Ultimate Tests Research Articles

Novel approach for in-line process monitoring during ultrasonic metal welding of dissimilar wire/terminal joints based on the thermoelectric effect

AbstractUltrasonic metal welding (USMW) is a manufacturing technique widely employed in the automotive and aerospace industries due to its efficiency in joining similar as well as dissimilar metals. Despite its prevalence, the lack of effective in-line process monitoring methods has resulted in high scrap rates, product recalls due to unrecognized scrap or financial losses due to pseudo-scrap, limiting its application in more sensitive industries. This paper presents a novel thermoelectric effect-based method for in-line process monitoring of USMW processes. This approach utilizes the thermoelectric properties, that manifest at the junctions of dissimilar metals during welding to accurately measure the temperature of the weld zone without the need of additional thermocouples, pyrometers or infrared cameras. An experimental setup was developed to validate the thermoelectric-based temperature measurement methodology. Key to this approach is the detection of thermoelectric voltage developed due to thermo diffusion when dissimilar materials are joined. The experiments showed a strong correlation between the thermoelectric voltage and the mechanical strength of the welds, suggesting that this parameter can effectively predict the quality of the weld. In the trials, a series of welded samples was created under controlled conditions to measure the generated thermoelectric voltage and correlate it with ultimate tensile strength tests. The data were analyzed using Spearman’s correlation coefficients to determine the correlation of the thermoelectric signals and joint strength. Results indicate that the thermoelectric voltage measurements correlate highly with the joint strength, with a Spearman’s correlation coefficient of over 0.94, thereby providing a promising predictive metric for assessing weld quality.

Bicuspid Valve Aortopathy: Is It Reasonable to Define a Different Surgical Cutoff Based on Different Aortic Wall Mechanical Properties Compared to Those of the Tricuspid Valve?

In this study, we examined and compared ex vivo mechanical properties of aortic walls in patients with bicuspid (BAV) and tricuspid (TAV) aortic valve aortopathy to investigate if the anatomical peculiarities in the BAV group are related to an increased frailty of the aortic wall and, therefore, if a different surgical cutoff point for ascending aortic replacement could be reasonable in such patients. Ultimate stress tests were performed on fresh aortic wall specimens harvested during elective aortic surgery in BAV (n. 33) and TAV (n. 77) patients. Three mechanical parameters were evaluated at the failure point, under both longitudinal and circumferential forces: the peak strain (Pstr), peak stress (PS), and maximum elastic modulus (EM). The relationships between the three mechanical parameters and preoperative characteristics were evaluated, with a special focus on evaluating potential risk factors for severely impaired mechanical properties, cumulatively and comparatively (BAV vs. TAV groups). The patient populations were inhomogeneous, as BAV patients reached surgical indication, according to the maximum aortic dilatation, at a younger age (58 ± 15 vs. 64 ± 13; p = 0.0294). The extent of the maximum aortic dilatation was, conversely, similar in the two groups (52 ± 4 vs. 54 ± 7; p = 0.2331), as well as the incidences of different phenotypes of aortic dilatation (with the ascending aorta phenotype being the most frequent in 81% and 66% of the BAV and TAV patients, respectively (p = 0.1134). Cumulatively, the mechanical properties of the aortic wall were influenced mainly by the orientation of the force applied, as both PS and EM were impaired under longitudinal stress. An age of >66 and a maximum dilatation of >52 mm were shown to predict severe Pstr reduction in the overall population. Comparative analysis revealed a trend of increased mechanical properties in the BAV group, regardless of the position, the force orientation, and the phenotype of the aortic dilatation. BAV aortopathy is not correlated with impaired mechanical properties of the aortic wall as such. Different surgical cutoff points for BAV aortopathy, therefore, seem to be unjustified. An age of >66 and a maximum aortic dilatation of >52 mm, however, seem to significantly influence the mechanical properties of the aortic wall in both groups. These findings, therefore, could suggest the need for more accurate monitoring and evaluation in such conditions.

Development of Multi-Walled Carbon Nanotube-Integrated Recycled Polyethylene Terephthalate Electrospun Antibacterial Face Mask

In this study, electrospun nanofiber membranes were successfully fabricated by modifying recycled polyethylene terephthalate (r-PET) with multi-walled carbon nanotubes (MWCNTs) for face mask applications. The recycling of PET bottles ensures effective waste management, while the electrospinning process facilitates the creation of delicate nano-range fibers. The inclusion of MWCNTs aimed to assess the antibacterial activity of the resulting nanomembranes. The fabricated samples underwent comprehensive characterization, including scanning electron microscopy (SEM), ultimate tensile testing, particulate filtration efficiency (PFE) testing, Fourier transform infrared spectroscopy (FTIR), and antibacterial sensitivity assays, revealing significant findings. MWCNTs incorporation led to minor bead formation in the membranes, with fiber diameters ranging from 446 to 862 nm. However, MWCNTs resulted in reduced stiffness and tensile properties due to the disruption of polymer chain alignment. The nanofiber membranes demonstrated effective filtration of 0.3 µm particulates, achieving filtration rates between 96 to 97%Functional group analysis confirmed the presence of both r-PET and MWCNTs in the composites. Although the r-PET/MWCNTs 12 kV membrane lacked an antibacterial zone of inhibition, it exhibited reductions of 28.64% for S. aureus and 31.9% for E. coli. These results collectively underscore the potential of r-PET/MWCNTs samples as an alternative nanofibrous membrane material for face masks. J. of Sci. and Tech. Res. 5(1): 63-74, 2023

Powder Bed Fusion Techniques in Metal 3D Printing: A Review

The use of 3D printing (additive manufacturing) with metal has grown significantly in demand recently, greatly reducing the time and expense required to produce complex interconnected metal components. This method minimizes material wastage, facilitates material recycling, and eliminates the need for support materials. Among the various Metal Additive Manufacturing techniques, Powder Bed Fusion (PBF) processes stands out as the most prevalent for manufacturing parts. Within the realm of PBF, electron beam melting technique, selective laser sintering technique, and selective laser melting technique are the primary methods employed. Selective laser melting and selective laser sintering operate without the need for any special conditions, unlike EBM, which necessitates a vacuum environment. Regarding the choice of materials, laser melting/sintering processes are suitable for almost all types of metals except those which surpasses beam melting capabilities. While electron beam melting is constrained to a few materials such as titanium alloys, cobalt and chromium alloys, and nickel alloys, whereas selective laser melting and sintering allows for a broad range of materials, including iron and steel alloys. However, electron beam melting exhibit the ability to process brittle materials that would typically be challenging for melting and sintering through laser. Nevertheless, the ductility, yield testing, and ultimate testing of materials created through EBM are inferior to those processed by laser methods. Although all PBF techniques excel at creating complex structures, finishing products to have a smooth surface directly over a rough surface remains a subject of ongoing research. To attain suitable mechanical properties such as hardness, tensile strength, and endurance, critical process factors include power of laser or beam, speed for scanning, density for powder bed, thickness of laser or beam, and material characteristics. Inadequate material selection coupled with incorrect process settings can lead to issues such as porosity, slag formation, and other flaws.

Characterization of the spin arc welding technique for dissimilar materials Hastelloy C-2000 and C-276

Hastelloy C-2000 and C-276 are primarily employed in the petrochemical and pharmaceutical industries. Finding an effective way to combine these alloys is still a complex task in industry. The main focus of this study is to investigate the potential efficacy of the spin arc welding process on Hastelloy C-2000 and C-276. The welding process was carried out under various conditions, such as weld current, spinning speed, and spin diameter. ERNiCrMo-4, with a diameter of 1.2 mm, was employed as a filler. Optical microscopy, XRD and FESEM were used for microstructural examination. The mechanical properties of the welded samples were critically analyzed. The results of the ultimate tensile strength (UTS), hardness value (HV), and impact tests of spin arc welding were compared with those of the multipass pulsed current gas tungsten arc welding process (MPCGTAW). In spin arc welding, Hastelloy C-2000 and C-276 exhibited higher UTS, HV, and toughness compared to MPCGTAW because there was no secondary TCP phase formation in the weld centre and hot cracking in spin arc weldments. Additionally, compared to MPCGTAW, the elongation with spin arc welding was noted to be lower. Moreover, microstructural analysis revealed no evidence of grain segregation, which may have contributed to the improved UTS and HV of the materials during spin arc welding. Thus, spin arc welding proves to be superior for dissimilar Hastelloy joints of C-2000 and C-276.

Analytical Solution for the Ultimate Compression Capacity of Unbonded Steel-Mesh-Reinforced Rubber Bearings

Unbonded steel-mesh-reinforced rubber bearings (USRBs) have been proposed as an alternative isolation bearing for small-to-medium-span highway bridges. It replaces the steel plate reinforcement of common unbonded laminated rubber bearings (ULNR) with special steel wire meshes, resulting in improved lateral properties and seismic performance. However, the impact of this novel steel wire mesh reinforcement on the ultimate compression capacity of USRB has not been studied. To this end, theoretical and experimental analysis of the ultimate compression capacity of USRBs were carried out. The closed-form analytical solution of the ultimate compression capacity of USRBs was derived from a simplified USRB model employing elasticity theory. A parametric study was conducted considering the geometric and material properties. Ultimate compression tests were conducted on 19 USRB specimens to further calibrate the analytical solution, considering the influence of the number of reinforcement layers. An efficient solution for USRBs’ ultimate compression capacity was obtained via multilinear regression of the calibrated analytical results. The efficient solution can simplify the estimation of USRBs’ ultimate compression capacity while maintaining the same accuracy as the calibrated solution. Based on the efficient solution, the design process of a USRB with a specific ultimate compression capacity was illustrated.

Exploring key factors affecting the ultimate compression capacity of Unbonded Steel-mesh-reinforced Rubber Bearings

To address bearing-sliding damage in highway bridges during seismic events, the Unbonded Steel-mesh-reinforced Rubber Bearing (USRB) was developed. This novel bearing employs flexible, high-strength steel wire meshes as reinforcement, enhancing lateral deformation capacity and reducing bearing-sliding risk. Recent seismic specifications increased the bearings' vertical design load to 30 MPa, where existing bearings with flexible reinforcements (e.g., fiber-reinforced bearings) fail to meet this standard. Hence, for the first time, our study thoroughly investigated the ultimate compression capacity of USRBs and the key factors influencing the capacity. Through ultimate compression tests on full-scale prototypes, we demonstrated that USRBs can comply with heightened seismic requirements, with primary failure attributed to the tensile failure of the steel mesh reinforcement. These tests were complemented by 3D finite element modeling in ANSYS, employing the LINK180 elements for mesh reinforcement and defining the ultimate capacity as the point at which reinforcement stress reached tensile strength. This particular modeling approach, validated against experimental data, can accurately predict the ultimate compression capacity and the force-deformation response of USRBs. A comprehensive parametric analysis, using the validated modeling approach and an advanced statistical method LHS-PRCC, was conducted to identify the key factors influencing the compressive capacity, including bearing geometric parameters (i.e., bearing width, the second shape factor, and rubber layer thickness), steel-mesh configuration characteristics, and steel-mesh material properties. Our findings emphasize the significance of rubber layer thickness, steel mesh weight, and steel wire tensile strength and strain in influencing the USRBs' ultimate compression capacity. Based on these key factors, an empirical equation for the ultimate compression capacity of USRBs was established to guide the optimization design of USRBs. This study not only fills the gap in USRB's performance under extensive compression but also provides a foundation for future optimization of these bearings to enhance their performance in bridge engineering.

Chronic lateral ankle instability using anterior tibiofibular ligament distal fascicle transfer augmentation repair: an anatomical, biomechanical, and histological study.

Background: The transfer of the anterior tibiofibular ligament distal fascicle (ATiFL-DF) for the augmentation repair of the anterior talofibular ligament (ATFL) shows potential as a surgical technique. However, evidences on the benefits and disadvantages of this method in relation to ankle joint function are lacking. Purpose: This study aimed to provide comprehensive experimental data to validate the feasibility of ATiFL-DF transfer augmentation repair of the ATFL. Methods: This study included 50 embalmed ankle specimens to measure various morphological features, such as length, width, thickness, and angle, for evaluating similarities between the ATiFL-DF and ATFL. Furthermore, 24 fresh-frozen ankle specimens were examined for biomechanical testing of the ATiFL-DF transfer augmented repair of the ATFL. Finally, 12 pairs of ATiFL-DF and ATFL tissues from fresh-frozen ankle specimens were treated with gold chloride staining to analyze mechanoreceptor densities. Results: Anatomical studies found that the lengths and thicknesses of the ATFL and ATiFL-DF are similar. Biomechanical outcomes showed that performing ATiFL-DF transfer for ATFL repair can improve the stability of the talus and ankle joints. This is evident from the results of the anterior drawer, axial load, and ultimate failure load tests. However, performing ATiFL-DF transfer may compromise the stability of the distal tibiofibular joint, based on the Cotton and axial load tests at an external rotation of 5°. Analysis of the histological findings revealed that mechanoreceptor densities for four types of mechanoreceptors were comparable between the ATiFL-DF and ATFL groups. Conclusion: ATiFL-DF transfer is a viable method for augmenting ATFL repair. This technique helps to improve the stability of the talus and ankle joints while compensating for proprioception loss. Although ATiFL-DF transfer augmented repair of the ATFL may negatively affect the stability of the distal tibiofibular joint, this procedure can enhance the stability of the talus and ankle joints.

Experimental Study of Reinforced Concrete T-Beam Retrofitted with Ultra-High-Performance Concrete under Cyclic and Ultimate Flexural Loading.

Structurally deficient bridges are commonly retrofitted using conventional methodologies, including reinforced concrete, steel jackets, and fiber-reinforced polymers. Although these retrofit methods aim to improve structural performance, exposure to aggressive environments may undermine the durability performance of the retrofit material. More recently, ultra-high-performance concrete (UHPC) has provided an alternative to conventional construction methods, with its superior material characteristics favoring its use in retrofit applications. In this study, a large-scale reinforced concrete (RC) T-beam is constructed and artificially damaged. The T-beam is then retrofitted with an external envelope of UHPC on all faces. Sandblasting is introduced to the surface, providing partially exposed reinforcement in the T-beam to simulate material deterioration. Additional reinforcement is placed in the web and flange, followed by casting the enveloping layer of UHPC around the specimen. The feasibility of this method is discussed, and the structural performance of the beam is assessed by subjecting the beam to cyclic and ultimate flexural loading. This paper presents the results of cyclic and ultimate testing on the RC-UHPC composite T-beam regarding load-displacement, failure mode, and strain responses. The retrofitted T-beam specimen is subjected to a cyclic loading range of 131 kN for 1.576 million cycles. Despite no visible cracks in the cyclic testing, the specimen experiences a 12.22% degradation in stiffness. During the ultimate flexural testing, the specimen shows no relative slip between the two concretes, and the typical flexural failure mode is observed. By increasing the longitudinal reinforcement ratio in the web, the failure mode can shift from localized cracking, predominantly observed in the UHPC shell, toward a more distributed cracking pattern along the length of the beam, which is similar to conventional reinforced concrete beams.

Biomechanical comparison of suture bridge rotator cuff repair with and without dermal allograft pledgets

BackgroundOne method to augment rotator cuff repair is to pass dermal allograft pledgets along the sutures that bridge from the medial to the lateral row. It remains unclear whether this augmentation method alters repair biomechanics. MethodsThis was a controlled laboratory study. After an a priori power analysis, nine pairs of rotator cuffs underwent double row suture bridge rotator cuff repair, half randomized to augmentation with dermal allograft pledgets passed along the suture bridge sutures. Repairs were then mounted on a material testing system and loaded cyclically 500 cycles to mesure applied force and displacement. Repairs then underwent ultimate failure testing and stiffness, ultimate failure force, and ultimate failure displacement were measured. Paired t-tests were performed to compare between groups. ResultsThere were no differences between groups in construct gapping with cyclic loading after 500 cycles (p = 0.885). There no differences between the augmented and control groups in yield force (103.5 ± 5.0 vs. 101.4 ± 5.9 N, respectively, p=0.183), stiffness (94.2 ± 13.9 vs. 90.9 ± 13.8, p=0.585), or ultimate failure force (255.3 ± 65.8 vs. 285.3 ± 83.2, p=0.315). There were no differences between groups in failure modes, with most specimens failing by cuff tissue tearing within or medial to the construct. ConclusionThe addition of dermal allograft pledgets does not positively or negatively influence the time-zero biomechanical characteristics of double-row suture bridge rotator cuff repair.

Differential Studies of Argon Particle and Antiparticle Interactions: Present Status and Future Possibilities

Although the comparison of fully differential ionization data for particle and antiparticle impact provides the ultimate tests of theoretical models, only very low antiparticle beam intensities are available. Hence, few experiments of this type have been performed. Therefore, available experimentally obtained single and double differential cross-sections, which are much easier to obtain, are compared in order to demonstrate differences when only the projectile mass or charge (+1 or −1) is changed. Included in the comparison are cross-sections calculated for positron and electron impact using a three-particle classical trajectory Monte Carlo method. The calculated cross-sections provide independent information about the ejected electron and the scattered projectile contributions, plus information about the impact parameters, all as functions of the collision kinematics. From these comparisons, suggestions as to where future investigations are both feasible and useful are provided.

Shear wave elastography demonstrates different material properties between the medial collateral ligament and anterolateral ligament

BackgroundAnterolateral ligament and medial collateral ligament injuries could happen concomitantly with anterior cruciate ligament ruptures. The anterolateral ligament is injured more often than the medial collateral ligament during concomitant anterior cruciate ligament ruptures although it offers less restraint to knee movement. Comparing the material properties of the medial collateral ligament and anterolateral ligament helps improve our understanding of their structure-function relationship and injury risk before the onset of injury. MethodsEight cadaveric lower extremity specimens were prepared and mechanically tested to failure in a laboratory setting using a hydraulic platform. Measurements of surface strains of superficial surface of each medial collateral ligament and anterolateral ligament specimen were found using three-dimensional digital image correlation. Ligament stiffness was found using ultrasound shear-wave elastography. t-tests were used to assess for significant differences in strain, stress, Young's modulus, and stiffness in the two ligaments. FindingsThe medial collateral ligament exhibited greater ultimate failure strain along its longitudinal axis (p = 0.03) and Young's modulus (p < 0.0018) than the anterolateral ligament. Conversely, the anterolateral ligament exhibited greater ultimate failure stress than the medial collateral ligament (p < 0.0001). Medial collateral ligament failure occurred mostly in the proximal aspect of the ligament, while most anterolateral ligament failure occurred in the distal or midsubstance aspect (P = 0.04). InterpretationDespite both being ligamentous structures, the medial collateral ligament and anterolateral ligament exhibited separate material properties during ultimate failure testing. The weaker material properties of the anterolateral ligament likely contribute to higher rates of concomitant injury with anterior cruciate ligament ruptures.

Biomechanical analysis of bridge combined fixation system as a novel treatment for the fixation of type A3 distal femoral fractures.

To compare the biomechanical parameters of AO/OTA type A3 distal femoral fractures fixed bilaterally with a bridge combined fixation system (BCFS) and lateral locking compression plate + locking reconstruction plate (LCP + LRP). Twelve A3 distal femoral fracture models with medial cortical defects of the distal femur were created using synthetic femoral Sawbones. BCFS and LCP + LRP were used for bilateral fixation, with six in each group. Axial compression and torsion tests were performed on the two groups of fracture models to determine their stiffness during axial compression and the Torsional stiffness during torsion tests. Axial compression failure tests were performed to collect the vertical loads of the ultimate failure tests. In the test conducted on the fixed type A3 distal femoral fracture models, the axial stiffness in the BCFS group (group A) (1,072.61 ± 113.5 N/mm) was not significantly different from that in the LCP + LRP group (group B) (1,184.13 ± 110.24 N/mm) (t = 1.726, P = 0.115), the Torsional stiffness in group A (3.73 ± 0.12 N.m/deg) was higher than that in group B (3.37 ± 0.04 N.m/deg) (t = 6.825, P < 0.001),and the ultimate failure test of type A3 fracture model showed that the vertical load to destroy group A fixation (5,290.45 ± 109.63 N) was higher than that for group B (3,978.43 ± 17.1 N) (t = 23.28, P < 0.05). Notably, intertrochanteric fractures occurred in groups A and B. In the fixation of type A3 distal femoral fractures, the anti-axial compression of the BCFS group was similar to that of the LCP + LRP group, but the anti-torsion was better.

In-Situ Test and Numerical Simulation of Anchoring Performance of Embedded Rock GFRP Anchor

Compared to traditional steel reinforcement, GFRP anchors demonstrate outstanding mechanical performance and corrosion resistance, and so they are an ideal substitute for steel reinforcement in anti-floating projects. Based on finite element software, a 3D axisymmetric calculation model of GFRP anti-floating anchors in medium-weathered granite was established in this paper. Combined with the in-situ ultimate pull-out tests, the bonding anchoring performance and bearing characteristics between the anchor body, anchoring mortar, and rock–soil mass were analyzed. The research findings indicated that the cohesive bonding elements exhibited a high degree of conformity in defining the interface contact relationship of the GFRP anti-floating anchor anchoring system. The axial force of the GFRP anti-floating anchor body is “attenuated” along the depth direction, and there was a critical value of anchoring length; under the same conditions, the reasonable anchoring length should be 3.5~5.0 m. All the anchors in the in-situ tests exhibited interfacial shear slip failure between the anchor body and the anchor mortar, with an average maximum load of 450 kN, which is consistent with the maximum failure load of the simulated anchors. Compared to a load of 50 kN, the maximum stress of the anchor mortar increased by 50% under a load of 450 kN. The displacement variation of the surrounding rock–soil mass showed a decreasing trend from the inside to the outside and from the top to the bottom. The research results provided valuable references for the optimization design of GFRP anti-floating anchors.

Achieving high-quality silver sintered joint for highly-reliable schottky barrier diodes via pressureless method

The fabrication of silver joints was done using the pressureless sintering technology to suit the demand of high-reliability schottky barrier diodes (SBD). Porosity of 10.6% and shear strength of 39.6 MPa were reached under the optimized parameters of 290°C sintering temperature and 40 min residence time. The sintered joint demonstrated good mechanical/thermal/electrical performance in the ultimate reliability assessment testing, including the temperature cycling test, second sintering test, steady-state lifetime test, and intermittent lifetime test. This study demonstrated the viability of pressureless sintering of silver joints with good high-temperature reliability, which has significant application potential for aeronautical high-reliability power electronics.

Continuous Vertical Inside-Out Versus Traditional Vertical Inside-Out Meniscal Repair: A Biomechanical Comparison.

Biomechanical assessment of meniscal repairs is essential for evaluating different meniscal suturing methods and techniques. The continuous meniscal suture technique is a newer method of meniscal repair that may have biomechanical differences compared with traditional techniques. To evaluate the displacement, stiffness after cyclical loading, and load to failure for a continuous vertical inside-out meniscal suture versus a traditional vertical inside-out meniscal suture in a porcine medial meniscus. Controlled laboratory study. A total of 28 porcine knees were acquired and divided into 2 test groups of 14 medial meniscus each. A 2.0-cm longitudinal red-white zone cut was made in the body of the medial meniscus for each knee. The continuous suture (CS) group received 4 vertical stitches performed with a continuous vertical meniscal suture technique, and the inside-out suture (IO) group received a traditional vertical suture with 4 stitches. Two traction tapes were passed between the sutures and positioned in the biomechanical testing fixture device. Each specimen underwent load-to-failure testing at 5 mm/s, and displacement, system stiffness, and maximum load to failure were compared between the groups. The displacement after the cyclic test was 0.53 ± 0.12 and 0.48 ± 0.07 mm for the CS and IO groups, respectively. There was no significant difference between the groups (P = .2792). The stiffness at the ultimate load testing was 36.3 ± 1.9 and 35.3 ± 2.4 N/mm for groups CS and IO, respectively, with no significant difference between the groups (P = .2557). In the load-to-failure test, the ultimate load was 218.2 ± 63.9 and 238.3 ± 71.3 N in the CS and IO groups, respectively, with no significant group differences (P = .3062). A continuous vertical meniscal suture created a configuration for treating longitudinal meniscal lesions that was beneficial and biomechanically similar to a traditional vertical suture technique. The study findings indicate that use of the continuous vertical inside-out meniscal suture technique is a possible therapeutic option.

Making of Biodegradable Plastic Based on Corn Starch (Amylum Maydis) with Addition of Acid (CH3 COOh) and Gliserol Plasticizer

Almost all countries face the problem of plastic waste due to the large production of conventional plastics and the long degradation process. Therefore, to protect nature from the accumulation of plastic waste, research on biodegradable plastics needs to be done. Biodegradable plastics are made from starch, cellulose, chitosan, and proteins extracted from renewable biomass. Starch for making biodegradable plastics can be obtained from plants, one of which is corn. This study aims to determine the effect of the composition of acetic acid, glycerol and corn starch on the quality of biodegradable plastics which include tensile strength, elongation and biodegradation. The independent variables were variations of acetic acid and glycerol. Control variables are plastic mold size, corn starch mass of 5 grams, other compounds outside the independent variables. The dependent variable is tensile strength, elongation and biodegradation. To test the tensile strength and elongation of biodegradable plastic, Ultimate Testing Machine Mini was used. The results showed that the addition of acetic acid and glycerol to the corn starch and glycerol blending material had an effect on increasing the tensile strength value and reducing the elongation and biodegradation values of biodegradable plastics. The highest tensile strength value is 50.04 Mpa, obtained from the addition of 1.44% acetic acid and 35.71% glycerol from a volume of distilled water of 70 ml. The highest length gain or elongation of 90% was obtained from the addition of 0.48% acetic acid and glycerol as much as 21.43% of the 70 ml volume of distilled water. Percent weight loss of the largest plastic obtained from the addition of acetic acid as much as 0.48% and glycerol as much as 21.43% of the volume of distilled water as much as 70 ml, which amounted to 93.33%.

Bearing performance and damage characteristics of rein‐infused thermoplastic 3D woven composites bolted joints

AbstractThis paper presents a comprehensive study on the single‐bolt single‐shear (SBSS) and double‐bolt single‐shear (DBSS) lap joint performance of resin‐infused thermoplastic 3D fiber‐reinforced composite (FRC) in on‐axis ( and ) and off‐axis () configurations. The bearing performance and failure mechanisms are compared with thermoset 3D‐FRC. The resin‐infused thermoplastic 3D‐FRC bolted joint shows improved bearing performance in terms of higher ultimate bearing strength, stiffness loss strength, and reduced damage severity than its thermoset counterpart. Additionally, this paper presents a detailed study on the intermediate and final failure mechanisms, obtained from scanning electron microscopy of the interrupted and ultimate bearing tests, to understand damage progression in SBSS and BDSS lap joints at the submicron level. The major damage characteristics of a thermoplastic 3D‐FRC bolted joint include plastic deformation and plastic kinking at the hole front tip, which improve the bearing capacity and reduce stress concentration, damage severity, and its deleterious effects.Highlights Single‐bolt and double‐bolt joint performances of 3D woven composites Failure investigation of different joint configurations and fiber orientations Effect of matrix toughness on the bearing performance of 3D woven composites Progressive damage development and failure modes of 3D woven composite joints.

The cross-linking and protective effect of artemisinin and its derivatives on collagen fibers of demineralized dentin surface

ObjectiveTo investigate the cross-linking and protective effect of artemisinin (ART), dihydroartemisinin (DHA), and artesunate (AST) on collagen fibers of demineralized dentin surface. MethodsMolecular docking was used to predict potential interactions of ART, DHA, and AST with dentin type I collagen. Human third molars without caries were completely demineralized and treated with different solutions for 1 min. The molecular interactions and cross-linking degree of ART and its derivatives with dentin collagen were evaluated by FTIR spectroscopy, total extractable protein content, and a ninhydrin assay. Scanning electron microscopy, hydroxyproline release, and ultimate microtensile strength tests (μUTS) were employed to confirm the mechanical properties and anti-collagenase degradation properties of dentin collagen fibers. ResultsART, DHA, and AST combined with dentin type I collagen mainly through hydrogen bonding and hydrophobic interactions, and the cross-linking reaction sites were mainly C=O and CN functional groups. Compared to the control group, ART and its derivatives significantly increased the degree of cross-linking. Additionally, significant increases were observed in resistance to enzymatic digestion and mechanical properties of the artemisinin and its derivatives group. ConclusionART, DHA, and AST could cross-link with demineralized dentin collagen, through improving the mechanical properties and anti-collagenase degradation properties. Clinical significanceThe study endorses the potential use of ART and its derivatives as a prospective collagen cross-linking agent for degradation-resistant and long-period dentin bonding in composite resin restorations.

Wrist-Level Tendon Repairs Utilizing a Novel Tendon Stapler Device: An Efficiency and Biomechanical Study.

A novel tendon stapler device (TSD) to improve the strength and consistency of primary tendon repairs was recently approved by the U.S. Food and Drug Administration. The authors hypothesized that this TSD would demonstrate faster and superior biomechanical properties compared with a standard suture coaptation. The authors also hypothesized that the TSD biomechanical properties would be consistent across participants with differing tendon repair experiences. Participants included a novice, intermediate, and expert in tendon repairs. Timed comparisons were performed in flexor zones IV and V and extensor zones VI and VII on human cadaver arms. Suture repairs were performed with a modified Kessler technique with a horizontal mattress. TSD repairs were performed on the matched donor arms. Biomechanical testing included 2-mm gap force, ultimate failure load, and mode of failure. In total, 228 tendon coaptations from 12 donor arms were performed and analyzed. TSD coaptations were 3 times faster and withstood nearly 50% higher forces on 2-mm gap testing and roughly 30% higher forces on ultimate failure testing. These findings did not change when the repair times were analyzed by participant. Suture coaptations failed owing to suture pull-through, suture breakage, or knot failure. TSD coaptation failures only occurred from device pull-through. The TSD produces significantly faster and stronger primary tendon coaptations compared with a standard 4-strand core suture repair in human donor arms. The findings demonstrated minimal variability among participants with differing tendon repair experience. Although further investigation is needed, this device has potential to revolutionize tendon repairs.