Tensile Shear Tests Research Articles

Analysis of aging effects on the mechanical and vibration properties of quasi-isotropic basalt fiber-reinforced polymer composites

Eco-friendly natural fiber composites, such as basalt fiber composites, are gaining traction in material science but remain vulnerable to environmental degradation. This study investigates the mechanical and vibrational properties of quasi-isotropic basalt fiber composites subjected to aging in two different environments: ambient (30 ºC) and subzero (-10 ºC), both in distilled water until moisture saturation. Aged specimens absorbed 8.66% and 5.44% moisture in ambient and subzero conditions, respectively. Mechanical testing revealed significant strength reductions in tensile, flexural, impact, and short beam shear tests, with ambient-aged specimens showing the largest decline (up to 31.7% in flexural strength). Vibrational analysis showed reduced natural frequencies, particularly under ambient conditions (27.27%). Sound absorption tests showed that pristine specimens had the highest transmission loss, while moisture-rich ambient-aged specimens had the lowest. SEM analysis confirmed surface degradation, with fiber pull-out and matrix debonding contributing to property loss. This research provides valuable insights into the environmental limitations of basalt fiber composites, emphasizing the need for enhanced durability in eco-friendly materials.

Physical Heat Cycle Measurement of Resistance Spot Welding

Resistance spot welding (RSW) is still the ideal joining method in the automotive industry. Mostly steel sheets are used in the car body, so overlap and layering are required for welding or riveting, as spot welding provides simultaneous clamping force with interfacial welding to ensure the required strength and quality. A fundamental understanding of heating and cooling rates in thermal distributions is essential for predicting microstructure formation in the weld and the heat-affected zones (HAZ) of RSW joints. The ability to measure the heat cycle in the RSW process can be valuable in weld control and welding parameter optimization. RSW parameters can be optimized through tensile shear tests and microscopic investigations. Heat cycle measurement (HCM) demonstrates the welding consequences in terms of the change in mechanical properties and microstructural formations. The accuracy of cooling rate measurements including t8/5 cooling time is very important to predict the microstructural evolution in the HAZ, however, the thermocouple measurement raises numerous challenges due to the high temperature gradient and small weld and HAZ size. During our investigations heat cycle measurement has been conducted experimentally by a K-type thermocouple. The data logger is connected to the output of the thermocouple for recording the voltage to measure the temperature distributions as a function of both time and position during the welding process. Measurement results of 1 mm thick martensitic MS1400 steel overlapped RSW joints are discussed, and the HCM curve of heating and cooling rates of the spot-welding process is presented. The heat cycle during RSW was measured with two different welding parameter combinations. In addition to welding current, welding time, and electrode force, pulsation has shown disparate curves. Numerous experiments have been attempted to measure the heat cycle in HAZ sub-zones due to the difficulty of positioning the thermocouple accurately, uppercritical HAZ, intercritical HAZ, and subcritical HAZ were investigated and measured in both welding parameter combinations. Difficulties were encountered in the experimental work as a result of the instantaneous welding time and the vibration resulting from the passage of alternating electrical current between the two electrodes. A magnetic field is generated that affects the thermocouple measurement and appears as a noisy curve that is filtered out and smoothed. Joule heat, interfacial heat generation, and cooling effects of electrodes are also considered in the experiment.

Indentation-Free Resistance Spot Welding of SUS301L Stainless Steel

Paint-free bodywork has become an attractive alternative for rail vehicles, in the direction of easy maintainability and low manufacturing costs. However, conventional resistance spot welding inevitably leaves indentation marks to detrimentally reduce the optical homogeneity of the paint-free bodywork. In light of this, indentation-free resistance spot welding is proposed for joining SUS301L stainless steel sheets in order to achieve superior surficial integrity. A tiny SUS301L steel ball with a diameter of 1.5 mm was chosen as the intermediate filler between two steel sheets to avoid the formation of surficial indentation. The influence of welding current and welding time on the mechanical properties of joints was studied. The optimal parameters of the mechanical properties were obtained when the welding current was 8.0 kA, the welding time was 150 ms, the electrode pressure was 0.35 MPa, and the electrodes were cylindrical planar electrodes, which was determined by comparing the tensile shear test results. The surficial indentation depth was less than 1% of the plate thickness, and no observable indentations were seen on the surface of the optimized welding spots.

A Study on the Green Laser Weldability of Copper-aluminum Battery Materials

Copper is widely utilized in electric vehicle batteries due to its excellent electrical conductivity, lightweight, and excellent corrosion resistance. However, copper has a high reflectivity of about 97% for infrared lasers, which makes it difficult to achieve stable welding quality. This study investigated using a green laser to weld nickel-coated copper and aluminum materials. After performing welding by changing the laser power and scan speed, the weld cross-section was observed with an optical microscope, and it was confirmed that the welding penetration depth and bead width increased as the heat input increased. The spatter on the bead surface and defects such as pores and cracks in the weld were caused by excessive heat input. Analysis of the weld cross-section using SEM-EDS showed that high heat input increased the formation of intermetallic compounds including CuAl2 and Cu9Al4. The mechanical properties of the weld were examined using a shear tensile test. The analysis results showed that intermetallic compounds caused brittleness in the weld joint, which lowered mechanical properties and caused defects such as pores and cracks. P60 (1.2 kW, scan speed: 250 mm/s), P80 (1.6 kW, scan speed: 375 mm/s), and P100 (1.2 kW, scan speed: 375 mm/s) were examples of excellent mechanical quality. The fastest welding condition, P100 (power: 2 kW, scan speed: 450 mm/s), was suggested as the most efficient welding condition.

Influence of the material properties on the clinching process and the resulting load-bearing capacity of the joint

This study focuses on the phenomenological change in material strength caused by a specific heat treatment and the subsequent analysis of the influence on the clinching process and the resulting joint properties. For this purpose, three series of tests were performed. In the first series of tests, the influence of heat treatment up to 340 °C on the mechanical properties of an age-hardenable AlMgSi alloy was investigated. Holding time and temperature were varied and the material strength was evaluated by tensile and hardness tests. Two strength-increasing and two strength-reducing heat treatment parameters were identified. In the second series of tests, selected heat treatment parameters were applied to a larger number of specimens and the joint strength was investigated by shear and head tensile tests. In the shear tensile test, mainly the properties of the punch-side material have an influence on the resulting joint strength. A change in strength of the die-side material can be neglected. In contrast, the properties of both sheets are important in the head tensile test. The strength of the joint will only increase if the strength of both sheets is increased. In general, a strength increasing heat treatment resulted in higher joint strength. In the third series of tests, the factor of punch displacement was considered, which was demonstrated to directly influence the formation of the clinched joint geometry.

Improving the joint strength of thermoplastic composites joined by press joining using laser-based surface treatment

Fibre-reinforced thermoplastic composites (TPC) provide an automated and cost-effective solution for their use in lightweight structures in series production. The combination of different material configurations allows the design of highly stress tolerant components. Previous studies demonstrated that the combination of TPC sheets, TPC hollow profiles and injection moulding compounds is even suitable for crash-relevant automotive parts. All three components are combined during the injection moulding process. To prevent collapse, the part must remain in a consolidated state and cannot be preheated. However, this results in poor adhesion between the hollow profile, the bulk material, and the TPC sheet. Previous studies have shown that the bonding strength between the hollow profile and the injection moulding compound can be increased by surface pre-treatment using laser structuring and plasma technology. In this work, laser structuring is employed to enhance the bonding strength between the hollow profile and the TPC sheet. Microscopy analysis is used to investigate the resulting surface morphology. Subsequently, single-lap-shear (SLS) specimens are produced by pressing the TPC sheets onto the flat part. The resulting bonding strengths are then evaluated by tensile shear tests. The study analyses the impact of various pre-treatment parameters on the bonding strength. Furthermore, it investigates the effect of sheet temperature on the bonding strength, including specimens without pre-treatment. Finally, the results of the surface treatment of hollow composite profiles are discussed.

Impact of graphene oxide lateral sizes on the mechanical and thermal properties of carbon fiber composites

AbstractThe impact of carbon fiber (CF) composites sizing with graphene oxide (GO) to form brick‐and‐mortar structures on their mechanical properties and thermal conductivity has not been closely examined. This study systematically investigates the effect of GO sheet size on the interfacial properties and thermal conductivity of CF composites. Three sizes of GO—small (0.11 μm), medium (0.33 μm), and large (0.97 μm)—were used to modify CF surfaces via layer‐by‐layer self‐assembly, forming the brick‐and‐mortar structures. The mechanical properties were assessed through flexural tests, interlaminar shear strength (ILSS) tests and tensile tests, while thermal conductivity was measured using a thermal constant analyzer. The results revealed that medium‐sized GO (GO‐M) significantly enhanced the interfacial strength and toughness of the composites. This improvement is attributed to the orderly arrangement of GO‐M on the CF surface, which enhances stress transfer between the fiber and the matrix. In contrast, small‐sized GO (GO‐S) tended to scatter, resulting in less effective reinforcement, while large‐sized GO (GO‐L) exhibited stacking and agglomeration, limiting its reinforcement effectiveness. However, GO‐L provided the highest thermal conductivity due to the formation of continuous heat conduction pathways. These findings suggest that GO‐M offers a balanced improvement in mechanical properties, whereas GO‐L is more suitable for applications requiring high thermal conductivity. This work underscores the importance of selecting the appropriate GO sheet size to optimize the interfacial properties and thermal conductivity of CF composites, which is crucial for enhancing their performance in high‐end engineering applications, such as aerospace, automotive, and marine industries.Highlights Modification of CF composites by GO‐M sheets significantly improved toughness and strength. GO‐L sheets formed an effective heat transfer channel with the highest thermal conductivity. The study emphasized the critical role of selecting the appropriate GO sheet size to optimize the mechanical and thermal properties of CF composites.

Mechanical Performance on Flax Fibre Epoxy Composites Filled with Montmorillonite Nanoclay for Lightweight Applications

The objective of this study is to investigate the mechanical performance on develop flax/epoxy composite filled with montmorillonite nanoclay for lightweight applications. For this purpose, firstly, nanoclay at different weight percentages montmorillonite nanoclay such as 0.5, 1, 1.5 was dispersed homogeneously into epoxy resin with the help of ultrasanitization process. For better nanoclay distribution in composite, the montmorillonite nanoclay concentration higher than 1.5% was not analyzed. Secondly, using this mixture, flax fiber based composites were produced by vacuum bag molding process. Finally, the mechanical properties of flax/epoxy composites filled with different percentages montmorillonite nanoclay were determined with tensile, flexural, and in-plane shear test. From the experimental results obtained, the addition of montmorillonite nanoclay indicate positive effect on the performance of the composites compared with the neat composite samples, if the montmorillonite nanoclay distribute homogeneously in the epoxy. The composites added with 0.5 wt.% nanoclay showed the highest tensile modulus and tensile strength. Moreever, the elasticity modulus of composite samples with 0.5% nanoclay addition is approximately 87% higher than the pure composite. Also, the composite samples loaded with 1.5 wt.% of montmorillonite nanoclay performs better under flexural loading conditions.

Dissimilar joining of aluminum alloy and low-alloy carbon steel by resistance spot welding

In this work, the resistance spot welding (RSW) process was performed to join aluminum alloy and low-alloy carbon steel plates. The macro characteristics including nugget diameters and indentation rates, microstructure and tensile-shear strength of RSW joints were investigated. The results showed that the nugget of the RSW joints comprises a ‘bowl’ shape nugget on the aluminum side and an elliptical shape nugget on the steel side. Also, the intermetallic compound (IMC) layers containing Fe4Al13 and Fe2Al5 were formed around the aluminum/steel interface with the steel side having a tongue-shape and the aluminum side having a needle-shape. According to metallurgical evaluation and temperature distribution of RSW joints analyzed by the finite element method, the nugget on the aluminum side contained the dendritic grains and equiaxed dendritic grains. The nugget on the steel side consisted of a large amount of bainite and a small amount of coarse lath martensite. The nugget diameters and the indentations rates of RSW joints increased when increasing either welding current or welding time, and decreased when increasing the electrode pressure. The maximum values of nugget diameter and indentation rate of RSW joints were 9.076 mm and 4.144% when using the welding current of 16 kA, welding time of 450 ms and electrode force of 3 kN. In tensile-shear tests, the RSW joints showed a shear-off fracture mode. When increasing the welding current, welding time or electrode force, the tensile-shear strength of RSW joints increased first, and then reached a maximum, and finally decreased. The welding current of 16 kA, the welding time of 300 ms, and the electrode pressure of 3 kN were considered as the optimal welding parameters in the present study which resulted in the maximum tensile-shear strength of 2.24 kN. In addition, the IMC layers of the RSW joints exhibited a uniform and continuous appearance with a thickness of approximately 1.9 μm, and the IMC layer in the central area was thicker than that in the edge area.

Feasibility study of carbon-fiber reinforced polymer linerless pressure vessel tank

Composite pressure vessels are used in aerospace engineering for storing fluids such as propellants, nitrogen, and oxygen. They are also used in life-support systems, High-performance pressure suits for astronauts, Helium Tanks for Balloons and Airships. Among many types of composites, Carbon fiber composites uses have been increasing due to its high strength to weight ratio, high thermal expansion, corrosion, fatigue and impact resistance and design flexibility. In order to improve the volume of the pressure vessel, the liner-less concept is tried. This increased volume efficiency is crucial in aerospace applications where space is at a premium and maximizing storage capacity within limited dimensions is important. Not only the volume efficiency, but also the Reduced Permeability Concerns, Enhanced Durability and Longevity, better thermal continuity and simplified manufacturing process make this research significant in the area of pressure vessel. This research paper deals with the fabrication and development of a cylinder without a lining. The test sample was subjected to several tests: tensile test, impact, shear test (3P Bending), leak test and Pressure test. The test sample was capable of withstanding 20 Bars without failure. The numerical results were also performed and compared with the experimental results. The difference was only 3%. Unsymmetrical dimethyl hydrazine (UDMH) AND red-fuming nitric acid can both be stored in this cylinder (RFNA). Unlike traditional composite overwrapped pressure vessels, the liner-less composite tanks rely completely on the composite shell to act as a permeation barrier as well as handling all pressure and environmental loads. The absence of a liner eliminates the potential for delamination or failure at the interface between the liner and the composite material.

Effect of High Fiber Content on Properties and Performance of CFRTP Composites

Continuously reinforced thermoplastic composites are widely used in structural applications due to their toughness, light weight, and shorter process cycle. Moreover, they provide flexibility in design and material selection. Unlike thermoset composites, continuous fiber content to maximize mechanical properties in thermoplastic composites has not been well investigated. In this paper, three thermoplastic systems are investigated to study the optimum content of continuous fiber reinforcement. These systems include carbon fiber/polyphenylene sulfide (PPS), glass fiber/PPS, and glass fiber/high-density polyethylene (HDPE). Tapes were made at several fiber contents, and samples were compression molded and tested using thermo-gravimetric analysis (TGA), differential scanning calorimetry (DSC), dynamic mechanical analysis (DMA), tensile, 3-point flexure, and short-beam shear tests. Results revealed that higher fiber content led to an increase in the glass transition and melt transition temperatures of the polymer. Some mechanical properties increased with fiber content and then began to decrease upon further addition of fibers, while other properties, such as ductility and interfacial bond strength, decreased with more reinforcement. Furthermore, the optimum fiber contents to maximize mechanical properties are different for different properties and different materials.

Study on the preparation and mechanical behavior of carbon fiber reinforced aluminum matrix composites stator blade

The advancement of high-performance stator blades stands as a critical avenue for enhancing the efficacy of aero engines. This study aims to prepare carbon fiber reinforced aluminum matrix (CF/Al) composite stator blades with high-quality shapes and properties, optimize the lay-up design using Fibersim software, and investigate the effect of extrusion temperature on the forming quality. The mechanical properties and damage behavior were systematically analyzed by tensile, compression, and interlaminar shear tests. In addition, the vibration mode simulation reveals the force state under the 1st to 8th-order vibration modes. Results indicate that the [0°/+45°/0°/-45°/90°/-45°/0°/+45°/0°] lay-up parameters were optimal, achieving excellent shape and performance of curved preforms after curing. Composite blades fabricated at an extrusion temperature of 680°C exhibited clear contours, consistent dimensions, and no macro defects. SEM and EDS analyses showed uniform impregnation in all regions of the blade, high density, and good densification. Compared with the matrix alloy, the tensile strength of the composite blade was improved by 64.94%, the compressive strength by 35.7%, and the interlayer shear strength was as low as 72.6 MPa. The vibration mode simulation verified the applicability of the blade in the first-order vibration mode, which provides strong support for the application of composite materials in the aerospace field.

Effects of Tool Geometry Parameters on Clinched Joint Strength Using FEM

Abstract Clinching joining is one of the predominant techniques used to join aluminium alloys in the automotive industry. Although the technique can be easily automated, cost-effective, and not affect the material’s mechanical properties during the joining process, the tool geometry parameters significantly affect the strength of the clinched joint. Therefore, a precise finite element model is critical to improve the strength and reduce the cliched joint’s production cost. This study investigated the effect of the punch fillet radius, the punch angle, the die diameter and the die depth on the strength of the clinched joint of 5754 aluminium alloys. The clinched joint was produced with different geometry parameters. The cross-section of the clinched joints was observed. In the meantime, the interlocking value, the neck thickness, and tool parameters were measured to investigate the joinability of the aluminium alloys. The static tensile shear tests were also conducted using the universal tensile machine. Numerical studies have been conducted to analyse the influence of the geometrical parameters using a 2D axisymmetric model. As a result, the numerical results agreed with the experimental results. Additionally, the result showed that the tool geometry significantly impacted the strength of the clinched joint of aluminium alloys. The study concluded that the neck thickness and the interlocking value have played a vital role in the enhancement of the cliched joint strength.

Experimental behavior and fracture prediction of a novel high-strength and high-toughness steel subjected to tension and shear loading tests

In this study, laboratory testing and numerical simulation methods are used to investigate the mechanical behavior and perform fracture prediction of a novel high-strength and high-toughness steel with a negative Poisson's ratio (NPR) effect under combined tensile-shear loading conditions. A test device capable of meeting different tensile-shear combination test angles is designed and manufactured, wherein the mechanical experiments on the NPR (Negative Poisson's Ratio) steel specimens are carried out at various testing angles. Q235 steel and MG400 steel are used as experimental control groups. The results show that the mechanical deformation of NPR steel is significantly better than that of Q235 steel and MG400 steel. Its tensile-shear test curve has no yield plateau and it has quasi-ideal elastic-plastic mechanical properties. The loading direction gradually changes from tension-dominated to shear-dominated as the tension-shear angle increases, and the strength and deformation of the specimens show a decreasing trend. Based on the laboratory test results, a finite element numerical model of NPR steel is established. A series of numerical simulations are carried out under the conditions of different tension and shear angles and the average stress triaxiality and fracture strain data are obtained. The fracture data of NPR steel are fitted using the Johnson-Cook fracture criterion, and the Johnson-Cook fracture parameters under the tensile-shear test conditions of NPR steel are thus obtained. The numerical simulation verifies that the fracture model can accurately predict the tensile-shear fracture behavior of NPR steel.

Microstructure and mechanical properties of similar and dissimilar resistance spot welded DC04 and HRP6222 (DD11) steels

Abstract Low carbon steels are frequently preferred in the automotive industry. The most preferred welding method in vehicle body manufacturing is resistance spot welding (RSW). In this study, RSW joints of DC04 and HRP6222 steels were carried out at two different electrode forces (2.1 kN, 2.4 kN) and three different welding currents (4 kA, 6 kA, 8 kA). The effects of different welding parameters on microstructure, tensile shear force, failure mode and microhardness were investigated. So, the focus was on optimizing the welding parameters. As a result, the RSW process caused the formation of three different regions in the microstructure (the base metal, the heat affected zone and the weld metal). It was observed that the tensile shear force increased as the welding current and electrode force increased. After the tensile shear tests, two different failure modes occurred (interface and pull-out type). Hardness values showed a linear relationship with tensile shear force results. In addition, a significant increase in hardness values was observed from the base metal to the weld metal in all welding parameters.

Explosively welded SLM-AlSi10Mg/SLM-SUS316L: Unveiling superiority of interlayer welding for enhanced mechanical properties

Following the advent of three-dimensional (3D) printing technology, multi-material 3D printing has garnered significant attention due to its potential to enhance the flexibility and development of high-performance 3D printing materials. This study investigated the application of explosive welding to create multi-material 3D printed structures. Specifically, we explored the use of direct and interlayer explosive welding to fabricate SLM-AlSi10Mg/SLM-SUS316L explosive composites with the aim of further improving material properties. Our primary objective was to explore the unique interfaces and mechanical characteristics of 3D printed materials subjected to explosive impact loading. This study provides a new idea of 3D printing multi-materials, which is of great significance for the development of both explosive welding and 3D printing. The results demonstrated the feasibility of using explosive welding to create multi-material composites from 3D printed metals, including both direct and interlayer welding of SLM-AlSi10Mg/SLM-SUS316L. Interlayer welding exhibited superior mechanical performance compared to direct welding, with a 70%–250% increase in strength observed in the macro tensile shear test. Additionally, samples fabricated with a 40 mm explosive thickness displayed more stable and exceptional performance in the micro tensile test. Corrosion testing and X-ray computed tomography (XCT) analysis were employed to investigate the distribution of pores within the 3D printed materials.

Influence of the Composition of Provisional Luting Materials on the Bond Strength of Temporary Single-Tooth Crowns on Titanium Abutments.

In addition to zinc oxide-based cements, resin-based materials are also available for temporary cementation. The aim of this in vitro study was to determine the influence of the different material compositions on temporary bonds. In nine test series (n = 30), temporary bis-acrylate single-tooth crowns were bonded onto prefabricated titanium abutments with nine different temporary luting materials. After simulating an initial (24 h, distilled water, 37 °C), a short-term (7 days, distilled water, 37 °C) and a long-term provisional restoration period (12h, distilled water, 37 °C; thermocycling: 5000 cycles) in subgroups (n = 10), the bond strength was examined using a combined tensile-shear test. Statistical analysis was performed by univariate analysis of variance or a non-parametric Kruskal-Wallis test, followed by post hoc tests. Of the three resin-based materials, two showed significantly higher bond strength values compared to all other materials (p < 0.001), regardless of the storage procedure. The resin-based materials were followed by eugenol-free and eugenol-containing zinc oxide materials. Significant intragroup differences were observed between the composite-based materials after all storage periods. This was only observed for some of the zinc oxide-based materials. The results show that under in vitro conditions, not only the composition of the temporary luting materials but also the different storage conditions have a significant influence on temporary bonds.

Insights into the microstructural evolution and strengthening mechanisms of friction stir spot welded advanced high strength ultrafine bainitic steel

Unlocking the full potential of advanced high-strength bainitic steels in spot-welding is a pivotal endeavor for harnessing their extraordinary mechanical properties in the automotive industry. This study suggests a shift in paradigm to address the inferior fusion weldability of this type of steel because of the formation of coarse martensite within the welded zone of weldments obtained by liquid-state welding, through the strategy of refining the martensite within the weld zone using the solid-state friction stir spot welding (FSSW) process. This paper delves into an in-depth investigation of the microstructural evolution and load-bearing capacity of a Fe-0.25C-3Cr-1.63Mn-1.5Si (wt%) ultrafine bainitic steel, having a remarkable tensile strength of 1.7 GPa, during the intriguing process of FSSW at rotational speeds of 600 to 2000 rpm. The research uncovers that the stir zone (SZ) undergoes dynamic recrystallization, resulting in a significantly refined microstructure. Regardless of the rotational speed employed, the high hardenability of the steel and rapid cooling during the process inevitably results in martensite formation within this region. However, a comprehensive microstructural characterization conducted by the electron backscatter diffraction (EBSD) analysis proves that the different thermal cycles induced by different rotational speeds lead into various prior austenite grain sizes, martensitic/bainitic packets and blocks attributes, and density of high-angle grain boundaries (HAGBs). Through the evaluation of strengthening mechanisms in different weld zones, the study sheds light on the key factors influencing strength. Block boundaries emerge as the primary contributor to SZ hardening, surpassing the role of geometrically necessary dislocations (GNDs) and solid solution strengthening. The load-bearing capacity observed during the tensile-shear test is governed by a delicate interplay between bonding width and crystallographic features (block size and HAGBs density) of the martensite formed within the SZ. The highest peak load was achieved under optimal welding conditions (rotational speed of 1000 rpm), which enabled the production of a sufficiently large bonding width, providing ample bonding area for load-bearing, along with an abundance of blocks and HAGBs to effectively impeding crack propagation.

Laser-induced surface reconstruction to enhance interfacial bonding reliability of CFRP/titanium hybrid joints

Adhesive bonding is widely used in aeronautical carbon fiber-reinforced polymer (CFRP)/titanium (Ti) alloy hybrid structures to satisfy the demands of high-strength and lightweight. The physicochemical properties of adherend surfaces significantly impact the bonding performance. In this study, laser-induced surface reconstruction (LISR) was designed for the reliable joining of Ti alloy and CFRP. A three-level-three-factor central composite design (CCD) approach-based response surface methodology (RSM) analysis was applied to statistically specify parameter optimization of the laser energy output. Surface morphology and wettability of CFRP ablated were studied. Chemical compositions were determined by X-ray photoelectron spectroscopy (XPS). Tensile-shear tests were performed, and fractured surfaces were analyzed. The tensile shear strength with LISR process has been improved by 19.1%, in comparison with that of mechanical grinding treatment. The cross-like texture based on designed geometric configuration was fabricated without damaging the underlying fibers, thus increasing the surface roughness and contact area at interface. The wettability transition mechanism was investigated, demonstrating that the hydrophilicity of reconstructed surfaces primarily attributes to the more polar groups (C–O, CO, etc.) on CF surfaces. This study provides a reliable surface treatment method for fabricating high-performance composite structures by adhesive bonding.

Experimental Study on the Mechanical Properties of Nano-Silicon-Modified Polyurethane Crack Repair Materials

This study aims to solve the problem of dynamic crack repair in concrete. Although conventional polyurethane has good strength, its tensile and shear properties are poor. It was found that nano-silicon had an overall enhancing effect on the mechanical properties of polyurethane; therefore, five sets of tests with different dosages (0%, 2%, 5%, 7.5%, and 10%) were designed. The compressive, tensile, and shear mechanical properties of nano-silicon-modified polyurethanes were tested by compression, tensile, and straight shear tests, and the microscopic appearance of the materials was observed by scanning electron microscopy. The results showed that nano-silicon could enhance the mechanical properties of polyurethane. The best filling effect on polyurethane was achieved at a dosage of 5%, which increased the compressive, tensile, and shear strengths by 29.4%, 257.6%, and 202.1%, respectively, compared with the substrate. The compressive and tensile moduli in the small strain range were enhanced by 268.5% and 511.8%, respectively. After exceeding 5%, the mechanical properties of the materials decreased due to the enhanced nanoparticle agglomeration effect, which led to the appearance of voids inside the materials. The comprehensive analysis shows that nano-silicon can better enhance the mechanical properties of polyurethane with an optimal dosage of 5%, which is stronger relative to other repair materials and does not require time maintenance.