Triaxial Tests Research Articles

Study on the Yield Surface of a Fibre-Reinforced Stabilised Soil – Effect of the Number of Loading Cycles

Cyclic loading may induce changes in the geomechanical behaviour of materials that should be characterised. This work studies the impact of the number of loading cycles on the mechanical behaviour of a fibre-reinforced stabilised soil focusing on its behaviour before failure (yield surface). To this end, an experimental testing program based on triaxial tests was performed on samples not subjected to a cycling loading stage, as well as on samples previously subjected to a cycling loading stage varying the number of loading cycles from 1,000 to 100,000. The results were studied in terms of the accumulated permanent axial strain and the yield surface of the composite material. It was observed that increasing the number of loading cycles led to a rise in the accumulated permanent axial strain and in the undrained resilient modulus. The results also showed an expansion of the yield surface during the first 1,000 loading cycles (the yield occurs later due to the partial mobilization of the tensile strength of the fibres during the cyclic stage) but its shape is maintained. The results also showed a progressive reduction in the yield loci with the increase in the number of loading cycles, reflecting the greater degradation of the solid matrix induced by the accumulated permanent axial strains.

Enhancing Dynamic Shear Resistance and Efficient Micro-Void Reduction of Expansive Soil Using Activated Nano-Desilicated Fly Ash

Excessive swelling and high compressibility of soil have posed countless challenges such as poor dynamic shear strength for engineers dealing with cyclic loading in pavement structure. To address this challenge, the durability and mechanical properties of the investigated subgrade were treated with 10%, 20%, and 30% of activated nano-disilicate fly ash (NDFA) to the dry mass of the subgrade soil. A series of swelling pressure tests, One-dimensional compression tests, and dynamic triaxial (DT) tests were conducted on the samples fabricated using altered moisture content. The findings demonstrated that the swelling pressure and compressibility of the NDFA-treated specimens significantly decreased to an average of 15.3% and 18.4% respectively upon 20% inclusion of NDFA beyond which the swelling stress and compressibility values further decreased signifying the impact of NDFA on the expansive subgrade. The consolidation results also revealed that the treated soil’s consolidation parameters greatly decreased compared to the untreated soil with a high void ratio and compression index (Cc\\documentclass[12pt]{minimal} \\usepackage{amsmath} \\usepackage{wasysym} \\usepackage{amsfonts} \\usepackage{amssymb} \\usepackage{amsbsy} \\usepackage{mathrsfs} \\usepackage{upgreek} \\setlength{\\oddsidemargin}{-69pt} \\begin{document}$${C}_{c}$$\\end{document}). The dynamic shear resistance of the subgrade soil increased by 36% upon the addition of 10% NDFA content compared to the untreated soil which portrayed a very low resistance against dynamic shear modulus (Gmax\\documentclass[12pt]{minimal} \\usepackage{amsmath} \\usepackage{wasysym} \\usepackage{amsfonts} \\usepackage{amssymb} \\usepackage{amsbsy} \\usepackage{mathrsfs} \\usepackage{upgreek} \\setlength{\\oddsidemargin}{-69pt} \\begin{document}$${G}_{max}$$\\end{document}) with a corresponding high damping ratio. The investigation revealed a strong correlation between Cc\\documentclass[12pt]{minimal} \\usepackage{amsmath} \\usepackage{wasysym} \\usepackage{amsfonts} \\usepackage{amssymb} \\usepackage{amsbsy} \\usepackage{mathrsfs} \\usepackage{upgreek} \\setlength{\\oddsidemargin}{-69pt} \\begin{document}$${C}_{c}$$\\end{document} and dynamic shear modulus which is closely correlated to a coefficient determination of 0.99 due to the parameter’s dependency on porosity, particle shape, and stiffness.

Development of high-performance fiber-reinforced concrete for drilling wellbore walls in highly mineralized strata and its sulfate attack resistanceattack resistance

Metakaolin has been incorporated into high-performance fiber-reinforced concrete for wellbore wall drilling to enhance its durability in strata with highly mineralized water. This study established a benchmark, utilizing fly ash, slag powder, and metakaolin as the factors in an orthogonal test to assess the durability of concrete against sulfate attack. The range analysis and an integrated balance method were employed to optimize the mix proportion, the optimized mix proportion of high-performance concrete was determined as concrete: cement: fly ash: slag powder: metakaolin: pumping agents: gravel: sand: water: polyvinyl alcohol = 1: 0.2: 0.075: 0.05: 0.106: 2.767: 1.556: 0.371: 0.003. The apparent and microscopic morphologies before and after the erosion of both the benchmark group and optimized mix proportion group were investigated. The triaxial permeability tests were conducted on these groups under varying confining pressures to elucidate concrete permeability trends. Additionally, a damage constitutive model for concrete under a sulfate attack was formulated based on the durability tests. This study could provide valuable insights into the industrial utilization of concrete in deep shafts within highly mineralized water strata in Northwestern China.

Resilient and rutting response of unbound granular material and subgrade soil influenced by initial state and stress conditions

Unbound pavements with thin seals, where traffic loads are primarily supported by unbound granular layers and subgrade soil, are favoured for their low initial cost. Rutting, the primary distress mechanism, leads to rough, uncomfortable surfaces, diminishing serviceability and safety. It depends on the material's initial dry density, degree of saturation, and applied stress levels. Resilient modulus, indicating layer stiffness, is crucial for determining load transmission to underlying layers, making accurate estimation essential for pavement design. This study conducted constant radial stiffness triaxial (CRST) tests on an unbound granular material and a subgrade soil at various dry densities, saturation degrees, and stress conditions. The CRST test applies dynamic confining pressure under constant radial stiffness boundary. New models for rutting and resilient modulus were developed, relating these parameters to initial dry densities, saturation degrees, and stress states. The study also presents rutting and resilient modulus isograms on the compaction plane, aiding field compaction control and robust pavement design.

Research on Multiple-Factor Dynamic Constitutive Model of Poured Asphalt Concrete.

This study conducted dynamic triaxial tests on a typical poured asphalt concrete material of core walls in Xinjiang, exploring the dynamic characteristics of poured asphalt concrete under various confining pressures, principal stress ratios, and vibration frequencies. On this basis, the dynamic constitutive relationship of poured asphalt concrete was investigated using the Hardin-Drnevich model. The results indicate that under different confining pressures, principal stress ratios, and vibration frequencies, the variation patterns of the backbone lines of dynamic stress-strain of poured asphalt concrete are basically identical, consistent with a hyperbolic curve. The confining pressure and principal stress ratio significantly affect the backbone line of dynamic stress-strain. By comparison, frequency has a minimal effect. The changing trends of dynamic elasticity modulus and damping ratio of poured asphalt concrete under various factors are almost the same. When the material has high dynamic stress and strain, the hysteresis loop is large. When the curve of the damping ratio becomes flat, the asymptotic constant can be used as the maximum damping ratio. The relationship between the reciprocal of the dynamic elasticity modulus and the dynamic strain of poured asphalt concrete exhibits a linear distribution. Under different ratios of confining pressure to principal stress, there are large discrepancies between the calculated values from the formula and the experimental fitting values of the maximum dynamic elasticity modulus, and the maximum relative errors reach 16.65% and 18.15%, respectively. Therefore, the expression for the maximum dynamic elasticity modulus was modified, and the calculated values using the modified formula were compared with the experimental fitting values. The relative errors are significantly reduced, and the maximum relative errors are 3.02% and 2.04%, respectively, in good agreement with the fitting values of the experimental data. The findings of this article render a theoretical basis and reference for the promotion and application of poured asphalt concrete.

Multi-scale investigation on staged deterioration mechanism of sliding-zone soils induced by reservoir fluctuations

Water level fluctuations in the reservoir deteriorate soils and rocks on the bank landslides by drying-wetting (D-W) cycles, which results in a significant decrease in mechanical properties. A comprehensive understanding of deterioration mechanism of sliding-zone soils is of great significance for interpreting the deformation behavior of landslides. However, quantitative investigation on the deterioration characteristics of soils considering the structural evolution under D-W cycles is still limited. Here, we carry out a series of laboratory tests to characterize the multi-scale deterioration of sliding-zone soils and reveal the mechanism of shear strength decay under D-W cycles. Firstly, we describe the micropores into five grades by scanning electron microscope and observe a critical change in porosity after the first three cycles. We categorize the mesoscale cracks into five classes using digital photography and observe a stepwise increase in crack area ratio. Secondly, we propose a shear strength decay model based on fractal theory which is verified by the results of consolidated undrained triaxial tests. Cohesion and friction angle of sliding-zone soils are found to show different decay patterns resulting from the staged evolution of structure. Then, structural deterioration processes including cementation destruction, pores expansion, aggregations decomposition, and clusters assembly are considered to occur to decay the shear strength differently. Finally, a three-stage deterioration mechanism associated with four structural deterioration processes is revealed, which helps to better interpret the intrinsic mechanism of shear strength decay. These findings provide the theoretical basis for the further accurate evaluation of reservoir landslides stability under water level fluctuations.

Modeling a Flexible Membrane for Triaxial Tests with Coupled FDM–DEM: Considering Realistic Particle Shape Effects

Modeling a Flexible Membrane for Triaxial Tests with Coupled FDM–DEM: Considering Realistic Particle Shape Effects

Effects of bacterial strains on undrained cyclic behavior of bio-cemented sand considering wetting and drying cycles

The microbial-induced calcite precipitation (MICP) technique has been developed as a sustainable methodology for the improvement of the engineering characteristics of sandy soils. However, the efficiency of MICP-treated sand has not been well established in the literature considering cyclic loading under undrained conditions. Furthermore, the efficacy of different bacterial strains in enhancing the cyclic properties of MICP-treated sand has not been sufficiently documented. Moreover, the effect of wetting-drying (WD) cycles on the cyclic characteristics of MICP-treated sand is not readily available, which may contribute to the limited adoption of MICP treatment in field applications. In this study, strain-controlled consolidated undrained (CU) cyclic triaxial testing was conducted to evaluate the effects of MICP treatment on standard Ennore sand from India with two bacterial strains: Sporosarcina pasteurii and Bacillus subtilis. The treatment durations of 7 d and 14 d were considered, with an interval of 12 h between treatments. The cyclic characteristics, such as the shear modulus and damping ratio, of the MICP-treated sand with the different bacterial strains have been estimated and compared. Furthermore, the effect of WD cycles on the cyclic characteristics of MICP-treated sand has been evaluated considering 5–15 cycles and aging of samples up to three months. The findings of this study may be helpful in assessing the cyclic characteristics of MICP-treated sand, considering the influence of different bacterial strains, treatment duration, and WD cycles.

Real-time monitoring of rock fracture by true triaxial test using fiber-optic strain monitoring in adjacent wells

The real-time monitoring of fracture propagation during hydraulic fracturing is crucial for obtaining a deeper understanding of fracture morphology and optimizing hydraulic fracture designs. Accurate measurements of key fracture parameters, such as the fracture height and width, are particularly important to ensure efficient oilfield development and precise fracture diagnosis. This study utilized the optical frequency domain reflectometer (OFDR) technique in physical simulation experiments to monitor fractures during indoor true triaxial hydraulic fracturing experiments. The results indicate that the distributed fiber optic strain monitoring technology can efficiently capture the initiation and expansion of fractures. In horizontal well monitoring, the fiber strain waterfall plot can be used to interpret the fracture width, initiation location, and expansion speed. The fiber response can be divided into three stages: strain contraction convergence, strain band formation, and postshutdown strain rate reversal. When the fracture does not contact the fiber, a dual peak strain phenomenon occurs in the fiber and gradually converges as the fracture approaches. During vertical well monitoring in adjacent wells, within the effective monitoring range of the fiber, the axial strain produced by the fiber can represent the fracture height with an accuracy of 95.6% relative to the actual fracture height. This study provides a new perspective on real-time fracture monitoring. The response patterns of fiber-induced strain due to fractures can help us better understand and assess the dynamic fracture behavior, offering significant value for the optimization of oilfield development and fracture diagnostic techniques.

Low-carbon metakaolin precursor for one-part and two-part geopolymer activation of demolition wastes

A critical part of civil engineering infrastructure works is to develop innovative construction materials for a low-carbon future development. This study delved into the feasibility of using metakaolin (MK) as a low-carbon precursor for one-part and two-part geopolymer stabilization of recycled demolition wastes. In this research, the effects of MK precursor were evaluated in combination with construction and demolition (C&D) waste aggregates such as crushed brick (CB), reclaimed asphalt (RAP) and recycled concrete (RCA) using one-part and two-part geopolymer activation. Various geotechnical tests were performed including compaction tests, repeated triaxial loading tests (RLT), unconfined compressive strength tests (UCS) and microstructural analysis. Results from this study indicated significant strength development of MK mixtures for both one-part and two-part geopolymer options. Furthermore, one-part geopolymer also showed better activation than two-part geopolymer under 7 days and 20℃ curing condition. Additionally, 30 % MK mixtures were optimal for road construction applications based on the obtained results. At 28 days or 40 ℃, MK mixtures performed best with RCA and CB as main aggregates, showing strength improvement of up to 250 % compared to 7 days and 20 ℃ curing condition. Resilient modulus (Mr) results indicated that the optimal mixtures experienced good resilient behavior with average Mr values ranging from 150 MPa to 200 MPa. Overall, MK precursor was found to be a suitable material for stabilizing demolition aggregates using geopolymer under various curing conditions.

Study on the influence of vertical stress difference coefficient on fracture characteristics of shale under high stress

AbstractTo study the effect of vertical stress difference coefficient on fracture characteristics of shale fracturing, high stress true triaxial hydraulic fracturing test was carried out. By analyzing the profile after fracturing, it was found that the area of hydraulic fracture increased with the increase of vertical stress difference coefficient, and the probability of shear fracture will increase when the stress difference coefficient was high. A high vertical stress differential coefficient exerts a strong control over the direction of crack propagation, while a low vertical stress difference coefficient is beneficial to improve the roughness of hydraulic fracture surface and promote the formation of complex fracture network. By analyzing the pump pressure curves of different tests, it was found that with the increase of vertical stress difference coefficient, the formation and expansion of hydraulic fractures were more difficult. The surface characteristics of hydraulic fractures were quantified based on three‐dimensional topography scanning technology, combined with fractal dimension and fracture area calculation method, the results showed that with the increase of vertical stress difference coefficient, the fractal dimension and fracture area decreased. Since shale is stratified, and the transformation of reservoir is mainly reflected in the enhancement of fracture complexity through tensile failure, Xsite discrete grid method was used to study the influence of fracture propagation behavior with different bedding strengths. The results showed that when the bedding tensile strength was high, hydraulic fractures were easy to pass through the bedding, and when the bedding tensile strength was low, hydraulic fractures were easy to be captured by natural fractures. In addition, tensile cracks were easy to form when the tensile strength of bedding was low, shear cracks were easy to form when the strength of bedding was high, and the fracture volume was larger when the strength of bedding was low. This study provides a theoretical basis for hydraulic fracturing in engineering.

Comparative study on in-situ resilient modulus of subgrade estimated using in-situ modulus detector

This study presents a comprehensive evaluation of the resilient modulus of unsaturated subgrade soils using a novel in-situ modulus detector (IMD) along with various laboratory and field-testing methods. The current study employs several testing devices, including bender elements, standard dynamic cone penetrometer, and crosshole-type dynamic cone penetrometer (CDP), to assess the reliability of the IMD in estimating the resilient modulus profiles of small-scale homogeneous subgrade models in unsaturated conditions. The index properties, compaction and strength characteristics of the compacted soils, are evaluated. The resilient modulus values obtained from the IMD are compared with those obtained from repeated load triaxial tests under various stress states. Experimental results show a decrease in the penetration depth per blow with increased dry unit weight. In addition, elastic modulus and shear wave velocity increase with soil density. The resilient modulus estimated from the IMD increase with both depth and soil density. A robust correlation has been established between the resilient modulus values estimated from the IMD and those estimated from the CDP or bender element tests. Furthermore, the resilient moduli estimated from the universal model and the IMD demonstrate linear relationships with a coefficient of determination greater than 0.8. Thus, the IMD may be useful for the in-situ evaluation of resilient modulus in unsaturated subgrade soils, considering influencing factors such as soil density and confining pressure.

Stress-dependent Mohr–Coulomb shear strength parameters for intact rock

Rock strength is imperative for the design and stability analysis of engineering structures. The Mohr–Coulomb (M-C) criterion holds significant prominence in geotechnical engineering. However, the M-C criterion fails to accurately capture the nonlinear strength response and neglects the critical state of rocks, potentially leading to inaccuracies in the design phase of deep engineering projects. This study introduces an innovative stress-dependent friction angle and cohesion (SFC) for the M-C criterion to capture the nonlinear strength responses of intact rocks, spanning from non-critical to critical states (brittle to ductile regions). A novel method for determining these stress-dependent parameters at each corresponding σ3\\documentclass[12pt]{minimal} \\usepackage{amsmath} \\usepackage{wasysym} \\usepackage{amsfonts} \\usepackage{amssymb} \\usepackage{amsbsy} \\usepackage{mathrsfs} \\usepackage{upgreek} \\setlength{\\oddsidemargin}{-69pt} \\begin{document}$$\\sigma_{3}$$\\end{document} is initially introduced. Subsequently, an examination of the confinement dependency of the friction angle and cohesion is conducted, leading to the derivation of the SFC model. The SFC-enhanced M-C criterion, utilizing parameters obtained from triaxial tests under lower σ3\\documentclass[12pt]{minimal} \\usepackage{amsmath} \\usepackage{wasysym} \\usepackage{amsfonts} \\usepackage{amssymb} \\usepackage{amsbsy} \\usepackage{mathrsfs} \\usepackage{upgreek} \\setlength{\\oddsidemargin}{-69pt} \\begin{document}$$\\sigma_{3}$$\\end{document}, demonstrates the capability to delineate the complete non-linear strength envelope from brittle to ductile regions. Validation through triaxial test data confirms that the predictions of the SFC-enhanced M-C criterion accurately correspond to the strength characteristics of the tested rocks.

Parameter determination of Johnson–Holmquist–Cook constitutive model and calibration for Indiana Limestone

In this study, a comprehensive parameter determination procedure for the Johnson–Holmquist–Cook (JHC) constitutive model is introduced, including calibration and validation processes for Indiana Limestone rocks. The procedure is conducted utilizing the existing physical and mechanical properties of Indiana Limestone. To obtain an accurate set of parameters for the JHC model for Indiana Limestone, an extensive dataset comprising mechanical and physical properties of Indiana Limestone rocks was initially compiled. The static mechanical tests incorporated uniaxial compression, triaxial compression, direct tensile, and uniaxial strain data, while the dynamic mechanical test data was primarily derived from the Split Hopkinson Pressure Bar experiments. Subsequently, the JHC constitutive model parameters were determined using existing literature data, employing statistical analysis, theoretical derivation, and numerical back analysis techniques. One of the damage parameters was determined through numerical post-peak behavior calibration of triaxial compression strength test results on experimental data. Finally, the accuracy of the determined parameters was validated by comparing the numerical and experimental results of both static and dynamic tests. This study effectively addresses the challenges associated with the numerical method using the JHC material model, such as the complex parameter determination process and the costly required tests, thereby preserving the efficiency and applicability of the numerical method.

Exploring the Macroscopic Behavior and Microstructure Evolution of Lightly Cemented Sand in the Post-Liquefaction Process Using DEM.

This study investigates the post-liquefaction monotonic undrained shearing behavior of cemented sand at the macro- and microscales, using the discrete element method. A series of cyclic undrained triaxial tests with different stress amplitudes and post-liquefaction monotonic undrained triaxial tests were simulated on cemented sand with diverse cement contents (CCs). For comparison, a series of monotonic undrained triaxial tests on cemented sand without liquefaction (virgin cemented sand) were also modeled. The macroscopic behavior was analyzed in conjunction with the microscopic characteristics of the assembly, such as the deviator fabric of contact normal orientation, mechanical coordination number, energy components, and bond breakage. The results show that the DEM model can capture the effect of CC and cyclic stress ratio (CSR) on the undrained shear strength, stiffness, and pore pressure observed in laboratory experiments. Referring to the virgin specimen, with an increase in CC, the mechanical coordination number and the input work increment increase, while the deviator fabric for total contacts changes irregularly, leading to a greater initial stiffness and shear strength. In the case of the liquefied specimen, the smaller initial mechanical coordination number results in a very low initial stiffness regardless of CC. Contrary to the uncemented sand, both the mechanical coordination number and the input work increment decrease with an increasing CSR for the cemented sand. The microstructure evolution governs the effect of cementation level and liquefaction history on the macroscopic post-liquefaction behavior.

Results of the cyclic triaxial testing on mechanically-biologically treated waste.

Accurate assessment of the dynamic strength characteristics of mechanically-biologically treated (MBT) waste is crucial for the construction and safe operation of landfill sites. Herein, samples of MBT waste from the Hangzhou Tianziling landfill were collected and subjected to consolidated undrained cyclic triaxial tests under four confinement levels and six cyclic stress ratios (CSRs). Under cyclic loading, the MBT waste exhibited a critical CSR. If the CSR exceeds the critical value, the MBT waste specimen rapidly undergoes deformation and failure. Dynamic strength of MBT waste decreases with an increase in the number of cyclic vibrations and increases with an increase in confining pressure. Considering the influence of cyclic vibrations and confining pressure, a formula for dynamic strength in terms of cyclic vibrations and confining pressure has been established. The dynamic shear strength parameter ranges for MBT waste were obtained under different seismic magnitudes. We compared the dynamic and static shear strength parameters of MBT waste and municipal solid waste. These study findings can serve as a reference for the dynamic stability analysis of MBT waste landfills.

The mechanism of low strain rate and moderate principal stress effects in triaxial prestressed marble under lateral impulsive load

Stress waves have a significant impact on the strength and deformation characteristics of deep rock masses at a certain distance from the epicenter or explosion source. In order to study the dynamic responses of deep-buried marble under the disturbance condition, the true triaxial compression test (TTC), the true triaxial disturbed compression test with lateral impulsive load (TTDC) and the synchronous acoustic emission monitoring on the marble were respectively conducted to simulate the influencing process of the seismic wave. The test results show that under lateral impulsive load, a ‘short-range plateau’ phenomenon occurs in the stress-strain curves of the marble samples. With the increase of intermediate principal stress σ2, the ‘short-range plateau’ of ε2 and ε3 curves gradually shrinks and even disappears, and the anisotropy of sample deformation becomes more obvious. The σ2 significantly affects the microfracture activity and the evolution of energy inside the samples under the impulsive load in the whole process of true triaxial disturbed compression. The lateral impulsive load weakens the marble strength which shows an obvious low strain-rate disturbance effect. The marble samples under the impulsive load have a high sensitivity to axial load and are liable to form local brittle fracture. This fracture induced by local stress concentration and strain energy release becomes more pronounced when the axial load is further applied to the samples. By contrast, the impulsive load in σ2 direction has a protective effect on limiting the lateral deformation of the samples and improving its axial deformation capacity, which greatly changes the action mechanism of σ2 on the sample lateral deformation. The variation of marble mechanical properties under lateral impulsive load is the result of the interaction between the low strain-rate disturbance and the intermediate principal stress effect.

Adopting a systems engineering approach to a feasibility study of a sidings development at the Midsomer Norton railway station

It is planned to reopen Midsomer Norton railway station, which is a station on the Somerset & Dorset Heritage Railway Line, to traffic. As a first step, Midsomer Norton will be a terminus, and it is proposed to build sidings and a depot for the trains that terminate there. However, a ground investigation is essential before commencing construction of the sidings and the depot, as this is a vital part of any civil engineering process. The behaviour of the ground must be known in order for a structure to be supported by it; therefore, data from the ground investigation are used as reference for any kind of structure development. This study covers a site investigation that includes a desk study, walkover survey, sampling and laboratory testing in order to ascertain the feasibility of a suitable design. Moisture content testing, liquid limit and plastic limit tests, standard compaction testing, shear vane tests, and triaxial compression tests were carried out to determine the soil characteristics and to analyse the soil behaviour. A strong recommendation was made to follow a systems engineering approach in the construction phase, as well as in the design stage. The dependability of the system is ensured by the good use of V – process of systems engineering.

Thermo-hydro-mechanical coupling in oil shale: Investigating permeability and heat transfer under high-temperature steam injection

Steam convective heating emerges as a sustainable and effective method for extracting oil shale, where understanding the temperature-dependent evolution of its pyrolytic characteristics, microstructure, and permeability is vital for efficient resource extraction. Through a stress-sensitive micro-CT scanning and a high-temperature and pressure triaxial test apparatus, this research utilizes Balikun oil shale samples to investigate the changes in microstructure and gas production from 20 °C to 550 °C. The study integrates theoretical analysis and numerical simulations to uncover the fundamental connections between internal permeability and heat transfer mechanisms during steam injection. It reveals that oil shale undergoes two critical evolutionary phases: a stability phase below 350 °C, where volatile dispersion occurs, and a rapid increase phase above 350 °C, marked by significant microstructural changes from micro-fractures to extensive through-going fractures due to intense thermal decomposition. This decomposition leads to increased gas production and enhanced thermal fracturing. The threshold temperature is identified at 400 °C, above which the oil shale's mechanical strength and pore pressure increase, leading to decreased volumetric compression until stabilization. These findings demonstrate that higher temperatures enhance fracture connectivity and steam flow, optimizing the heating efficiency in oil shale extraction.

Study on the Shear Strength and Erosion Resistance of Sand Solidified by Enzyme-Induced Calcium Carbonate Precipitation (EICP).

Sand solidification of earth-rock dams is the key to flood discharge capacity and collapse prevention of earth-rock dams. It is urgent to find an economical, environmentally friendly, and durable sand solidification technology. However, the traditional grouting reinforcement method has some problems, such as high costs, complex operations, and environmental pollution. Enzyme-induced calcium carbonate precipitation (EICP) is an anti-seepage reinforcement technology emerging in recent years with the characteristics of economy, environmental protection, and durability. The erosion resistance and shear strength of earth-rock dams solidified by EICP need further verification. In this paper, EICP-solidified standard sand is taken as the research object, and EICP-cemented standard sand is carried out by a consolidated undrained triaxial test. A two-stage pouring method is adopted to pour samples, and the effects of dry density, cementation times, standing time, and confining pressure on the shear strength of cemented standard sand are emphatically analyzed. The relationship between cohesion, internal friction angle, and CaCO3 formation was analyzed. After the optimal curing conditions are obtained through the triaxial shear strength test, the erosion resistance model test is carried out. The effects of erosion angle, erosion flow rate, and erosion time on the erosion resistance of EICP-solidified sand were analyzed through an erosion model test. The results of triaxial tests show that the standard sand solidified by EICP exhibits strain softening, and the peak strength increases with the increase in initial dry density, cementation times, standing time, and confining pressure. When the content of CaCO3 increases from 2.84 g to 12.61 g, the cohesive force and internal friction angle change to 23.13 times and 1.18 times, and the determination coefficients reach 0.93 and 0.94, respectively. Erosion model test results indicate that the EICP-solidified sand dam has good erosion resistance. As the increase in erosion angle, erosion flow rate, and erosion time, the breach of solidified samples gradually becomes larger. Due to the deep solidification of sand by EICP, the development of breaches is relatively slow. Under different erosion conditions, the solidified samples did not collapse and the dam broke. The research results have important reference value and scientific significance for the practice of sand consolidation engineering in earth-rock dams.