Three-point Bending Experiments Research Articles

Insights into the fracture properties of recycled ceramic and rubber composite cement-based materials: Fracture mechanics, acoustic emission, and digital image correlation

Recycling plays a pivotal role in construction waste management, offering a path toward sustainability for the industry. Although waste ceramics can compensate for the mechanical properties of rubberized cement-based materials, the smooth glaze surface of waste ceramics increases the risk of brittle failure. This study investigated the effect of ceramic waste aggregate (CWA) on the fracture properties of rubberized mortar through the three-point bending experiment. The fracture parameters were calculated using the Double-K fracture criterion. Simultaneously, acoustic emission (AE) and digital image correlation (DIC) technologies were used to explore the fracture damage mechanism and the crack evolution process. The results indicate that the integration of 15 % and 45 % CWA significantly enhances both initiation (KICini) and unstable (KICun) fracture toughness, whereas incorporating 90 % CWA leads to a 16.8 % and 8.2 % decrease in (KICini)and (KICun), respectively. The fracture energy (GF) of rubberized mortar exhibits a continuous decline as a function of increasing CWA substitution rates. Furthermore, GMM-based RA-AF analysis elucidates a positive correlation between CWA content and tensile crack proportion in specimens. When the CWA content reaches 90 %, the proportion of tensile cracks is quantified at 29.83 %, surpassing that in standard mortar. Crack tip opening displacement (CTOD) at 0.5post-Pmax for specimens with 15 %, 45 %, and 90 % CWA substitution reveal improvements of 49.1 % and 17.2 %, and a decrease of 23.3 %, respectively, compared to standard mortar, indicating that 15 % and 45 % CWA effectively preserve the ductility of rubberized mortar. Elevated CWA substitution leads to an amplified strain localization phenomenon around the crack tip, heightening the propensity for brittle failure.

Facile purification of glass fiber powder by sedimentation for enhanced epoxy resin composites

Glass fiber powder contains two distinct forms: crumb-shaped and rod-shaped glass fiber powder particles. The shape and size of the particles in glass fiber powder have a great influence on its application. In order to separate rod-shaped glass fiber, the effects of different dispersants, such as SHMP, NaOL, and Na2SiO3 on them were investigated by settling experiments. Zeta potential, X-ray photoelectron spectroscopy (XPS), optical microscope, and other methods were used to analyze the adsorption behavior and settling mechanism. Three-point bending experiment and dynamic mechanical analysis (DMA) were used to evaluate the performance of epoxy resin composites reinforced with the raw glass fiber powder and the rod-shaped glass fiber powder. The results show that SHMP can effectively separate crumb-shaped glass fiber powder and rod-shaped glass fiber powder, leading to a notable increase in sedimentation recovery difference, up to Δ=51.08%. A preferential sedimentation separation mechanism is proposed to elucidate the settling mechanism. When the content of glass fiber powder and rod-shaped glass fiber is 5%, the glass transition temperature shifts significantly towards higher values, leading to the optimum comprehensive mechanical properties of the composites. Compared with the original epoxy resin, the flexural strength increased by 10.38% to 95.18 MPa and by 20.11% to 103.57 MPa. Similarly, the storage modulus increased by 14.14% to 2083 MPa and by 21.64% to 2220 MPa.

Crack development and fracture performance of Recycled Powder Engineered Cementitious Composites (ECC): Experimental investigation

In this paper, recycled concrete powder (RCP) and recycled brick powder (RBP), with particle sizes ranging from 10 to 130 μm, are used to completely replace the fine aggregate quartz sand at a ratio of 1:1. On this basis, recycled glass powder (RGP), with a discussed particle sizes range of 38–300 μm, is used to partially substitute the cementitious materials. Polyethylene (PE) fibers are used as the reinforcement in the Engineered Cementitious Composites (ECC). Using the particle size range and substitution rate of RGP as variables, the crack development, crack mouth opening displacement (CMOD), fracture toughness and fracture energy of Recycled glass powder ECC (RGP-ECC) were discussed through a three-point bending experiment on a single-edge notch beam. A relatively comprehensive evaluation was made on the fracture performance and behavior of recycled ECC, and a suitable mix ratio of recycled powder ECC was given. The results show that the addition of various recycled powders will not affect the multi-slit cracking behavior of ECC, and the cracks can still spread densely, giving the specimen greater deformation capacity and CMOD. The total substitution of fine aggregate by RCP and RBP has a positive impact on the fracture toughness KICini, KICun and fracture energy (GF), but the addition of RGP has some minor negative effects. Among the particle size range and substitution rate of RGP, the influence of substitution rate is more obvious, and the fracture performance will show a downward trend after growth as the substitution rate increases. Choosing the appropriate RGP substitution rate and particle size range can maximize the recycling of construction waste while ensuring fracture performance.

Static and modal analysis of sandwich panels with rib-reinforced re-entrant honeycomb

The low stiffness resulting from substantial core porosity within the re-entrant honeycomb sandwich panel can be addressed by introducing rib-reinforcements. To investigate its static and vibration characteristics, an energy-based 2D equivalent-homogenization model (2D-EHM) was derived through asymptotic analysis of the leading terms in the governing equations considering the energy-related characteristics. The accuracy of the constructed model for predicting the elastic bending performance of the sandwich panel was verified by comparing the results of a three-point bending experiment with 3D-printed specimens. Comparative analysis with a 3D FE model demonstrates that the 2D-EHM exhibits maximum errors of only 4.65% and 6.46%, respectively, in analyzing static deformation and natural frequency while improving computational efficiencies by up to 59- and 173-folds. Parameter analysis reveals that the performance of SP-RRH is minimally affected by the reinforcement-to-honeycomb wall thickness ratio. However, its performance is compromised when the honeycomb walls align in an equilateral triangle with the reinforcing walls. Comparing specific stiffness as well as static and vibration characteristics of sandwich panels with different core configurations (including traditional and diamond reinforced re-entrant honeycombs) shows that inclusion of rib reinforcements enhances deformation resistance and natural frequencies through increased specific stiffness. These findings provide valuable insights for optimizing design of re-entrant honeycomb sandwich panels.

Study on the Mechanical Properties of a Carbon-Fiber/Glass-Fiber Hybrid Foam Sandwich Structure.

Considering the different structural strength requirements of different parts of fiberglass yachts, carbon fiber/glass fiber hybrid reinforcement can be applied to the skins of sandwich panels in special areas. This paper designs and prepares 12 foam sandwich panel samples composed of pure carbon fiber, a carbon fiber/glass fiber hybrid, pure glass fiber skin, and PVC and SAN foam sandwich, with reference to the layup structure of the outer panel of a fiberglass yacht. Through a comparative analysis of low-speed impact experiments, edge compression experiments, and short beam three-point bending experiments, we seek the optimal carbon fiber/glass fiber hybrid layup design scheme for local structures to guide production. The results show that a reasonable hybrid carbon fiber layup in fiberglass skin can effectively reduce the low-speed impact damage of the sandwich structure, reduce edge compression damage, and improve the bending and compression resistance of sandwich structure. The impact resistance, compression resistance, and shear resistance of the SAN sandwich structure are stronger than the PVC sandwich structure. The carbon fiber/glass fiber hybrid SAN foam sandwich structure can be used for the local structural reinforcement of special parts such as the bow, side, and main deck of fiberglass yachts.

Mode I fracture propagation and post-peak behavior of sandstone: Insight from AE and DIC observation

Microcracks generated at the crack tip, particularly in quasi-brittle materials such as sandstone, give rise to a non-linear region known as the fracture process zone (FPZ), which cannot be analyzed using linear elastic fracture mechanics (LEFM). To gain insights into the nonlinear fracturing behavior of rock, this study conducted three-point bending experiments on sandstone beams with prefabricated notch. Stable mode-Ⅰ fracture propagation during the post-peak stage was achieved by the monotonic increment of crack mouth opening displacement (CMOD) measured by a clip gauge. The acoustic emission (AE) and digital image correlation (DIC) techniques were utilized to visually track the detailed crack propagation process from both micro and macro perspectives. Nonlinear fracture parameters, including FPZ length, were identified by AE and DIC measurements and compared with the theoretical calculation. A nonlinear fracture criterion relating applied load, equivalent crack length, and stress intensity factor were established, from which the theoretical CMOD-P curve at the post-peak stage were obtained and validated with experimental measurement from MTS machine. The results reveal that microcracks formulating the FPZ materialize in the pre-peak stage, with the majority emerging post-peak to facilitate the propagation of the traction-free crack and FPZ in the loading direction, as evidenced by AE locations and DIC displacement gradient. Throughout the crack propagation process, over 65 % of microcracks are estimated to be tensile mode based on both AF/RA and polarity analysis, aligning with anticipated outcomes from macroscopic three-point bending fracture tests. Energy dissipation primarily occurs within the FPZ to facilitate separation of crack faces, with the dissipated energy region advancing towards the beam boundary. By integrating AE source locations and DIC displacement gradient, the FPZ length of the 3-point-bending sandstone specimens is determined to be lp = 8.1 mm, slightly exceeding the theoretical FPZ lengths calculated by the Irwin model (lp = 7.0 mm) and the Dugdale-Barenblatt model (lp = 7.6 mm). Using a non-linear fracture criterion that incorporates the FPZ and employing the in-time equivalent crack length measured by AE and DIC as an intermediate variable, the theoretical applied load-crack length curve during the post-peak stage is calculated, showing close agreement with load cell measurements with a negligible error of approximately 2 %. Furthermore, the theoretical post-peak CMOD vs. load curve aligns with experimentally obtained results, demonstrating a non-linear crack propagation speed at a constant CMOD rate, wherein crack propagation speed decreases as crack length increases.

New Method for Determining Mode-I Static Fracture Toughness of Coal Using Particles.

Understanding the mechanical properties of coal is crucial for efficient mining and disaster prevention in coal mines. Coal contains numerous cracks and fissures, resulting in low strength and challenges in preparing standard samples for testing coal fracture toughness. In engineering, indicators such as the hardness coefficient (f value) and Hardgrove grindability index (HGI) are straightforward to measure. Various experiments, including drop weight, grinding, uniaxial compressive strength and three-point bending experiments, were conducted using notched semi-circular bend (NSCB) specimens and particle sizes of 1-2 mm/0.425-1 mm. Theoretical and experimental results indicate that the hardness coefficient of coal and rock is proportional to the crushing work ratio and inversely proportional to the mean equivalent diameter. Moreover, the square of the fracture toughness of coal and rock is directly proportional to the crushing work ratio, inversely proportional to the newly added area, directly proportional to the mean equivalent diameter and directly proportional to the hardness coefficient. The Mode-I fracture toughness of coal and rock can be rapidly determined through the density, the equivalent diameter after crushing and the elastic modulus, with experimental verification of its accuracy. Considering that smaller particle sizes exhibit greater resistance to breakage, the distribution mode of new surface areas after particle breakage was established, influenced by the initial particle size and the energy of a single broken particle. This study can assist in quickly and accurately determining the fracture toughness of coal.

Microstructure and mechanical properties of Ti6Al4V/W bimetallic structure via selective laser melting

The titanium alloy Ti–6Al–4V (TC4) and tungsten (W) possess excellent complementary properties that would be useful for a wide range of industrial applications if they could be suitably combined. Selective laser melting was applied to prepare TC4/W specimens with a bimetallic structure. A strong bond without interfacial macrocracks was obtained by adjusting the laser line energy density to <0.75 J/mm. The bond interface of the bimetallic structure reached a microhardness of 503 ± 20 HV, which was harder than that of the two base materials, and the transverse and longitudinal ultimate compressive strengths were 1510 ± 40 MPa at strains of 20%–22.5%. Three-point bending experiments showed that when TC4 was used as the base material, the flexural strength of the specimen was 2210.5 ± 44.5 MPa. The high strength of the bond interface was attributed to sufficient agitation of the molten pool and reinforcement by fine crystalline grains. The agitation was provided by the melting and elemental diffusion of TC4 owing to the high energy input during the formation of W, and the fine crystalline grains were obtained by the dispersed W particles providing multiple nucleation sites for liquid TC4. The bimetallic structure retained the strength of W and toughness of TC4, which bodes well for its industrial application.

Damage Mechanics Challenge: Predictions based on the phase field fracture model

In this work, we describe our contribution to the Purdue-SANDIA-LLNL Damage Mechanics Challenge. The phase field fracture model is adopted to blindly estimate the failure characteristics of the challenge test, an unconventional three-point bending experiment on an additively manufactured rock resembling a type of gypsum. The model is formulated in a variationally consistent fashion, incorporating a volumetric–deviatoric strain energy decomposition, and the numerical implementation adopts a monolithic unconditionally stable solution scheme. Our focus is on providing an efficient and simple yet rigorous approach capable of delivering accurate predictions based solely on physical parameters. Model inputs are Young’s modulus E, Poisson’s ratio ν, toughness Gc and strength σc (as determined by the choice of phase field length scale ℓ). We show that a single mode I three-point bending test is sufficient to calibrate the model, and that the calibrated model can then reliably predict the force versus displacement responses, crack paths and surface crack morphologies of more intricate three-point bending experiments that are inherently mixed-mode. Importantly, our peak load, crack trajectory and crack surface morphology predictions for the challenge test, submitted before the experimental data was released, show a remarkable agreement with experiments. The characteristics of the challenge, and how changes in these can impact the predictive abilities of phase field fracture models, are also discussed.

The investigation and estimation of flexural strength in shear-critically designed RC beams considering the steel fiber content

Despite numerous studies investigating the effectiveness of steel fibers in RC members subjected to various loading conditions, the majority ignored the impact of the interaction between the tensile reinforcement ratio, compressive strength of fibrous concrete, and steel fiber dosage. This paper aimed to inspect and quantify the effects of hooked-end steel fiber dosage on the bending behavior of RC beams considering the interaction arising from various longitudinal reinforcement ratios. For this purpose, an extensive and hybrid investigation involving both experimental and numerical techniques was conducted. In the experimental part, an investigation was carried out to evaluate the contribution of a specific amount of fiber ratio and various aspect ratios to the behavior of large-scale RC beams having a shear-deficient design. Three beams with a 0.5% hooked-end steel fiber ratio and one without fibers but with a minimum amount of stirrups were produced, and three-point bending tests were conducted. All beams having fibers utilized full flexural strength as in the beam with stirrups. Once the experimental studies were completed, the numerical models were then developed and validated with those of experimental three-point bending tests using the non-linear finite element code VecTor2 to establish a basis for the comprehensive parametric study. The parametric study consisted of 33 analyses. Rebar and volumetric fiber ratios were selected to be variables, and the ratios adopted were within the typical range used in structural engineering applications. Based on the regression analysis a linear and a quadratic model were proposed for estimating the yield and peak strength depending on the steel fiber content. Finally, the obtained models were verified using work from the literature and found to be effective in forecasting the strength of shear-deficient RC beams with 0.8%, 1.0%, and 1.2% tensile reinforcement ratios and hooked end steel fibers (0.5 to 1.5%).

Investigation of the impact of heating and liquid nitrogen (LN2) cooling on the mechanical and acoustic emission (AE) properties of coal

Liquid nitrogen has emerged as a promising fracturing medium for unconventional natural gas extraction, particularly in the context of coalbed methane extraction, generating significant interest in recent times. In this paper, we analyze the acoustic emission (AE) characteristics of coal samples treated with liquid nitrogen under three-point bending load conditions using indoor experiments and field investigations. We investigate the impact of liquid nitrogen on coal samples by analyzing AE data. The mechanical properties of coal samples with varying initial temperatures were tested under three-point bending load conditions after treatment with liquid nitrogen. The load-displacement curve was analyzed to study the mechanical properties of the coal samples after treatment with liquid nitrogen. Through indoor three-point bending experiments, data analysis, and knowledge of mechanics, we systematically investigated the changes in mechanical properties caused by liquid nitrogen treatment under different conditions. The results demonstrate that the application of liquid nitrogen has significant impacts on the mechanical and AE characteristics of coal samples. The load-displacement curve indicated that the mechanical properties of the coal samples changed after treatment with liquid nitrogen. The AE experiment revealed regular changes in vibration and energy parameters of coal samples after liquid nitrogen treatment under different conditions. We further investigated the changes in mechanical properties and deformation characteristics of coal samples after undergoing liquid nitrogen freezing and thawing in differing environments. Graphs such as load-displacement curves, load-time curves, cumulative vibration count-energy count graphs, and RA-AF density distribution diagrams visually demonstrated the changes in mechanical properties and deformation characteristics. Through an integrated approach of indoor experiments, data analysis, and knowledge of mechanics, our study provides a better understanding of the behavior of coal samples under different conditions. This understanding can contribute to the development of safer and more efficient methods for extracting coalbed methane.

Experimental study on mechanical properties and evolution of fracture failure of granite considering initial temperature damage and prefabricated fissure length

With the increasing mining depth of deep mineral resources, the influence of high temperature on the fracture failure of surrounding rock with fissures becomes increasingly serious. To investigate the fracture mechanical properties and the evolutionary characteristics of fracture process of fissured rock experiencing initial temperature damage, the three-point bending experiment was conducted on the small sized granite samples with different initial damaging temperatures and prefabricated fissure lengths by applying a μTS mesoscopic testing system. Based on the digital image correlation methods, the evolution of fracture process zone of sample was revealed. Moreover, the macroscopic fracture failure of sample was predicted by the evolution of time-varying acoustic emission b-value. The results show that with the increase of initial damaging temperature and prefabricated fissure length, the peak load of granite sample has a decreasing trend and the fracture characteristics of sample experiencing initial temperature damage gradually transform from brittleness fracture to ductility fracture, resulting in a decrease in the fracture toughness of sample. The crack tip opening displacement, the critical opening displacement and the length of fracture process zone of sample all show an increasing trend. The time interval from the time when time-varying acoustic emission b-value continues to decline to the appearance moment of macroscopic cracks is selected as the warning time of fracture failure of sample, which can conclude that the warning time increases with increasing the initial damaging temperature and prefabricated fissure length, indicating an increase in ductility and a reduction in failure suddenness of sample.

Bottom-up stochastic multiscale model for the mechanical behavior of multidirectional composite laminates with microvoids

This study for the first time develops a coherent and efficient bottom-up stochastic multiscale modeling approach, which aims at revealing the impact of microvoids on the mechanical properties and damage mechanisms of multidirectional (MD) carbon fiber-reinforced polymer (CFRP) composites. To this end, void defects within the composites are characterized using X-ray micro-computed tomography to construct a high-fidelity representative defective volume (RDV). Subsequently, the influence of voids on the microscale failure modes and macroscopic mechanical properties are analyzed by using micromechanics-based finite element (FE) method. Finally, a stochastic multiscale analysis method is developed to predict the mechanical response of MD CFRP laminates and validated by tensile and three-point bending experiments. The results indicate that the proposed framework can accurately predict the mechanical behavior and damage mechanisms of MD CFRP composites. This framework is believed to be a promising method to provide valuable guidance for reliability design and optimization of CFRP composites.

Effect of selective enhancement on the bending performance of fused deposition methods 3D-printed PLA models

The top and bottom shells of fused deposition 3D-printed PLA models are exposed to the highest stresses. To improve the bending performance of PLA models under three-point bending conditions, the models were strengthened by a selective enhancement method. Several sets of PLA models were fabricated using FDM technology, and three-point bending experiments were conducted to compare the bending strength of PLA models when the layer height, top/bottom shell thickness, and extrusion rate were varied. The bending strength of the PLA models increased as the layer height of the top/bottom shell decreased, the thickness increased, and the extrusion rate increased. The average bending strength of the PLA models after selective enhancement was 84.4 MPa, and the average bending modulus of elasticity was 0.816 GPa, which were higher than the average bending strength of 68.6 MPa and the average bending modulus of elasticity of 0.736 GPa of the conventional groups. These results indicated that the selective enhancement method improved the bending performance of 3D-printed PLA models, and it also provided a reference for the improvement of the mechanical properties of the 3D-printed models with cellulose composite reinforced materials.

Mechanical Properties of Sandwiched Construction with Composite and Hybrid Core Structure

In the field of lighter substitute materials, sandwich plate models of composite and hybrid foam cores are used in this study. Three core structures: composite core structure and then the core is replaced by a structure of a closed and open repeating cellular pattern manufactured with 3D printing technology. It finally integrated both into one hybrid open-cell core filled with foam and employed the same device (WBW-100E) to conduct the three-point bending experiment. The test was conducted based on the international standard (ASTM-C 393-00) to perform the three-point bending investigation on the sandwich structure. Flexural test finding, with the hybrid polyurethane/polytropic acid (PUR/PLA) core, the ultimate bending load is increased by 127.7% compared to the open-cell structure core. In addition, the maximum deflection increased by 163.3%. The simulation results of three-point bending indicate that employing a hybrid combination of PUR-PLA led to an increase of 382.3%, and for PUR–TPU by 111.8%; however, the highest value recorded with PUR/PLA, which has the slightest stress error among the tests. Also, it is reported that when the volume fraction of reinforced aluminum particles is increased, the overall deformation becomes more sufficient, and the test accuracy improves; for example, rising from 0.5% to 3%, the midspan deflection of composite (foam-Al) is increased by 40.34%. There were noticeable improvements in mechanical properties in the 2.5% composite foam-Al.

Comparative analysis for strain response and life monitoring of composite using carbon-based nanosensors

Sensing technology based on carbon nanomaterials has become a very promising technology in the field of composite health monitoring, which requires high-sensitivity piezoresistive strain sensors to serve. In this study, two different carbon nano-sensors were used. Based on the traditional carbon nano-paper sensor, a flexible printed circuit and a polysulfone membrane were added to ensure the stability and sensitivity of the sensor. The conductive mechanism of adjacent carbon nanotubes (CNT) was analyzed. The electrical network model inside the carbon nanosensor was established, and its working mechanism during loading and unloading was described. The research mainly adopts three-point bending experiment. The deformation and failure of composite laminates containing two kinds of sensors under load experience low strain and high strain cyclic loading. Both sensors have the same response and stability as the load growth trend. Experiments show that the CNT-Paper sensor is suitable for long-term health monitoring of composite materials. The carbon nanotube-ultrafiltration membrane (CNT-UM) sensor is more sensitive to the cyclic monitoring of small strain.

Study of the defect-crack offset distance on the impact fracture behavior of plexiglass

To study the interaction of moving cracks and pre-cracks of plexiglass (PMMA) under impact loading, a three-point bending experiment was carried out using dynamic caustics experimental system. Research showed that when the offset distance between the pre-crack and the defect is 9 mm, the failure mode of the crack is the most complicated. When the offset distance is 0 mm, the crack experiences the attraction force of the defect, the stress intensity factor and the crack growth speed increase gradually, and the peak value is reached when the defect and the crack intersect. When the offset distance is greater than 6 mm, the attraction effect of the defect on the crack is no longer significant, and the crack propagates toward the drop hammer location until it penetrates the specimen. As the crack propagates, the caustic speckle rotates counterclockwise and is subjected to compression and shear.

Recurrent Neural Networks and Three-Point Bending Test on the Identification of Material Hardening Parameters

The continuous evolution of metallic alloys in the automotive industry has led to the development of more advanced and flexible constitutive models that attempt to accurately describe the various fundamental properties and behavior of these materials. These models have become increasingly complex, incorporating a larger number of parameters that require an accurate calibration procedure to fit the constitutive parameters with experimental data. In this context, machine learning (ML) methodologies have the potential to advance material constitutive modeling, enhancing the efficiency of the material parameter calibration procedure. Recurrent neural networks (RNNs) stand out among various learning algorithms due to their ability to process sequential data and overcome limitations imposed by nonlinearities and multiple parameters involved in phenomenological models. This study explores the modeling capabilities of long short-term memory (LSTM) structures, a type of RNN, in predicting the hardening behavior of a sheet metal material using the results of a standardized experimental three-point bending test, with the aim of extending this methodology to other experimental tests and constitutive models. Additionally, a variable analysis is performed to select the most important variables for this experimental test and assess the influence of friction, material thickness, and elastic and plastic properties on the accuracy of predictions made by neural networks. The required data for designing and training the network solutions are collected from numerical simulations using finite element methodology (FEM), which are subsequently validated by experiments. The results demonstrate that the proposed LSTM-based approach outperforms traditional identification techniques in predicting the material hardening parameters. This suggests that the developed procedure can be effectively applied to efficiently characterize different materials, especially those extensively used in industrial applications, ranging from mild steels to advanced high-strength steels.

Performance of 3D printing biomimetic conch shell and pearl shell hybrid design composites under quasi-static three-point bending load

The failure process of biomimetic hybrid design composite composed of layers of conch shell and pearl shell was studied through quasi-static three-point bending experiments and numerical simulations. The biomimetic conch shell structure with inclined angles serves as the upper layer of the hybrid structure, while the biomimetic pearl shell structure with traditional brick and mud structure serves as the lower layer of the hybrid structure, forming a hybrid design structure. Four inclined angles were designed for the structural units of the conch shell, namely 15°, 30°, 45°, and 60°. Twenty-four specimens (six specimens for each inclined angle) were prepared using 3D printing technology using both soft and hard matrix materials. The influence of different inclined angles on the fracture strength, fracture toughness, and energy absorption of hybrid design structures was experimentally studied. The biomimetic hybrid design composite specimen with a notch is placed between two supporting rollers, and a loading indenter acts at mid-span. All twenty-four specimens were notched with a triangular tip and a rectangular bottom. A loading rate of 1 mm/min is used to avoid the viscoelastic effect of the composite materials. Details of the specimens, the experimental set-up and procedure are discussed in this paper. Complementary to the experimental studies, an extensive numerical investigation was carried out to study the influence of the aspect ratio of brick and mud units on the fracture initiation and failure of hybrid design structures. The causes of crack initiation and propagation, and failure modes in biomimetic hybrid design structures were postulated. These numerical findings help in reinforcing the experimental results and provide crucial information to enhance further research in this exciting area.

Experimental validation of auxetic stent designs: three-point bending of 3D printed Titanium prototypes.

Numerical simulations have demonstrated the superior bending flexibility of auxetic stents compared to conventional stent designs for endovascular procedures. However, conventional stent manufacturing techniques struggle to produce complex auxetic stent designs, fueling the adoption of additive manufacturing techniques. In this study, we employed DMLS additive manufacturing to create Titanium Ti64 alloy stent prototypes based on auxetic stent designs investigated in a previous study. These prototypes were then subjected to experimental three-point bending tests. The experimental results were replicated using a finite element model, which showed remarkable accuracy in predicting the bending flexibility of four auxetic stents and two conventional stents. Although this validation study demonstrates the promising potential of DMLS and other additive manufacturing methods for fabricating auxetic stents, further optimization of current stent design limitations and the incorporation of post-processing techniques are essential to enhance the reliability of these additive manufacturing processes.