Surface Roughness Values Research Articles

Comparative Analysis of Surface Roughness and Plastic Deformation of Reciprocating Instruments after Clinical Use.

This study assessed the surface topography and plastic deformation (PD) of new and used contemporary reciprocating instruments. Twenty-six WaveOne Gold (WOG) and EdgeOne Fire (EO) instruments were photographed under magnification. The instruments were randomly assigned to a control group of new instruments preserved for surface roughness analysis (n = 6 each), or to an experimental group to shape the root canal system of a single molar (n = 20 each), making a total of four groups (WOGnew, EOnew, WOGused, EOused). Used instruments were also photographed after instrumentation. The presence of fractures was registered. Preoperative and postoperative images were randomly ordered for evaluation. Two blinded calibrated examiners evaluated the presence of PD. Inter-observer agreement was calculated with the Kappa coefficient (K = 0.89). 3D profilometry was also used for the surface roughness analysis of six randomly selected instruments from the WOGused and EOused groups. Chi-square and two-way ANOVA tests were used to, respectively, compare PD and changes in surface roughness among the groups. No instruments fractured; however, a significantly greater percentage of EO instruments suffered plastic deformation than WOG instruments (p < 0.001), (OR = 11.09 (CI 95% 2.6-56.3)). The overall surface roughness was higher for most parameters in the EO instruments (p < 0.05). Single uses of EO instruments produced significantly higher chances of PD and increased surface roughness values compared to WOG.

The effect of laser therapy for the treatment of dentin hypersensitivity on surface roughness and bacterial adhesion

The aim of the study was to measure the degree of dentine surface roughness caused by five distinct lasers used to treat dentine hypersensitivity, as well as to evaluate the subsequent bacterial colonization on these irradiated surfaces. Sixty human maxillary premolar teeth without caries or restoration which were extracted for periodontal reasons were used in this study. Five different types of lasers were applied to the root dentin surface. Tested samples were divided into six groups of 10 samples each; control, diode (810 nm), diode (980 nm), Nd: YAG, Er: YAG, and Er, Cr: YSGG laser groups. The arithmetic mean of the surface roughness values (Ra) and the average roughness over a measurement area (Sa) were measured pre- and post-application using any of the laser types. Swab samples were then collected from the dentin surface. Following a 24-hour incubation period at 37 °C, the colony forming units were counted using a stereoscope. The results demonstrated a statistically significant difference in the surface roughness values pre- and post-application (Ra and Sa, respectively) in the Er, Cr: YSGG laser group (p = 0.037,p = 0.007). No significant difference was observed in the other groups (p > 0.05). There was no statistically significant difference in the number of bacterial colonies observed between the test and control groups. Diode and Nd: YAG lasers showed either a decrease or no change in surface roughness; however, the hard tissue lasers (Er: YAG, Er, Cr: YSGG) showed an increase. The Er: YAG and Nd: YAG laser groups exhibited decreased bacterial adhesion compared to the other groups.

Investigation of open air and under water laser surface texturing on surface roughness and wettability of Al-Mg alloy

Aluminum-Magnesium (Al-Mg) alloy is widely used in aerospace and marine related applications due to its high corrosion resistance, tensile strength and ductility properties. However, due to hydrophilic nature, its applications are restricted in areas where water absorption may cause problems like corrosion. In this research work, high speed laser texturing was carried out on Al-Mg alloy (AA5754) to improve hydrophobic properties of the material surface. Four different types of pattern, namely lines, grids, concentric circles and concentric rectangles were created on the material surface using a nanosecond fiber laser. Scanning speed was varied at two levels i.e., 500 mm/s and 1000 mm/s. Line density of texture designs was also varied at two levels of 10 lines per mm and 15 lines per mm. The texturing process was carried out in two different processing environment namely open air and in underwater condition. Distilled water with 1 mm thickness above the surface was used during underwater texturing condition. Surface morphology, surface roughness and wettability of all the surfaces were studied for all the experimental conditions. It was observed that lower scanning speed of 500 mm/s resulted in higher values of surface roughness and contact angles. Also, larger texture density leads to lower surface roughness and contact angles for all the pattern designs. Among all the studied texture patterns, grid structures, textured at 500 mm/s of scanning speed resulted in largest surface roughness and surface hydrophobicity.

Surface roughness of different types of resin composites after artificial aging procedures: an in vitro study

BackgroundThe temperature changes, chemical agents, and brushing activity that resin composite restorations are exposed to in the oral environment can cause changes in surface roughness. In this study, the aim was to investigate in vitro the clinical one-year surface roughness changes of different types of composites (flowable or conventional) from the same companies by subjecting them to immersion in solutions, brushing, and thermal cycling procedures to simulate intraoral conditions.MethodsFour different resin composite brands were included in the study using both their conventional (Charisma Smart, 3M Filtek Ultimate Universal, Omnichroma, Beautifil II) and flowable resin composites (Charisma Flow, 3M Filtek Ultimate Flowable, Omnichroma Flow, Beautifil Flow Plus F00), giving 4 groups with 2 types of resin composite in each. 40 samples were prepared for each group/resin type, for a total of 320 samples. After initial surface roughness measurements by a mechanical profilometer, the samples were divided into 4 subgroups (n = 10) and immersed in solutions (distilled water, tea, coffee, or wine) for 12 days. The samples were then subjected to 10,000 cycles of brushing simulation and 10,000 cycles of thermal aging. Surface roughness measurements were repeated after the procedures. For statistical analysis, the 3-way analysis of variance and the Tukey test were used (p < 0.05).ResultsIt was concluded that composite groups and types had an effect on surface roughness at time t0 (p < 0.001). At time t1, the highest surface roughness value was obtained in the Beautifil-conventional interaction. When the surface roughness values between time t0 and t1 were compared, an increase was observed in the Beautifil II and Beautifil Flow Plus F00, while a decrease was observed in the other composite groups.ConclusionComposite groups, types, and solutions had an effect on the surface roughness of resin composites. After aging procedures, it was concluded that the Beautifil group could not maintain the surface structure as it exceeded the threshold value of 0.2 μm for bacterial adhesion.

Fabrication and growth mechanism of Al-Si coatings deposited on Mo substrate by hot dip plating technology

The Al-Si coatings with a low surface roughness were deposited on Mo substrate via the hot-dip plating technology, and the effects of deposition parameters on the microstructure, phase composition and surface roughness were systematically investigated. The results show that the hot-dip Al-Si coating is consist of a Mo(Si, Al)2 inner layer and an Al(Si)-Mo(Si, Al)2 outer layer. The coating surface is composed of Si(70.21–92.66 at%)-Al alloy phase containing Mo (Si, Al)2 grains and Al(73.83–92.32 at%)-Si alloy phase. With the increase of deposition temperature and the extension of time, the average grain area of Mo (Si, Al)2 increases from 0.264 μm2 to 0.623 μm2. The coating surface becomes smoother with the increase of deposition temperature, while rougher with the time. The maximum and minimum average surface roughness(RSa) values of the coating are 0.847 and 0.431μm, respectively. The coating thickness increased with the increase of deposition temperature and times. When the deposition temperature is 1000 ℃, the thickness value of the Mo (Si, Al)2 layer of the coating increases in a parabolic law with deposition time, and the Kp(reaction rate constant) is 4.5 ×10−13 m2/s. The growth of coatings is essentially a process of depositing Al, Si elements in the form of Mo (Si, Al)2 intermetallic compounds on Mo substrate.

DEVELOPMENT AND PERFORMANCE EVALUATION OF A MODEL CUTTING FLUID DEVELOPED FROM SHEA BUTTER OIL

This research was carried out to develop a model cutting fluid from Shea Butter oil and evaluate its performance in relation to temperature and surface roughness when compared to a commercial cutting fluid. The effectiveness of the cutting fluid was evaluated on a mild steel using a turning operation on the lathe machine. Temperature variations during the turning operation were measured using an infra-red gun thermometer while surface roughness was evaluated by employing a surface roughness tester. In this work Taguchi method was used to guide the selection of machine parameters such as cutting speed (rev/min), feed rate (mm/rev), and depth of cut (mm). Using Minitab, the cutting temperature and resulting surface roughness were measured for both the developed cutting and commercial fluids. The results obtained for the average cutting temperature of ~ 30oC and overall surface roughness value of 0.32μm for shea butter oil show a significant difference from that of ~ 35oC and 0.47 μm respectively for commercial grade cutting fluids. These results show that the shea butter oil-based cutting fluid not only exhibits great potential but also surpasses the current capabilities of commercial cutting fluids in terms of its cooling and surface finishing performances.

STUDY OF INNER AND OUTER POCKET CHARACTERISTICS USING AREA ROUGHING METHOD

Pocket milling is one of the CNC milling processes. This research aims to analyze the characteristics of pocket milling using Area Roughing on surface roughness and machining time. The method applied is experimental research on the Area Roughing method for working on inner and outer pockets. Research variables include depth cut 0.5, 1, 1.5, and 2 mm, stepover percent 40, 50, and 60%. The test is in the form of surface roughness value, while the analysis of the machining process is the time during the milling process. The workpiece material is 2024 aluminum and a flat endmill tool with a diameter of 12 mm. The expected result is the parameter that has the most optimal value for the processing time and surface roughness value. So it can be a guide for milling processes, especially those that use Area Roughing. The machining results show that the faster machining time results from larger settings for depth cut and stepover percent. Average machining time increase of 28%. Meanwhile, the surface roughness value will increase as the depth cut and stepover settings increase, namely 17.65% for the outer pocket and 18.61% for the inner pocket. The surface roughness value of the ordering results ranges from 2.4-4.8 µm.

Examination of Surface Hardness and Roughness of AISI 1050 Steel Material in Milling Based on Surface Processing Conditions

It is known that material hardness and surface conditions have a significant impact on the operating life of machine elements working with each other. In this study, Surface roughness values obtained depending on processing conditions and hardness changes on the machined surfaces during milling of AISI 1050 steel were examined. In experimental studies, ideal machining conditions were determined by taking into account surface roughness values and hardness changes using the Taguchi L18 experimental design method. In all experiments, it was observed that the lowest surface hardness was achieved under dry conditions when 6500 1/min speed, 4000 mm/min feed rate, and 0.4 mm cutting depth values were applied. When the speed increased from 5500 1/min to 6000 1/min and the feed rate increased from 4500 mm/min to 5000 mm/min, improvements in surface quality were observed in both machining conditions. In conclusion; In experiments where coolant was applied at high cutting speeds, it was determined that surface hardness and surface roughness values were higher than in dry machining conditions.

The effect of simulated food liquids on the surface structure and solubility of various esthetic restorations

Aims: The aim of this study is to investigate the surface roughness and solubility of restorative materials when exposed to foodstuffs in the oral environment using simulated food liquids as defined by the Food and Drug Administration. Methods: In this study, a total of four esthetic restorative materials were used: one universal compomer (Dyract XP, Dentsply), one conventional microhybrid composite (FiltekTM Z250, 3M ESPE), one nanofilled, and one high-viscosity glass ionomer cement (ChemFil Rock, Dentsply). A total of 160 samples, each 8 mm in diameter and 2 mm in thickness, were prepared using molds. The initial weights of the samples were recorded in micrograms using a precision balance to determine solubility values. Initial surface roughness values were measured using an atomic force microscope device. The samples were immersed in four different simulated food liquids (ethanol, heptane, citric acid, and distilled water) for a period of 7 days. After removal from the solutions, the samples were desiccated to a constant weight, and the second set of weights was recorded. Subsequently, the second surface roughness values were measured Results: Among the materials immersed in the simulated food solutions, ChemFil Rock exhibited the highest solubility and increase in surface roughness. Citric acid was found to be the solution that caused the highest increase in surface roughness values and solubility for this material (p

(Kesan Rawatan Permukaan pada Ikatan Struktur Mikro antara Muka Zirkonia-Dentin terhadap Saiz Zarah Serbuk Zirkonia yang Berbeza)

Zirconia-based materials have emerged as promising resources for dental restoration applications owing to their excellent strength and aesthetic appearance. In clinical practices, surface treatment on zirconia is essential to ensure enhanced dental bonding. In this study, a novel method was used to produce zirconia block, and the influence of surface treatment on zirconia-dentine microstructure bonding interface was investigated for different particle sizes of zirconia powder. The particle sizes used in this study were 90 and 30 nm on the basis of manufacturer claims. A zirconia block of both particle sizes underwent surface treatment airborne-particle abrasion (50 μm, 0.4 MPa). Dentine specimens were prepared from extracted premolars stored in 0.1% tymol solution before being randomly cemented with the zirconia block sample by using self-adhesive resin cement (RelyX U2000 Clicker, 3M) and then light polymerised. The results after surface treatment showed higher surface roughness values for 90 and 30 nm at 0.17 and 0.18 μm, respectively, than those of the sample without surface treatment at 0.05 and 0.06 μm, respectively, showing no significant difference between particle sizes. Surface treatment improved the bonding of zirconia because the surface roughness allowed for enhanced interlocking of the cement onto the zirconia surface. However, the unbonded dentine and cement was due to the existence of a smear layer on the dentine surface that prevented the selfadhesive resin cement to work well with the dentine surface. Thus, dentine primer must be used to chemically remove the layer and allow for proper bonding between the resin cement and dentine surface.

An Investigation of the Effect of Novel Mono/Bi-Layered PVD-Coated WC Tools on the Machinability of Ti-5Al-5V-5Mo-3Cr.

The Ti-5Al-5V-5Mo-3Cr (Ti-5553) alloy is a relatively novel difficult-to-cut material with limited machinability and tool life analysis available in the literature, and hence requires further investigation. This study focuses on the machining and tribological performance of Ti-5553 under high-speed finish turning (150 m/min, 175 m/min, and 200 m/min) via novel mono/bi-layered PVD-coated WC tools. A base AlTiN coating is used as the reference monolayer coating, with AlCrN, diamond-like ta-C, and TiAlSiN coatings each deposited on top of a base AlTiN coating, totaling four separate coated tools (one monolayer and three bi-layer). Tool life, cutting forces, workpiece surface quality, and tribological chip analysis are among the subjects of investigation in this study. Overall, the AlTiN/AlCrN coated tool outperformed all the other combinations: an improvement of ~19% in terms of tool life in reference to the base AlTiN coating when averaging across the three speeds; lowest surface roughness values: ~0.30, 0.33, and 0.64 µm; as well as the lowest chip back surface roughness values: ~0.80, 0.68, and 0.81 µm at 150, 175, and 200 m/min, respectively. These results indicate that the AlTiN/AlCrN coating is an excellent candidate for industrial applications involving high-speed machining of Ti-5553.

Experimental investigation and parametric optimization of rotary ultrasonic machining of different bio-ceramic materials

Rotary ultrasonic machining (RUM) is a highly promising technique for machining bio-ceramic materials due to its ability to achieve high precision and superior surface quality. This research focuses on an experimental investigation and parametric optimization of RUM for different bio-ceramic materials, intending to optimize multiple machining responses simultaneously. The experimental setup involves utilizing a 3-axis CNC ultrasonic machine to machine three different workpieces with slot cutting. Various machining parameters, such as tool feed rate and tool rotating speed, are studied to determine their impacts. An orthogonal array design based on Taguchi optimization is used to execute the experiments effectively. Material removal rate (MRR) and surface roughness (SR) are monitored and statistically analyzed as a consequence of the responses. ANOVA demonstrates that the tool feed rate has a considerable impact on the output reactions, with material type and tool rotational speed also playing a role. For multiple response optimizations, the Taguchi-Grey method is used to achieve the best trade-off between MRR and Sr The results demonstrate that material type has the most substantial impact on surface roughness, followed by feed rate and spindle speed. In contrast, feed rate has the most significant effect on the material removal rate, followed by the material type and spindle speed. The optimal parameter settings for achieving the desired output parameter are determined. The confirmation experiments validate the effectiveness of the optimized parameters. The feed rate of 5 mm min−1, and spindle speed of 2500 rpm were discovered to be the optimal condition for achieving maximum MRR and minimum Ra. The MRR and surface roughness values were measured as 1.7266 mm3 min−1 and 1.5611 microns respectively.

An In Vitro Analysis of the Effects of Mouthwashes on the Surface Properties of Composite Resin Restorative Material.

Restorative composite resins have clinical prime importance in modern dental practice, but numerous factors influence their prognosis in the oral environment. Their interaction with oral care products, like mouthwashes, is one such factor. This study aimed to evaluate the quantifiable effects of different mouthwashes on the surface properties of the composite resin restorative material. The method involved formulating 90 samples of nanohybrid composite resins (Medicept Dental India Private Limited, Mumbai, India). The samples were treated with 1% alcohol, without alcohol, and with a saline solution (control). Surface roughness (Ra values) and microhardness had been checked before and after an exposure period of 24 hours. Data were thus tabulated, and from that, average values of surface roughness and microhardness were derived. This data was analyzed using the IBM SPSS Statistics for Windows, V. 26.0 (IBM Corp., Armonk, NY). Analysis of variance (ANOVA) and a t-test were used to compare the means of the variables. The level of significance was fixed at p < 0.05. The surface roughness value was significantly highest in the ethanol-containing mouthwash-treated samples after 24 hours of exposure (p < 0.05). The microhardness was statistically lower in these samples (p < 0.05). These research data give quantitative information, however, about the mass effect of mouthwashes on the composite resin restorative material. The presented changes, which were illustrated by the values of surface roughness and microhardness, are drawing attention to the fact that a cautious approach must be taken in the recommendations for oral care in the provision of intensive treatments with restorative composite resins.

Comparative Analysis of Microabrasive Film Finishing Effects across Various Process Variants.

The paper investigates various methods of microfinishing and arrives at the best technique to produce a very smooth surface. Various setups, with and without oscillation, were developed, together with a microfinishing attachment used on conventional lathes and milling machines. The workpiece material used was an amorphous nickel-phosphorus Ni-P alloy. The surface roughness parameters, such as Sa, Sv, and Sp, were measured with the TalySurf CCI6000 instrument. For the measurement of the surface protrusions, an "analysis of islands" technique was used at various levels of cut-off. The 2BA method-machining below the workpiece axis with oscillation-turned out to be the most effective method applied because it had the highest density of protrusions while having the smallest value of surface roughness. Non-oscillation with the machining zone below the axis also becomes effective, indicating that repositioning can compensate for a lack of oscillation. Already, the very compact surface structure achieved with minimized depths in the valleys by the 2BA method supported the improvement in tribological performance and increase in load-carrying capacity, together with lubricant retention enhancement. These results show that the microfinishing process can be optimized by parameter tuning, and also, non-oscillating methods could come to be a practical alternative, probably reducing the complexity of equipment and cutting costs. Further studies need to be aimed at the scalability of these methods and their application to other materials and fields.

Parametric Analysis and Optimization on Fiber Laser Micro-Milling on AZ31 Magnesium Alloy

One of the proficient machining technologies to create micro-features in a variety of materials is the laser micro-milling process. This procedure involves irradiating a highly concentrated laser beam on the sample and performing laser cutting at various cutting patterns to change the surface conditions and enhance the characteristics of that surface tribology. In this work, an effort has been made to mill magnesium alloy (AZ31) material using a laser. The pulse frequency, laser beam power, cutting speed, number of passes, and transverse feed are among the different process variables taken into account for the current research effort. Measured results include depth of cut and surface roughness. To ensure the validity of the established empirical models, this paper also presents experimental data. Several surface plots have been used to examine the test data. To get the lowest values of surface roughness and depth of cut, multiperformance optimization is also utilized. The influence of process factors on response has also been examined using optical microscopic images. Gray relational analysis approach is also applied to obtain the multiobjective optimization parametric combination and based on the calculated results of gray relational grade, it is revealed that improvement in the value of gray relational grade at predictive setting is 0.054 compared to the initial parametric combination.

Extreme roughness reduction and ultrafine quality of innovative dual function material extrusion 3D printer

PurposeThis paper aims to use hybrid manufacturing (HM) to overcome several drawbacks of material extrusion three-dimensional (3D) printers, such as low dimension ranging from 0.2 to 0.5 µm, resulting in a noticeable staircase effect and elevated surface roughness.Design/methodology/approachSubtractive manufacturing (SM) through computer numerical control milling is renowned for its precision and superior surface finish. This study integrates additive manufacturing (AM) and SM into a single material extrusion 3D printer platform, creating a HM system. Two sets of specimens, one exclusively printed and the other subjected to both printing and milling, were assessed for dimension accuracy and surface roughness.FindingsThe outcomes were promising, with postmilling accuracy reaching 99.94%. Significant reductions in surface roughness were observed at 90° (93.4% decrease from 15.598 to 1.030 µm), 45° (89% decrease from 26.727 to 2.946 µm) and the face plane (71% decrease from 12.176 to 3.535 µm).Practical implicationsThe 3D printer was custom-built based on material extrusion and modified with an additional milling tool on the same gantry. An economic evaluation based on cost-manufacturing demonstrated that constructing this dual-function 3D printer costs less than US$560 in materials, offering valuable insights for researchers looking to replicate a similar machine.Originality/valueThe modified general 3D printer platform offered an easy way to postprocessing without removing the workpiece from the bed. This mechanism can reduce the downtime of changing the machine. The proven increased dimension accuracy and reduced surface roughness value increase the value of 3D-printed specimens.

The effect of detox solution on color stability, roughness, and microhardness of monochromatic universal composite resins

BackgroundCurrently, the advantages of monochromatic universal composite resin restorative materials have increased their use in dentistry. Accordingly, the optical, surface and mechanical properties of these materials have become more important. This study aimed to evaluate the effect of detox solution on discoloration, surface roughness (SR), and microhardness of different monochromatic universal composite resins (Omnichroma [O], Zenchroma [Z], Vittra [V], and Charisma Diamond One [CDO]). Another aim of this study was to evaluate the monomer conversion degree (DC) of the materials.MethodsA total of 80 specimens were prepared to evaluate the materials (n = 10). After the initial measurements, the specimens were immersed in a red detox solution for 21 days. Statistical data analysis was performed using one-way ANOVA and Tukey’s multiple comparisons.ResultsThe ∆E values of Z were highest on the 21st day. There was an increase in the SR values of the materials immersed in the detox solution. On the 21st day, top surface microhardness of O was lower than the other materials. There was no statistically significant difference at DC values among material groups.ConclusionsThe use of detox solutions for a commercially recommended period of 21 days is suggested. However, this usage period can cause discoloration in restorative materials. Furthermore, especially in the initial one-week period, detox solution may have a negative impact on the microhardness of the materials. In light of all these data, we recommend the cautious use of detox solutions to prevent adverse effects on restorative materials.

Subnanoscale Ion Beam Modification-Assisted Smoothing of Heterostructure Surfaces.

Glass ceramic (GC) is the most promising material for objective lenses for extreme ultraviolet lithography that must meet the subnanometer precision, which is characterized by low values of high spatial frequency surface roughness (HSFR). However, the HSFR of GC is typically degraded during ion beam figuring (IBF). Herein, a developed method for constructing molecular dynamics (MD) models of GC was presented, and the formation mechanisms of surface morphologies were investigated. The results indicated that the generation of the dot-like microstructure was the result of the difference in the erosion rate caused by the difference in the intrinsic properties between ceramic phases (CPs) and glass phases (GPs). Further, the difference in the microstructure of the IBF surface under different beam angles was mainly caused by the difference in the two types of sputtering. Quantum mechanical calculations showed that the presence of interstitial atoms would result in electron rearrangement and that the electron localization can lead to a reduction in CP stability. To obtain a homogeneous surface, the effects of beam parameters on the heterogeneous surface were systematically investigated based on the proposed MD model. Then, a novel ion beam modification (IBM) method was proposed and demonstrated by TEM and GIXRD. The range of ion beam smoothing parameters that could effectively converge the HSFR of the modified surface was determined through numerous experiments. Using the optimized beam parameters, an ultrathin homogeneous modified surface within 3 nm was obtained. The HSFR of GC smoothed by ion beam modification-assisted smoothing (IBMS) dropped from 0.348 to 0.090 nm, a 74% reduction. These research results offer a deeper understanding of the morphology formation mechanisms of the GC surfaces involved in ion beam processing and may point to a new approach for achieving ultrasmooth heterostructure surfaces down to the subnanometer scale.

Morphological Characterization of Sb-Doped SnO2 Thin Films Developed by Spray Pyrolysis

In the present work, we have successfully deposited Sb antimony doped tin dioxide (SnO2) thin films with different concentrations (0 at%, 1 at%, 3 at% and 5 at%) from a stannous (II) chloride dihydrate solution (SnCl2.2H2O), by the pyrolysis chemical spray deposition technique on ordinary microscope glass substrates preheated to a fixed temperature of 350 °C. After deposition, the films were annealed at temperatures 400 °C for 4h. The aim of this work is on the one hand to study the morphological properties of pure and doped tin dioxide thin films and to determine the different morphological parameters such as: the roughness Ra, Rq and on the other hand to study the effect of Sb doping on the morphological properties of SnO2 thin films. To achieve this purpose, the thickness of all the films was estimated by profilometer with standard scan type. The morphology of the films was examined by atomic force microscope (AFM) in contact mode at room temperature to visualize the surface of our samples (the structure, size and morphology of crystallites ... etc). The 2D and 3D AFM images confirm the formation of nanostructures on the surface, with shapes and dimensions influenced by the amount of antimony doping. All the samples show a polycrystalline morphology, and the grain size progressively decreases with the increase of the Sb concentration (1% and 3%). On the other hand, for high antimony doping (5% Sb) the grains are larger than those observed at 3% doping. The root mean square (RMS) surface roughness values for samples with Sb concentrations (5%) were found to be 8.334 nm.

Powder Bed Fusion-Laser Beam of IN939: The Effect of Process Parameters on the Relative Density, Defect Formation, Surface Roughness and Microstructure.

This study investigates the effects of process parameters in the powder bed fusion-laser beam (PBF-LB) process on IN939 samples. The parameters examined include laser power (160, 180, and 200 W), laser scanning speed (400, 800, and 1200 mm/s), and hatch distance (50, 80, and 110 μm). The study focuses on how these parameters affect surface roughness, relative density, defect formation, and the microstructure of the samples. Surface roughness analysis revealed that the average surface roughness (Sa) values of the sample ranged from 4.6 μm to 9.5 μm, while the average height difference (Sz) varied from 78.7 μm to 176.7 μm. Furthermore, increasing the hatch distance from 50 μm to 110 μm while maintaining constant laser power and scanning speed led to a decrease in surface roughness. Relative density analysis indicated that the highest relative density was 99.35%, and the lowest was 93.56%. Additionally, the average porosity values were calculated, with the lowest being 0.06% and the highest reaching 9.18%. Although some samples had identical average porosity values, they differed in porosity/mm2 and average Feret size. Variations in relative density and average porosity were noted in samples with the same volumetric energy density (VED) due to different process parameters. High VED led to large, irregular pores in several samples. Microcracks, less than 50 μm in length, were present, indicating solidification cracks. The microstructural analysis of the XZ planes revealed arc-shaped melt pools, columnar elongated grains aligned with the build direction, and cellular structures with columnar dendrites. This study provides insights for optimizing PBF-LB process parameters to enhance the quality of IN939 components.