Temperature Gas Flow Research Articles

Core‐Shell Catalyst Pellets for CO2 Methanation in a Pilot‐Scale Fixed‐Bed Reactor

AbstractPower‐to‐methane (PtM) offers an efficient opportunity for surplus renewable energy storage, but heat management is a major challenge for conducting the highly exothermic methanation reaction. To address this challenge, this study presents the first successful demonstration of core‐shell catalyst pellets in a pilot‐scale reactor for CO2 methanation. Experiments in a wall‐cooled fixed‐bed reactor are conducted with diluted and undiluted reactant feed under systematic variation of cooling temperature and inlet gas flow rate. The results show that core‐shell catalyst pellets significantly reduce the hot‐spot temperature while maintaining comparable reactant conversions to uncoated catalyst pellets at the same conditions. Additionally, core‐shell catalyst pellets allow for undiluted reactant feed at comparably low hot‐spot temperatures (approx. 600 °C).

Synthesis and Characterization of Boron Nitride Thin Films Deposited by High-Power Impulse Reactive Magnetron Sputtering

In the present research, hexagonal boron nitride (h-BN) films were deposited by reactive high-power impulse magnetron sputtering (HiPIMS) of the pure boron target. Nitrogen was used as both a sputtering gas and a reactive gas. It was shown that, using only nitrogen gas, hexagonal-boron-phase thin films were synthesized successfully. The deposition temperature, time, and nitrogen gas flow effects were studied. It was found that an increase in deposition temperature resulted in hydrogen desorption, less intensive hydrogen-bond-related luminescence features in the Raman spectra of the films, and increased h-BN crystallite size. Increases in deposition time affect crystallites, which form larger conglomerates, with size decreases. The conglomerates’ size and surface roughness increase with increases in both time and temperature. An increase in the nitrogen flow was beneficial for a significant reduction in the carbon amount in the h-BN films and the appearance of the h-BN-related features in the lateral force microscopy images.

Experimental study on surface temperature and emissivity of rotating turbine blades of a micro turbojet engine

The temperature of the rotating turbine blades of a turbojet engine must be known to assess the combustion state and improve turbine blade quality. Obtaining online temperature measurements of high-speed rotating turbine blades in high-temperature gas flow remains challenging. A multispectral radiation thermometry method without emissivity assumption is proposed to measure the temperature of high-speed rotating turbine blades of a micro turbojet engine. The relative radiative intensity is calculated by accounting for smooth changes in the wavelength using the moving narrowband method to determine the influence of emissivity on multispectral radiation thermometry results. The method’s performance in measuring the surface temperature of high-speed rotating objects is tested. The wavelength range of 970 nm to 1700 nm is selected because the radiation from gases is weaker in comparison to the radiation emitted by solid surfaces within this band. The spectral radiation of the turbine blade surface is measured at three rotational speeds: 38,000 r/min, 48,000 r/min, and 58,000 r/min. The results show that, unlike thermocouples that measure the temperature of the hot gas flow near the blade, multispectral radiation thermometry provides the average surface temperature with high consistency (with a deviation smaller than 50 K). Multispectral radiation thermometry can be applied to measure the surface temperature and emissivity of high-speed rotating objects, such as the blades of turbojet engines.

Thermal Stability and Purity of Graphene and Carbon Nanotubes: Key Parameters for Their Thermogravimetric Analysis (TGA).

Thermal analysis is widely employed for the characterization of nanomaterials. It encompasses a variety of techniques that allow the evaluation of the physicochemical properties of a material by monitoring its response under controlled temperature. In the case of carbon nanomaterials, such as carbon nanotubes and graphene derivatives, thermogravimetric analysis (TGA) is particularly useful to determine the quality and stability of the sample, the presence of impurities and the degree of functionalization or doping after post-synthesis treatments. Furthermore, TGA is widely used to evaluate the thermal stability against oxidation by air, which can be, for instance, enhanced by the purification of the material and by nitrogen doping, finding application in areas where a retarded combustion of the material is required. Herein, we have evaluated key parameters that play a role in the data obtained from TGA, namely, gas flow rate, sample weight and temperature rate, used during the analysis. We found out that the heating rate played the major role in the process of combustion in the presence of air, inducing an increase in the temperature at which the oxidation of CNTs starts to occur, up to ca. 100 °C (from 1 °C min-1 to 50 °C min-1). The same trend was observed for all the evaluated systems, namely N-doped CNTs, graphene produced by mechanical exfoliation and N-doped reduced graphene samples. Other aspects, like the presence of impurities or structural defects in the evaluated samples, were analyzed by TGA, highlighting the versatility and usefulness of the technique to provide information of structural aspects and properties of carbon materials. Finally, a set of TGA parameters are recommended for the analysis of carbon nanomaterials to obtain reliable data.

Dehydration by Pervaporation of an Organic Solution for the Direct Synthesis of Diethyl Carbonate

Pervaporation has been a central subject in the research community within the scope of the further development of energy- and cost-efficient alternatives to conventional liquid–liquid separation technologies. The potential eligibility of four commercial membranes (ZEBREX ZX0, PERVAPTM 4155-80, PERVAPTM 4100, PERVAPTM 4101) for use in an integrated dehydration application of a diethyl carbonate/water/ethanol mixture by pervaporation was assessed experimentally. The impact of feed concentration, operating temperature, pressure, and sweep gas flow rate on membrane separation performance, including permeation flux, permeate quality, selectivity, and permeance, was thoroughly investigated. Applying the ZX0 membrane delivered the best qualities of all tested membranes of the permeate stream, with a water concentration of mostly >98%. In comparing the water flux, the ZX0 membrane remained reasonably competitive with the polymer membranes. Furthermore, the sweep gas volume flow rate and the operating temperature were identified as influencing the flux significantly but not the product composition. At the same time, the feed concentration of water also influenced the water purity within the permeate. The experiments were monitored with a partial least squares model, allowing a quick assessment of obtained samples while delivering accurate results.

SEMI-BATCH EXPERIMENTAL STUDY ON MULTIPLE CARBON DIOXIDE BUBBLES ABSORPTION IN SWEETENER SOLUTION UNDER VARYING PRESSURES

Increasing the absorbed carbon dioxide amount in sweetener solution is a new trend to modify soft drinks. This research investigated the optimum increase in absorbed carbon dioxide within the limits of permissible food specifications in the bubble column. Response surface methodology (RSM) utilizing the Box Behnken design (BBD) was used to conduct experiments operating conditions for achieving desired responses within specified ranges of pressure (2-4 bar), temperature (5-25°C), gas flow rate (0.2–0.4 L/min), and absorbent concentration (0–150 g/L). The experimentally obtained results were fitted to a second-order polynomial model—the increase in pressure and gas flow rate results in an increase in absorption yield (YCO2). Also, increasing the gas flow rate and temperature will increase the volumetric mass transfer coefficient (KLa), while, at high pressure and pore size KLa will be reduced. According to the obtained results at optimum conditions, 4 bar, 5°C, gas flow rate 0.4 L/min, sucrose concentration of 0 g/L, and pore diffuser 0.5 μm; The CO2 content (YCO2) was 8.34 g/L. The optimum conditions for combining the effect of high CO2 content (6.125 g/L) and best KLa value (0.1043 L/min) were: 2.83 bar, 5 °C, a gas flow rate of 0.4 L/min, a sucrose concentration of 65.15 g/L, and pore diffuser of 0.5 μm.

CFD Modelling and Optimization of Solid Waste Combustion in a 1 MW Fixed Bed Combustion Chamber

The global population and energy consumption grow each year. Therefore, the tendency to use biofuels instead of fossil fuels assist the global requirement. Also, enhancing of the combustion efficiency and minimizing pollutant emissions during the combustion of municipal solid waste (MSW). The present study employed a CFD model to simulate solid fuel combustion in a grate combustion chamber which was commonly used in small-capacity boilers. computational fluid dynamics technique was used to simulate complex solid fuel reactions where 1 MW boiler was supposed for wood and coal combustion. The achievements found that 10%-dried MSW was used as fuel. The results of the study were related to the average gas flow temperatures and composition in the furnace outflow section, as well as the high combustion temperatures of fossil fuels. The results for the average temperature and average chemical molecular fractions (CO, O2, CO2, H2O, and N2) generated at the exit of the combustion process were positive. Thus, it was found that the thermal efficiency of the boiler was significantly affected by the amount of air supplied to the system at a temperature of 273 K and atmospheric pressure. We observed variations in flame morphology, temperature profiles, and corresponding numerical values.

Assessment of Flavor Compounds in Blended Malt Whisky Aged with Acacia, Cedar and Oak Wood Using Liquid Chromatography Hyphenated to Electrospray Ionization and Tandem Mass Spectrometry (LC-ESI-MS/MS)

Selected flavor compounds from wood were quantified, with liquid chromatography hyphenated to electrospray ionization and tandem mass spectrometry (LC-ESI-MS/MS), in four samples of base spirit matured with acacia, cedar, virgin oak, and used port wine oak wood cubes and the results were used to describe and differentiate their different wood congener profiles. ESI-MS/MS parameters were optimized in terms of capillary voltage, cone- and desolvation gas flow, source- and desolvation temperature, cone voltage, and collision energy. The method was validated in terms of linearity (R2 > 0.995), limit of detection, limit of quantification, recovery, and repeatability. One-way analysis of variance (ANOVA) showed that for most compounds there were no significant differences (α = 0.05) between seven to 30 days of aging plus a heat treatment at 40 °C, but wood type did significantly influence the wood congener profile. Principal component analysis discriminated the spirits based on relative amounts of wood congeners extracted, and the chemical profile. Aging with cedar wood led to a less pronounced chemical profile, not very distinct from the base spirit. Aging with acacia and virgin oak wood produced a second chemical profile with relatively higher levels of synapaldehyde, syringaldehyde, scopoletin, and coniferyl aldehyde. Aging with port oak wood produced a third chemical profile with relatively higher levels of 5-HMF, gallic acid, furfural, vanillic acid, and syringic acid.

Dielectric barrier discharge plasma for chlorobenzene removal: Performance optimization, process modeling, and toxicity evaluation

Bio-purification has been recognized as an effective method of removal of volatile organic pollutants (VOCs), yet exist a technical bottleneck of low removal efficiency in the treatment of high toxicity and low water-soluble VOCs, especially chlorobenzene (CB). Herein, dielectric barrier discharge (DBD) technology was used as a pre-treatment technology, and the effect of process parameters (specific input of energy (SIE), inlet concentration of CB, humidity, and discharge length) of DBD on the removal performance of CB was analyzed, in order to investigate the feasibility of DBD as a pre-treatment approach for bio-purification. Taking energy yield, by-product analysis and exhaust evaluation as considerations, an SIE of 1,131.57 J·L-1, an inlet CB concentration of 300 ppm, a humidity of 50 %, and a discharge length of 10 cm were selected as the most suitable experimental conditions for the air DBD reactor. The temperature of gas flow was analyzed. Results suggested that DBD have no adverse thermal effect on the subsequent biotechnology (decreased by about 8 K during the discharge process). The temperature change caused by the degradation of CB (e.g., phenyl ring-opening and other processes) accounts for about 90 % of the total temperature change, where remaining part of temperature decreased caused by the large number of active substances produced by electron excitation, collision and cracking during discharge. The regulation of short-life active substances (e.g., ·NO, ·NO2,·OH, and O2–·) further reduced the toxicity of the outlet gas generated by DBD through affect the contents the long-life active substances (e.g., H2O2, and O3). This study provides a better understanding of the feasibility of DBD as a treatment for bio-purification and a new coupling technology for the effective removal of CB.

粮食干燥机自吸式热风变温装置设计与试验验证

During the grain drying process, in order to adjust the temperature, it is necessary to match the proportion of hot and cold air. This is the problem that the two components in the mixed gas cannot fully mix with each other in a short period of time, resulting in the problem that it takes a long time for the gas flow temperature to reach a stable value. Based on the process and technical requirements of the dryer, a self-priming hot air temperature changing device suitable for the dryer was designed. The two gas components used to improve the variable temperature ratio of the dryer are fully mixed with each other in a short time and a short distance, thereby reducing the loss caused by the food not reaching safe moisture. Based on Bernoulli's principle and the basic theory of airflow mixing in fluid dynamics, a mathematical model of airflow mixing in the constriction section of the main pipeline was established. Fluent was used to numerically simulate the distribution of uniform mixing distance and temperature field in the necking section. The results show that the mixing uniformity in the necking section reaches 75%-80%, which effectively improves the mixing efficiency. A self-priming hot air temperature change device test bench developed independently was used, and the quadratic orthogonal rotation combined test method was used for parameter optimization. Design-Expert.V8.0.6.1 was used for analysis and testing, and the regression equation and response surface were obtained to analyze the effects. Interaction between factors to determine the best combination of optimization parameters: when the number of air inlet pipes is 3.16, the incision axial angle is 27.6°, the temperature difference is 43.5°C, and the pipe diameter is 23.8mm, the post-mixing temperature is 50.93°C, and the mixing distance is uniform is 39.33mm. The test results are consistent with the optimization results. The self-priming hot air temperature changing device of the dryer has certain practical application value.

The catalytic deoxygenation reaction temperature and N2 gas flow rate influence the conversion of soybean fatty acids into Green Diesel

BackgroundGreen diesel is a promising alternative as a petroleum replacement given the worldwide demand for petroleum fuel. Environmental issues have drawn public attention and concerns towards advancing renewable energy development. A catalytic deoxygenation (deCOx) was carried out to produce green diesel from soybean oil (SO) using a low-cost NiO-doped calcined dolomite (NiOCD) catalyst. MethodThe structure, chemical composition and morphology of NiOCD were comprehensively characterized by XRF, BET, TPD-CO2, SEM and TEM. In this study, the effect of two operating parameters, reaction temperature and flow rate of nitrogen, was discovered using a one-factor-at-a-time (OFAT) optimisation study. In addition, the life cycle cost analysis (LCCA) of stepwise catalyst preparation and green diesel production has been performed. Significant findingsAn optimal reaction temperature of 420 °C was found to provide the highest yield of green diesel (47.13 wt.%) with an 83.51% hydrocarbon composition. The ideal nitrogen flow rate, however, was found to be 50 cm3/min, which produced 41.80 wt.% of green diesel with an 88.63% hydrocarbon composition. The deoxygenation reaction was significantly impacted by both reaction temperature and nitrogen flow rate. According to LCCA, NiOCD catalyst has potential to lower the overall cost of producing green diesel compared to commercial zeolite catalysts.

Thermal runaway front propagation characteristics, modeling and judging criteria for multi-jelly roll prismatic lithium-ion battery applications

Large-format prismatic Li-ion batteries (LIBs) are prominent energy storage devices in electric transportation applications. However, large-format LIB induces severe thermal runaway (TR) disasters. Battery failure commonly initiates from a local point of one jelly roll and then propagates to the whole cell, called thermal runaway front (TRF) propagation. This study investigates the TRF propagation mechanism of multi-jelly roll-based LIBs through experiments, modeling, and theoretical analysis for thermal runaway propagation (TRP) mitigation. Experiments prove that battery venting changes along the jelly roll-safety valve directions during the TRF boundary movement. Besides, TRF propagation speed is found to be accelerated inside each cell (from 3.6 to 10.6 mm/s) during TRP, driven by a significant temperature gradient, chemical reactions, and gas flow along the TRP direction. The in-cell TRF acceleration behavior is more noticeable for batteries with more jelly rolls. The TRF speed-jelly roll index equations are proposed to reveal the propagation acceleration principle mathematically. Furthermore, a thermal-physical model is developed to precisely simulate in-cell TRF propagation behavior, which is validated by experimental data. Moreover, the TRF boundary temperature equation and “No TRP” judging criteria are proposed through theoretical analysis. This study proposes promising strategies for potential TRP suppression, contributing to future safe battery system design.

Synthesis of nano-silicon carbide by SiO–C reaction

Carbon black has been successfully converted into silicon carbide by reacting it with SiO vapor at 1500 °C under Ar gas environment. The influence of reaction temperature, duration and Ar gas flow rate on the final product was examined. The structural and microstructural property of synthesized SiC was characterized using X-ray diffraction (XRD), Raman spectroscopy and scanning electron microscopy (SEM). Micrographs of synthesized SiC showed that the final product was an agglomeration of SiC nano-powder of 50–500 nm size and nano-whiskers/fibres having a diameter of 50–500 nm and lengths in 0.1–10 μm depending on Ar gas flow rate. The higher conversion of C into SiC was observed at 1500 °C with Ar gas flow rate ∼250 ml/min.

Numerical simulation of the effect of coaxial and cross-axis injection modes on pulverized coal combustion in the raceway of blast furnace tuyere

The aim of this study is to investigate the influence of the angle of the pulverized coal (PC) injection lance on the combustion characteristics of fuel in the raceway of blast furnace tuyeres. Using FLUENT software, a Euler-Lagrange three-dimensional numerical model was constructed to analyze the influence of different positions of blast furnace tuyere coal powder injection lance (coaxial and cross-axis) on key parameters such as temperature distribution, gas flow, and combustion efficiency. The results demonstrate that adjusting the angle of the injection lance significantly modifies the average and peak temperatures in the raceway, while the composition of gas components remains relatively stable. When the injection lance angle is 10°, the average temperature and peak temperature in the raceway are 2294 K and 2747 K, respectively. When the injection lance angle is 12°, the combustion efficiency of the PC reaches 80.8%. This study reveals the significant impact of the injection lance angle on the combustion process. Especially at an angle of 12°, the combustion efficiency of the blast furnace significantly improves. With coaxial injection, the combustion rate increases as the distance between the injection lance tip and the tuyere increases. This paper is instructive for the optimization of the blast furnace combustion system, which improve fuel utilization efficiency and reduce environmental emissions. This paper provides practical recommendations for adjusting blast furnace operational parameters, offering insights for achieving more efficient and environmentally friendly industrial production.

Optimization of brazing parameters for 316L stainless steel with AgCuZn filler metal under argon atmosphere

This research studies the optimal parameters for brazing 316L stainless steel using AgCuZn as filler metal under an argon gas atmosphere. The brazing parameters included temperature, brazing time, and argon gas flow rate. The study employed Box-Behnken design for experimental design and desirability function as the optimization tool. Mechanical properties study included the measurements of shear force, microhardness, microstructure, and fracture of brazing joints through a scanning electron microscope (SEM) as well as the chemical composition using an energy dispersive x-ray spectroscopy (EDS). As a result, the temperature and the brazing time significantly affected the shear force of the brazed joint at a 95 percent confidence interval. The optimal condition of the study was 800°C of temperature and a 20-minutes brazing time which caused the maximum shear force at 5,909.1 N. The brazing joint strength was increased when the temperature and time of brazing were increased and reached the optimal point. Microstructure showed a formation of an Ag-rich phase, a Cu-rich equiaxed dendrite phase, and a eutectic Ag-rich phase, which completely combined as the network structure and evenly small fine grains. Moreover, the shear force of the brazed joint was decreased when the temperature and time of brazing exceeded the optimal point due to the grain growth of the interface layer.

Insights into nanostructured silica particle formation from sodium silicate using spray drying: An experimental and theoretical study

Spray drying is a widely used operational procedure utilized in diverse sectors. The current knowledge of droplet mobility processesinside the drying chamber is not fully comprehensive due to the complex nature of droplet evaporation issues. The present study used a comprehensive methodology that integrated numerical models and actual testing to investigate the drying process of droplets in the context of spray drying. The precursor material utilized in this investigation was colloidal silica. The influence of external hydrodynamic variables, such as drying temperature (473, 673, and 873 K) and carrier gas flow rate (2, 4, 6 L/min), was thoroughly investigated in connection to the dynamics of droplets and the subsequent creation of silica particles. Distinct alterations in the size and shape of the silica particles were observed due to variations in drying temperature and carrier gas flow rate. The validity of this investigation was established by the generation of two discrete particle morphologies, namely spherical particles and doughnut-shaped particles. Spherical particles were produced under reduced carrier gas flow rates of 2 L/min and lower drying chamber temperatures of 473 K. In the quantitative evaluation, the computational fluid dynamics (CFD) computations properly established the evaporation rate constant (K) and the temperature difference (ΔT) inside the droplets. Furthermore, qualitative calculations provide insight into the complex dynamics of droplet motion inside the spray chamber. The results of this study have the potential to open up new possibilities for regulating nanoparticle creation via the use of the spray drying process.

Predictive modeling and multi-parametric optimization of catalytic pyrolysis of disposable face mask using a combinational approach of response surface methodology and machine learning: Insights into the influence of waste-derived catalyst

The current study aims to model and optimize the catalytic pyrolysis of face masks incorporating a waste-derived catalyst to analyze the effect of process parameters (temperature, feed-to-catalyst ratio, and inert gas flow rate) on the oil yield of the process. An integrated approach of response surface methodology (R2-0.95) and machine learning (decision trees regression, R2-0.83) demonstrated a higher prediction accuracy and lower error margins. Explainable artificial intelligence tools spotlighted temperature to be the predominant parameter followed by feed-to-catalyst ratio. Experimental oil yield (13.5%) obtained at optimized parameters (516 °C temperature, 3:1 feed-to-catalyst ratio, and 163 mL/min inert gas flow rate) was compared with those predicted through response surface methodology (13.7%) and decision trees regression (13.12%), showcasing an absolute error range of 0.2–0.4 wt%. Gas chromatography-mass spectroscopy analysis of oil highlighted the presence of silica compounds that can be extracted as value-added chemicals. Further, the overall percentage of naphthene's, paraffins, and olefins in the oil were approximated to be around 40.5% based on the peak area. The presence of hydrocarbons in oil having carbon numbers predominantly in the range of gasoline and diesel as well as a high heating value of 36.56 MJ/kg demonstrated its potential to be used as a fuel. The present study demonstrates the feasibility of valorizing the face mask into energy-dense oil comparable to commercial range fuel using a spent adsorbent based catalyst.

Flow structure and heat transfer characteristics of sweeping and steady impingement jets with/without chevrons on a semi-circular concave surface

Striving for improved gas turbine performance requires operating at higher gas flow temperatures, posing challenges in preserving the structural integrity of the gas turbine. To respond to these challenges, gas turbine manufacturers have turned to internal cooling and jet impingement to provide an effective solution for cooling the leading edge of the gas turbine blades. Fluidic oscillator is known for its sweeping behavior and expansive coverage of targeted surface and, thus, it can efficiently remove heat. In this study, the author numerically simulated the cooling performance of the leading edge of the gas turbine blades under constant heat flux while using four different configurations of jet impingement: a sweeping jet, a sweeping jet with chevrons, a steady jet, and a steady jet with chevrons. The results showed that the sweeping jet configuration with chevrons outperformed the steady jet configurations owing to oscillating jet impingement and a higher intensity of turbulence that increased the entrainment of jet flow. Under the configuration of a sweeping jet with chevrons, the targeted surface recorded an average Nusselt number that is 19.2% higher than the one with a steady jet without chevrons, along with a more uniform distribution of the surface temperature. The outstanding behavior of the sweeping jet with chevrons is due to the its internal flow behavior, i.e., oscillating flow nature of the sweeping jet with augmented turbulence at the exit of the chevron's nozzle.

Calculation of the required methanol consumption during the flow of wet hydrocarbon gas in a horizontal pipeline

One of the main problems that have to be solved during the development of hydrocarbon deposits is the formation of gas hydrates in pipelines. In this regard, the article presents a preventive method to struggle against the formation of gas hydrate deposits on the pipes inner walls associated with the supply of a hydrate formation inhibitor to the gas stream. The research was conducted on the basis of a mathematical model of the wet hydrocarbon gas flow in a horizontal pipeline. The research object is to determine the minimum required consumption of methanol, in which there is no formation of gas hydrate deposits on the channel inner walls. The practical significance of this study is that it is aimed at reducing the risks associated with the formation of gas hydrates in pipelines. The numerical implementation of a mathematical model of natural gas flow in a horizontal channel is based on a sequential solution of a system of four differential equations by the Runge-Kutta method of 4 orders of accuracy, followed by a search for sequential approximations of the minimum inhibitor flow rate, in which the "gas + water ↔ gas hydrate phase" transition process does not occur on the inner surface of the channel. The article presents a calculation of the proportion of a hydrate formation inhibitor in the liquid phase by solving a cubic equation using the Cardano method. Based on the computational experiments results, graphs were constructed and interpreted of the dependencies of the minimum inhibitor consumption on the soil temperature, inlet gas pressure, total water concentration in the gas flow, initial gas temperature and total gas flow rate.

Effect of pressurant flow rate and ullage conditions on mass transfer and thermal stratification in a partially filled LN2 tank

Experimental and numerical computations have been carried out to investigate the evolution of pressure and temperature in the liquid nitrogen (LN2) tank pressurized with gaseous nitrogen (GN2). A parametric study has been carried out to study the effect of ullage volume and pressurant gas (GN2) flow rate (0.25–2 g/s) and temperature (250–350 K) on the pressure evolution and thermal stratification in the tank during active pressurization from 1 bar to 3 bar. Experiments are conducted in a small range of mass flow rates at a given pressurant gas temperature (302 K). The numerical simulations are validated with the experiments and a parametric study has been performed. It has been observed that pressurization time varies linearly with the liquid depth. Thermally stratified mass in LN2 increases with the decrease in pressurant mass flow rate for a given pressure rise. Numerical simulations revealed that mass condensed during the pressurization is a weak function of ullage depth and temperature but a strong function of the mass flow rate. The pressurant gas requirement follows the correlation of Ludwig and Dreyer (2014) for relatively higher mass flow rates. The pressurant gas temperature has a strong influence on the flow pattern in the ullage. The pressurant gas flows along the wall and reaches the interface without disturbing the bulk vapor. Heat transfer at the interface is dominated by the heat carried by the pressurant than by transfer from the bulk vapor.