see text]) in MJ/m3 and break energy ([Formula: see text]) in MJ/m3. Results of experimentations were analyzed using analysis of variance (ANOVA), perturbation curve and 3D surface plots. The research established the anisotropic nature, durability and less brittleness of the FDM fabricated ABSP400 part, which leads to lower strength and also influence the energy absorbing behavior while deformation under compression. Complex relationships were exhibited between the chosen parameters and studied measures. It was also observed that [Formula: see text] is noticeable due to less brittleness of ABS P400 however, [Formula: see text] and [Formula: see text] vary in a contradictory fashion with changes in process parameters. The models were validated using normality plots. Multi-objective optimization was done using the desirability approach to determine the optimal combination of FDM process parameters for optimum responses. The desirability result showed that the optimized input parameter is [Formula: see text][Formula: see text]mm, and [Formula: see text][Formula: see text]mm which yield maximized optimum responses as [Formula: see text]%, [Formula: see text][Formula: see text]MJ/m3, and [Formula: see text][Formula: see text]MJ/m3. The work not only reflects the effect of three FDM parameters on the total deformation up to failure ([Formula: see text] in %) but, in addition, energy absorption behavior of FDM parts under compression is also investigated. The study on the behavior of energy at ultimate stress or ultimate load and breaking stress or breaking load were rarely investigated in earlier research which reflects the novelty of our research.

Wide scan angle multibeam conformal antenna array with novel feeding for mm-wave 5G applications

This paper presents a low-profile wide scan angle multibeam conformal antenna array system with a novel feeding network for 28 GHz mm-wave 5G applications. The proposed antenna system utilizes two conventional branch-line couplers as its beamforming network. A novel feeding technique is applied to generate 7 beams with these couplers that are usually capable of generating 2 beams. The proposed solution provides a wide scanning range with a minimum realized gain of 5 dBi from −90° to 90° owing to this feeding approach and the peculiar placement of the array elements on a 0.15 mm thick R-F775 bendable substrate. The generated beams at their steer direction have the minimum and maximum gain values of 6.5 dBi and 9.7 dBi, respectively. A low-cost PCB manufacturing technique based on soft lithography and wet etching is used. The system dimensions excluding extra connector sections are 67×15×3mm3. The proposed flexible design is suitable for lightweight 5G communication systems and handsets with its compact low-complexity beamforming network, and wide 180° continuous covering angle.

A perfect absorber based on a VO2-tunable Fabry–Perot cavity: an analysis of periodic oscillation absorption characteristics

Terahertz metamaterial absorbers (TMAs) have garnered significant attention as vital electromagnetic wave-absorbing devices. In this study, we designed a terahertz metamaterial absorber (TMA) utilizing an asymmetric Fabry–Perot nanocavity comprising vanadium dioxide (VO2), gold (Au), and polyimide. The TMA exhibits five perfect absorption peaks within 0.1 THz to 10 THz, with an absorption rate exceeding 97%, peaking at 99%. The absorption rate oscillates periodically between 0 and 1, and its oscillating absorption peak can be determined by f m ( fm=(2m+1)c0/(4tε2 ), while tunability of the absorption rate between 15% and 97% is achievable by adjusting the conductivity of (VO2) (2×102∼2×105S/m). The physical mechanism of the absorption peak was analyzed by simulation and compared with theoretical analysis. The results show that the absorption peak of the absorber’s absorptivity can be insensitive to polarization and has a wide absorption angle of 80% up to 40◦ or more. Importantly, the thickness of the absorber (VO2) layer can be calculated from the desired absorption frequency and dielectric constant of the interlayer medium, d=ε0/μ0/σ , thus reducing the need for redesigning different resonant layer patterns. This work provides a new perspective on terahertz absorber design.

Metamaterial Broadband Absorber Induced by Synergistic Regulation of Temperature and Electric Field and Its Optical Switching Application.

Nowadays, metamaterial absorbers still suffer from limited bandwidth, poor bandwidth scalability, and insufficient modulation depth. In order to solve this series of problems, we propose a metamaterial absorber based on graphene, VO2, gallium silver sulfide, and gold-silver alloy composites with dual-control modulation of temperature and electric field. Then we further investigate the optical switching performance of this absorber in this work. Our proposed metamaterial absorber has the advantages of broad absorption bandwidth, sufficient modulation depth, and good bandwidth scalability all together. Unlike the single inspired layer of previous designs, we innovatively adopted a multi-layer excitation structure, which can realize the purpose of absorption and bandwidth width regulation by a variety of means. Combined with the finite element analysis method, our proposed metamaterial absorber has excellent bandwidth scalability, which can be tuned from 2.7 THz bandwidth to 12.1 THz bandwidth by external electrothermal excitation. Meanwhile, the metamaterial absorber can also dynamically modulate the absorption from 3.8% to 99.8% at a wide incidence angle over the entire range of polarization angles, suggesting important potential applications in the field of optical switching in the terahertz range.

Monitoring the dynamics of nanozeolite formation by combined in situ coherent small angle X-ray scattering techniques

Understanding the dynamics of zeolite formation is key to synthesising high-quality zeolitic materials with controllable properties, in order to develop more efficient and performant materials. X-ray photon correlation spectroscopy (XPCS) using coherent X-rays offers new possibilities for in situ observation of nano to micron-scale fluctuation dynamics during crystal growth. An in situ cell, which is capable of collecting time-resolved coherent X-ray scattering data under hydrothermal conditions has been developed and used to study, by in situ XPCS combined with small and wide angle X-ray scattering, zeolite formation and dynamics. Analysis of the results using two-time correlations enables to accurately identify the successive growth and crystallisation steps, revealing the dissolution process of the LTA topology during the SOD growth. This approach opens a powerful new avenue for studying the dynamics of nanomaterials formation, phase transitions and growth processes under in situ conditions that will enable profound insights into the nanoscale synthesis mechanisms.