AbstractThe Hartbeesfontein basin is one basin within the Late Archaean rift system of South Africa. This rift system has been recently compared to the Basin and Range province in western North America and may therefore be an ensialic extensional back‐arc basin. Structurally, the Hartbeesfontein basin is a half‐graben structure bounded to the south‐east by a major, normal, listric fault and to the north‐east and south‐west by strike‐slip (transfer?) fault zones. It is infilled by over 2000 m of diamictites, shales, lavas and chemical sediments. Initial basin formation appears to be accompanied by phreatomagmatic volcanic activity caused by the interaction between basic tholeiitic magmas rising along fractures and groundwater. Volcaniclastic debris from these eruptions was incorporated into laharic debris flows and deposited on basin marginal alluvial fans. At the same time a deep, permanent lake formed within the basin in which silts and muds accumulated. Major fissure eruptions of basic, tholeiitic lavas followed, their eruptive centres being apparently located along the strike‐slip (transfer?) fault /ones. Initially, these fissure eruptions had high rates of magma discharge accompanied by intense fire fountaining that resulted in the rapid accumulation of aa type flows. Later lava discharge rates decreased and more quiescent pahoehoe type flows were erupted. Localized centres of acid volcanism within the basic lava pile were located along the south‐western strike‐slip fault zone. These acid volcanic rocks are interpreted as co‐ignimbrite lag breccias and pyroclastic flow deposits and tuffs produced by the repeated formation and collapse of Plinian eruption columns. Towards the top of the basic lava pile, two breaks in volcanism permitted the formation of dolomitic playa lakes. Sedimentation in these lakes was terminated by further basic lava flows. At the top of the basin fill sequence is a thick, bedded chert interpreted as a magadiitic, alkaline playa lake fed by silica‐rich hot springs located along the south‐eastern edge of the basin. Quartzites and conglomerates deposited by braided rivers unconformably overlie the basin‐fill sequence and probably represent a through flowing river system signifying termination of the Hartbeesfontein basin as a separate basin. The Hartbeesfontein basin and its fill demonstrate that a close relationship exists between fissure volcanism, sedimentation and basin evolution and that the strike‐slip, transfer faults acted as the loci of volcanic activity.