ABSTRACT A rectangular slit weir is used to measure small flows, namely, those flows less than 5 L/s and contraction ratios (b/B) less than 0.25. In the present study, flow tests were conducted in a laboratory setup with various contraction ratios (b/B) under models A (b/B = 1/12), B (b/B = 1/8), C (b/B = 1/6), D (b/B = 5/24), and E (b/B = 1/4). The dimensional analysis revealed that b/B, the height of the flow on the crest of the weir to the height of the weir crest (h/P), the Reynolds number (Re), and the Weber number (We) are effective parameters for predicting the discharge coefficient of the slit weir. The experimental results indicated that the discharge coefficient is variable for different contraction ratios; the maximum average discharge coefficient was achieved at the lowest b/B (Model A), with a value of 0.72. The minimum average discharge coefficient obtained in Model B equals 0.639. In addition, former prediction equations were compared with the obtained experimental data, and the minimum, average, and maximum errors were calculated. Furthermore, a relationship was established for deriving the discharge coefficient in slit weirs with R2 = 0.9212, RMSE = 0.02244, and MAE = 0.0134 based on the obtained experimental data with four effective parameters, b/B, h/P, Re, and We.