Water resources occupy a vital position regarding the source of human hope for longevity and significant shortfalls on the strive towards sustainable development globally. Host communities to quarry companies without a water treatment plant are greatly affected by use of untreated water. This research highlights statistical evaluation and quality analysis of water resources around a quarry site in FCT Nigeria. The study engaged biological assay, physiological and chemical analysis to quantify contamination levels in the water resources and obtained data were subjected statistically using Pearson’s Correlation, descriptive statistics, Levene’s test for homogeneity and one–way analysis. The physiochemical analysis revealed the water resources to have high turbidity value in 58.3% of sampled population while nitrate concentration and electrical conductivity value were very low. The bioassay revealed presence of coliform bacteria in 100% of sampled population while thermotolerance count discovered disease-causing-pathogens in 41.7% of sampled population. Chemical analysis revealed that Pb, Cr, Ni and As were 91.7%, 83.3% 100% and 100% above recommended permissible limits for sampled population. These results suggests that water resources in this study is unsafe and holds a health-treat with regards to the contaminations inherent in them. Statistical evaluation revealed average positive linear relationship between heavy metal concentration suggesting close relationship of contamination source. Observed strong positive linear relationship between lead and copper, nickel and chromium as well as nickel and arsenic in the scatterplot depicts same source of contamination.