Surface Mechanical Treatment Research Articles

Strain induced recrystallization in lanthanum zirconate ceramic

The focus of this work is to investigate the strain-induced recrystallization behavior on the surface of La2Zr2O7 ceramic through annealing. Unlike in metallic materials, the recrystallization phenomenon resulting from surface mechanical treatment in ceramics has not been extensively explored. In this study, we examine the strain-induced recrystallization in La2Zr2O7 that has undergone surface deformation and subsequent annealing at different temperatures. It reveals the presence of recrystallized grains in the region of the surface that was deformed, following the annealing process. To better understand the driving force for the recrystallization behavior, we analyze the variation of stored deformation energy in La2Zr2O7 using Raman spectroscopy. The study also highlights the microstructural evolution, revealing that shear bands, characterized by a high density of dislocations, serve as preferential sites for the nucleation of recrystallized grains. Finally, we discuss the mechanism of strain-induced recrystallization in ceramic materials.

A Study on Surface Quality and Mechanical Property Improvement Through Mechanical Surface Treatment of Amorphous Metal

A Study on Surface Quality and Mechanical Property Improvement Through Mechanical Surface Treatment of Amorphous Metal

Development of a Cavitation Generator Mimicking Pistol Shrimp.

Pistol shrimp generate cavitation bubbles. Cavitation impacts due to bubble collapses are harmful phenomena, as they cause severe damage to hydraulic machinery such as pumps and valves. However, cavitation impacts can be utilized for mechanical surface treatment to improve the fatigue strength of metallic materials, which is called "cavitation peening". Through conventional cavitation peening, cavitation is generated by a submerged water jet, i.e., a cavitating jet or a pulsed laser. The fatigue strength of magnesium alloy when treated by the pulsed laser is larger than that of the jet. In order to drastically increase the processing efficiency of cavitation peening, the mechanism of pistol shrimp (specifically when used to create a cavitation bubble), i.e., Alpheus randalli, was quantitatively investigated. It was found that a pulsed water jet generates a cavitation bubble when a shrimp snaps its claws. Furthermore, two types of cavitation generators were developed, namely, one that uses a pulsed laser and one that uses a piezo actuator, and this was achieved by mimicking a pistol shrimp. The generation of cavitation bubbles was demonstrated by using both types of cavitation generators: the pulsed laser and the piezo actuator.

Surface characteristic of Ti-6Al-4V alloy fabricated by Electron Beam Melting prepared by different surface post treatments

Metal additive manufacturing (AM) is a technique in constant growth that offers freedom in design in the production of complex shape components. However, it is well documented that most types of material failures in the AM parts are very sensitive to their surface properties. Hence, in this work, some surface post-treatments such as grinding, drag finishing and Surface Mechanical Treatment (SMT) are used as post-treatment processes to improve the performance of Ti-6Al-4V samples fabricated by the Electron Beam Melting technique. The influences of different post-treatment were investigated on the surface properties. The outcomes demonstrated that the SMT has- the highest efficiency in the surface treatment and could reduce surface roughness, increase hardness and improve wettability. This work demonstrates the potential of SMT to achieve favourable surface properties of AM metallic components.

Mechanical properties, surface treatments, and applications of jute fiber reinforced composites—A review

AbstractThe rise in environmental concerns and pollution is largely to blame for the popularity of jute and its hybrid composites. Jute fibers are inexpensive, plentiful, and have acceptable mechanical characteristics such as tensile, flexural, and impact strength, along with a moderate to high tensile modulus. Environmental worries about the risks of composites made with synthetic fibers have caused an exponential growth in research into all‐natural fibers and materials. Many applications have made heavy use of jute and its hybrid composites. Hybrid jute‐based composites offer improved mechanical and physical characteristics that are marginally superior to jute fiber composites. This review includes a thorough examination of composites made of jute fiber. The main objective of this review article is to offer a critical analysis and highlight all recent advancements in jute‐based composites. The information in the article covers a variety of jute‐based composites topics, such as their chemical composition, surface treatments, mechanical and physical properties, applications, and hybrid jute‐based composites.

Low strain hardening enables improved water droplet erosion performance through deep rolling

The present work investigates the role of deep rolling surface treatment on the water droplet erosion behavior of 17–4 PH stainless steel. Standard heat treatments were first applied to samples of 17–4 PH stainless steel to achieve three states, solution treated and two different aging conditions. The mechanical properties of these conditions were determined using hardness and tensile tests. Then, deep rolling surface treatments were applied to the various conditions of the 17–4 PH. Water droplet erosion tests were subsequently performed at impact velocities of 250 m/s and 300 m/s, and the erosion performance in terms of incubation period and maximum erosion rate before and after the deep rolling treatment is compared. It was found that deep rolled samples exhibited considerably longer incubation periods compared to only heat-treated samples. The improvement in erosion resistance of the 17–4 PH stainless steel is attributed to its lower strain hardening exponent values, which reduces embrittlement that is usually associated with the work hardening due to deep rolling. Hence, it is concluded that low strain hardening exponent is essential to the effectiveness and success of mechanical surface treatments to combat water droplet erosion.

Mechanical and chemical surface treatment enhances bond strength between zirconia and orthodontic brackets: an in vitro study

ObjectivesTo assess the shear bond strength (SBS) between metal orthodontic brackets and zirconia after receiving different mechanical and chemical surface treatments, and different types of resin adhesive. The failure mode of each treatment protocol was also evaluated.Materials and methodsThe present in vitro experimental study consisted of six surface treatment protocols with two different resin adhesives. One-hundred and forty-four rectangular-shaped 3 mol% yttrium-stabilized tetragonal zirconia polycrystal blocks were milled, sintered, and embedded in acrylic resin. They were randomly divided into three mechanical (none, air abrasion, and bur grinding) and two chemical surface treatment conditions (no primer and Z-primer). The specimens were divided into two groups according to the resin adhesive received: self-cured (RelyX U200) and light-cured adhesives (Transbond XT). The SBS between the metal bracket and zirconia was tested using a universal testing machine (1-mm/min crosshead speed), and the failure mode was evaluated. Differences in SBS and failure mode were analyzed using Welch ANOVA followed by post-hoc comparison and Fisher’s Exact test, respectively.ResultsBur grinding produced the highest SBS, followed by air abrasion. Z-primer application typically provided a higher SBS regardless of resin adhesive used (p < 0.001). Without primer application, RelyX U200 provided a higher SBS than Transbond XT (p < 0.001). After grinding, using Z-primer and RelyX U200 resulted in a higher SBS than no primer and using Transbond XT (p < 0.001). Adhesive failure at the zirconia–adhesive interface occurred only when Transbond XT was applied without bur grinding, and when using Transbond XT after grinding, but no Z-primer application.ConclusionBur grinding combined with applying an MDP-containing primer and resin adhesive enhances the SBS between zirconia and metal orthodontic brackets.

Influence of post-processing treatment on the surface roughness of polyamide PA12 samples manufactured using additive methods in the context of the production of orthoses

Additive techniques are gaining popularity, primarily due to the emergence of new 3D printing methods, advancements in 3D printers, and the availability of innovative materials. Models produced using additive processes can undergo additional post-processing and dyeing to modify their functional and visual properties. This article presents the results of surface roughness tests conducted on samples made of polyamide PA12, using the Selective Laser Sintering (SLS) and HP MultiJet Fusion (MJF) methods. Regarding the processing methods, chemical surface treatment contributed to reducing Ra and Rz parameters by about 80% for both analyzed printing methods, while mechanical surface treatment resulted in a reduction of approximately 40% for SLS samples and 30% for MJF samples. On the other hand, dyeing and applying an antibacterial coating did not significantly affect the Ra and Rz parameter values. Considering the obtained results, the recommended manufacturing method for orthosis is the MJF method, and the finishing process should include mechanical treatment followed by dyeing.

Shear Strength of Repaired 3D-Printed and Milled Provisional Materials Using Different Resin Materials with and without Chemical and Mechanical Surface Treatment.

The aim of this study was to assess the shear bond strength of 3D-printed and milled provisional restorations using various resin materials and surface finishes. There were 160 preliminary samples in all, and they were split into two groups: the milled group and the 3D-printed group. Based on the resin used for repair (composite or polymethylmethacrylate (PMMA)) and the type of surface treatment utilized (chemical or mechanical), each group was further divided into subgroups. The specimens were subjected to thermocycling from 5 °C to 55 °C for up to 5000 thermal cycles with a dwell time of 30 s. The mechanical qualities of the repaired material underwent testing for shear bond strength (SBS). To identify the significant differences between the groups and subgroups, a statistical analysis was carried out. Three-way ANOVA was used to analyze the effects of each independent component (the material and the bonding condition), as well as the interaction between the independent factors on shear bond strength. Tukey multiple post-hoc tests were used to compare the mean results for each material under various bonding circumstances. The shear bond strengths of the various groups and subgroups differed significantly (p < 0.05). When compared to the milled group, the 3D-printed group had a much greater mean shear bond strength. When compared to PMMA repair, the composite resin material showed a noticeably greater shear bond strength. In terms of surface treatments, the samples with mechanical and chemical surface treatments had stronger shear bonds than those that had not received any. The results of this study demonstrate the effect of the fabrication method, resin type, and surface treatment on the shear bond strength of restored provisional restorations. Particularly when made using composite material and given surface treatments, 3D-printed provisional restorations showed exceptional mechanical qualities. These results can help dentists choose the best fabrication methods, resin materials, and surface treatments through which to increase the durability and bond strength of temporary prosthesis.

Hybrid Mechanical Surface Treatment Technology via UNSM and Burnishing for Realizing High Surface Hardness

Hybrid Mechanical Surface Treatment Technology via UNSM and Burnishing for Realizing High Surface Hardness

A Review—Effect of Accelerating Methods on Gas Nitriding: Accelerating Mechanism, Nitriding Behavior, and Techno-Economic Analysis

Gas nitriding, as a surface modification technology to improve the wear resistance of workpiece surfaces, is widely used in wind turbine gears, pressure vessel gears, high-precision die casting abrasives, and other areas. However, the gas nitriding time is too long, reaching 40–60 h, which reduces the efficiency of nitriding and hinders the development of gas nitriding. Therefore, various accelerating methods are born accordingly. This review first introduces the basic principle, microstructure, and process parameters of conventional gas nitriding. Then, five common accelerating methods are summarized: process parameter optimization, surface mechanical nano-crystallization, surface-active catalysis, surface pre-oxidation, and surface laser treatment. Then, the effect of acceleration methods on gas nitriding is analyzed for the acceleration mechanism, nitriding behavior, and nitriding efficiency. Finally, the technical economy of the acceleration methods is compared for three aspects: energy consumption, carbon dioxide emission, and cost. And, the technical maturity of the acceleration methods is compared according to technology readiness level (TRL) technology. Based on the above content, the advantages and disadvantages of the five accelerating methods are reviewed, and the concept of a multi-technology collaborative processing acceleration method is proposed.

Effect of Aging and Different Surface Treatments on Repair Bond Strength of Hybrid Resin Composites

Background: With the trend for minimally invasive dentistry and the rapid evolution of composite resin materials, repair of defective composite resin restorations is a popular choice rather than replacement of the restoration. The durability of the bond between the old and repaired composite restoration is important for a successful outcome. Objective: To evaluate the immediate and delayed shear bond strength of two types of repaired hybrid resin composites using different chemical and mechanical surface treatments. Methods: Two types of hybrid resin composites, micro-hybrid resin composite and nanohybrid resin composite, were used to prepare 288 pre-polymerized resin composite specimens. After polymerization, repair was done after 24 hours and 6 months. Each hybrid resin composite group was divided into 3 groups according to surface treatment used to repair the substrate: group 1: no surface treatment, group 2: treated by medium abrasive stone, and group 3: treated by fine abrasive stone. Each group was further subdivided into 3 subgroups according to different agents used for repair: group 1: Silane, group 2: Universal adhesive, and group 3: Silane + adhesive. Shear bond strengths of the repaired specimens were measured using a Universal testing machine. Failure modes were evaluated under a stereomicroscope. Results: Different chemical and mechanical surface treatments had a significant effect on the shear bond strength values of all groups (p ≤ 0.05). The highest mean shear bond strength values were found in nano-hybrid composites immediately repaired by silane after treatment by a medium abrasive stone while the lowest mean shear bond strength values were found in micro-hybrid composites with delayed repair and no surface treatment. Conclusion: Diamond burs using silane with adhesive improved the repair bond strength of the tested hybrid composites. In composite repair, using abrasive mechanical pretreatment followed by adhesive conditioning is crucial for the success of the repair restoration.

Surface Conditions after LASER Shock Peening of Steel and Aluminum Alloys Using Ultrafast Laser Pulses.

Laser shock peening (LSP) is a mechanical surface treatment process to modify near-surface material properties. Compared to conventional shot peening (SP) the process parameters can be finely adjusted with greater precision and a higher penetration depth of compressive residual stresses could be reached. However, high process times of LSP leads to high production costs. In this study, ultrafast LSP (U-LSP) with an ultrafast laser source (pulse time in the picosecond range) was applied on specimens made of X5CrNiCu15-5 and AlZnMgCu1.5. The surface characteristics (surface roughness) and surface-near properties (microstructure, residual stresses, and phase composition) were compared to the as-delivered condition, to conventional laser shock peening (C-LSP), and to SP, whereas metallographic analyses and X-ray and synchrotron radiation techniques were used. The process time was significantly lower via U-LSP compared to C-LSP. For X5CrNiCu15-5, no significant compressive residual stresses were induced via U-LSP. However, for AlZnMgCu1.5, similar compressive residual stresses were reached via C-LSP and U-LSP; however, with a lower penetration depth. A change in the phase portions in the surface layer of X5CrNiCu15-5 after C-LSP compared to SP were determined.

Surface Modification Methods of Self-Cured Acrylic Resin Repaired with Resin Composite Using a Universal Adhesive

This research study’s purpose was to evaluate the mechanical and chemical surface treatment methods for self-cured acrylic resin repaired with a resin composite employing a universal adhesive agent. Eighty self-cured acrylic resins were built and designed into eight groups of ten specimens and surface conditioned using sandblasting (SB) and/or with methylmethacrylate monomer (MMA) and/or universal adhesive (UA) as follows: Group 1, non-surface modified; Group 2, SB; Group 3, UA; Group 4, SB + UA; Group 5, MMA; Group 6, SB + MMA; Group 7, MMA + UA; Group 8, SB + MMA + UA. A template was put on the specimen center, and the pushed resin composites. Mechanical testing machinery was used to examine the samples’ shear bond strength (SBS) values. To examine failure patterns, the debonded specimen surfaces were examined using a scanning electron microscope. The one-way ANOVA method was used to evaluate these data, and Tukey’s test was used to determine the significance level (p &lt; 0.05). The highest SBS was obtained in Group 8 (27.47 ± 2.15 MPa); however, it was statistically equivalent to Group 7 (25.85 ± 0.34 MPa). Group 1 (4.45 ± 0.46 MPa) had the lowest SBS, but it was not statistically significant compared to Group 2 (5.26 ± 0.92 MPa). High SBS values were frequently correlated with cohesive patterns. The application of MMA prior to UA is the best method for increasing the SBS between self-cured acrylic resin and resin composite interfaces. However, the use of SB is not significantly different from not using SB.

Effect of combination of microstructure and surface treatment on shear strength of precision bonded joints

ABSTRACT To improve the bonding strength of precision adhesive joints, mechanical and electrochemical surface treatments were combined to modify the original bonding surfaces. Microgrooves with different aspect ratios were manufactured on aluminum-alloy surfaces and phosphoric acid anodizing (PAA) was then applied to the surfaces. Wettability, shear strength, and fracture morphology were tested and analyzed. PAA treatment could change the original flat surface to be hydrophilic, and microgrooves could further enhance these characteristics. Compared with the original flat surface, the shear strength of the micro-structured surfaces without PAA treatment increased by 8.54% at an aspect ratio of 0.02, but decreased by 0.22% and 1.90% as the aspect ratio increased to 0.04 and 0.08, respectively. The shear strength of the flat surface only treated by PAA increased by 22.88%, while combining microgrooves could further improve the shear strength by 38.17%, 39.09%, and 42.24% at aspect ratios of 0.02, 0.04, and 0.08, respectively. Fracture morphology analysis and observation of interfacial wetting indicated that manufacturing microgrooves and applying PAA treatment on the aluminum-alloy surfaces could eliminate many tiny interface failures and greatly increase the effective bonding area, which significantly improved the shear strength.

Development of Laser Cavitation Peening Using a Normal-Oscillation Nd:YAG Laser

The impact induced by cavitation bubble collapse can be utilized for mechanical surface treatment to improve fatigue properties of metals including additive manufactured metallic materials. A peening method using cavitation impact induced by a pulsed laser is called “laser cavitation peening (LCP)”. Normally, a Q-switched Nd:YAG laser, whose pulse width is a few nanoseconds, is used for LCP, which improves the fatigue strength. The problem with LCP is that the processing time is too slow. If a laser pulse whose pulse width is a few hundred microseconds can be utilized for LCP, the repetition frequency can be increased drastically using other types of laser systems such as a fiber laser. In the present paper, in order to reveal the possibility of LCP using a pulsed laser width of a few hundred microseconds, the use of LCP with a normal-oscillation Nd:YAG laser (pulse width ≈ 200 μs) was investigated. It is demonstrated that LCP with the normal-oscillation Nd:YAG laser produced curvature in an aluminum alloy plate. The shock pressure wave and impulsive vibration of the target surface at the first collapse of laser cavitation (LC), which was induced by the normal-oscillation Nd:YAG laser, was 3–4 times larger than those of laser ablation (LA).

Residual stress associated with crystalline phase transformation of 3–6 mol% yttria-stabilized zirconia ceramics induced by mechanical surface treatments

Monolithic dental prostheses made of 3–6 mol% yttria-stabilized zirconia (3–6YSZ) have gained popularity owing to their improved material properties and semi-automated fabrication processes. In this study, we aimed to evaluate the influence of mechanical surface treatments, such as polishing, grinding, and sandblasting, on the residual stress of 3–6YSZ used for monolithic prostheses in association with crystalline phase transformation. Plate specimens were prepared from five dental zirconia blocks: Aadva Zirconia ST (3YSZ), Aadva Zirconia NT (6YSZ), Katana HT (4YSZ), Katana STML (5YSZ), and Katana UTML (6YSZ). The specimens were either polished using 1, 3, or 9 μm diamond suspensions, ground using 15, 35, or 55 μm diamond discs, or sandblasted at 0.2, 0.3, or 0.4 MPa. The residual stress, crystalline phase, and hardness were analyzed using the cosα method, X-ray diffraction (XRD), and Vickers hardness test, respectively. Additionally, we analyzed the residual stress on the surfaces of monolithic zirconia crowns (MZCs) made of 4YSZ, 5YSZ, and 6YSZ, which were processed using clinically relevant procedures, including manual grinding, followed by polishing using a dental electric motor on the external surface, and sandblasting on the internal surface. Residual stress analysis demonstrated that grinding and sandblasting, particularly the latter, resulted in the generation of compressive residual stress on the surfaces of the plate specimens. XRD revealed that the ground and sandblasted specimens contained a larger amount of the rhombohedral phase than that of the polished specimens, which may be a cause of the residual stress. Sandblasting significantly increased the Vickers hardness compared to polishing, which may possibly be due to the generation of compressive residual stress. In the case of MZCs, compressive residual stress was detected not only on the sandblasted surface, but also on the polished surface. The difference in the residual stress between the plate and crown specimens may be related to the force applied during the automated and manual grinding and polishing procedures. Further studies are required to elucidate the effects of the compressive residual stress on the clinical performance of MZCs.

Application of gradient severe shot peening as a novel mechanical surface treatment on fatigue behavior of additively manufactured AlSi10Mg

Post-processing methods can be crucial in addressing the associated anomalies of the as-built state of additively manufactured materials. In this study, for the first time, the effects of gradient severe shot peening as a novel mechanical surface treatment, along with other types of shot peening treatments, including conventional, severe, and over shot peening processes were investigated individually and combined with heat treatment on fatigue behavior of hourglass AlSi10Mg samples fabricated by laser powder bed fusion. Detailed experimental characterizations in terms of microstructure, porosity, surface texture, hardness and residual stresses as well as rotating bending fatigue behavior were conducted. The experimental results revealed a significant fatigue behavior improvement after applying gradient severe shot peening treatments due to their remarkable capacity to modulate surface texture, known as a side effect of peening, besides surface layer nanocrystallization, enhanced hardness, and high compressive residual stresses.

To Evaluate and Compare the Effect of Various Surface Treatment Modalities on Shear Bond Strength of Composite to Polyetherketoneketone and SEM Analysis: An In vitro Study

Abstract Context: It is a challenge to bond resin materials with polyetherketoneketone (PEKK). To increase the bond strength, surface treatments using chemical adhesion, mechanical adhesion, or a combination of both can be used. Aims: The objective of the present study was to evaluate and compare the shear bond strength of PEKK to the composite resin after various surface treatments and to evaluate the fracture mode analyses. Materials and Methods: One hundred and twenty PEKK specimens were randomly divided into four groups (n = 30) after three different surface treatments (95% sulfuric acid etching, airborne abrasion with 110 μm aluminum-oxide, and 99% acetone). With the help of polytetrafluorethylene tube, resin composite (3M ESPE) was bonded on all the specimens, thermocycled, and subjected to shear bond strength testing. Thereafter, 15 samples from each group were assessed for fracture mode analyses using a scanning electron microscope. Statistical Analysis Used: Mean, Standard deviation, one-way analysis of variance (ANOVA) f-test, post hoc Tukey’s test. Results: Statistical analysis using one-way ANOVA f-test revealed that the results were significant with a P &lt; 0.05 with the maximum value obtained in the case of air abraded group and the minimum value obtained in the case of the untreated group. Adhesive failure mode was the most common among the air-abraded group. Conclusions: The mechanical surface treatment group (air abrasion) showed higher shear bond strength than the chemical surface treatment groups (sulfuric acid and acetone). The mixed-type fracture mode was most commonly noted in the air-abraded group.

Improvement of Fatigue Properties of EN AW 6082 Aluminum Alloy using Different Deep Rolling Directions

Deep rolling (DR) is an effective mechanical surface treatment method to improve the fatigue properties of engineering components. In this method, the surface of the component was rolled using a roller with a predetermined force to obtain reduced roughness, hardness increases and compressive residual stresses in the surface region. These alterations allow for increasing the fatigue lives of the components in industrial applications. In the current study, DR was applied in tangential and longitudinal directions on specimens that were manufactured using EN-AW 6082-T6 aluminum. The resulting roughness, hardness and residual stresses were determined experimentally. Fatigue tests were carried out to determine the improvements in fatigue properties after DR. It was found that DR-induced compressive residual stresses depend on DR direction considerably. Due to this reason, fatigue strength improvements were found to be different for different DR direction applications. Longitudinal rolling resulted in a 23% fatigue strength increase compared to a 7% increase for tangential rolling. For both DR direction applications, fatigue cracks were shown to initiate at the sub-surface region, whereas the as-turned specimens exhibited surface crack initiation.