Submillimeter Gaps Research Articles

Shear properties and dynamic responses of greases in a micrometer-order gap

Grease is used as a lubricant in a wide range of fields, including bearings, because it reduces friction, prevents harmful wear of components, protects against rust and corrosion, and acts as a seal to prevent the invasion of dirt and water. Although most of the research on grease has focused on the environment inside the bearing, there has been little research on the fundamental lubrication mechanism of grease. It is known that thickeners, which keep a complex three-dimensional structure in the grease, have a significant effect on the shear characteristics of grease, and it is assumed that this is due to the orientation of the thickener structure in the shear direction. In this study, the apparent viscosity of grease in a micro-order gap was measured using our original viscometer and compared with the apparent viscosity measured with a submillimeter-order gap rheometer because grease may show different rheological properties compared to conventional measurements. In addition, the dynamic response of viscous resistance that appeared when each grease was subjected to a change in the shear force was quantitatively evaluated using relaxation time. As a result, the apparent viscosity remarkably decreased in a micro-order gap compared to a submillimeter gap, and two types of shear thinning mechanisms were proposed based on the orientation of the thickener: one caused by the narrow gap and the other by the shear force. In addition, the behavior of viscous resistance due to changes in the shear force depended on the type of thickener. It was also confirmed that the relaxation time of each grease correlates with its oil film-forming ability and the entanglement level of the thickener’s structure. Furthermore, the mechanism of the dynamic response was proposed based on the reorientation of thickeners.

A computational study on the effects of fast-rising voltage on ionization fronts initiated in sub-mm air and CO2\\documentclass[12pt]{minimal} \\usepackage{amsmath} \\usepackage{wasysym} \\usepackage{amsfonts} \\usepackage{amssymb} \\usepackage{amsbsy} \\usepackage{mathrsfs} \\usepackage{upgreek} \\setlength{\\oddsidemargin}{-69pt} \\begin{document}$$_{2}$$\\end{document} gaps

Gas discharge and breakdown phenomena have become increasingly important for the development of an ever-growing number of applications. The need for compact and miniaturized systems within power, pulsed power, semiconductor, and power electronic industries has led to the imposing of significant operating electric field stresses on components, even within applications with low operating voltages. Consequently, the interest in gas discharge processes in sub-millimeter and microscale gaps has grown, as the understanding of their initiation and propagation is critical to the further optimization of these technologies. In this work, a computational study of primary ionization fronts has been conducted, which systematically investigated the role of voltage rate-of-rise in point-plane and point-point electrode geometries with an inter-electrode gap maintained at 250 μ\\documentclass[12pt]{minimal} \\usepackage{amsmath} \\usepackage{wasysym} \\usepackage{amsfonts} \\usepackage{amssymb} \\usepackage{amsbsy} \\usepackage{mathrsfs} \\usepackage{upgreek} \\setlength{\\oddsidemargin}{-69pt} \\begin{document}$$\\upmu$$\\end{document}m and a needle radius of 80 μ\\documentclass[12pt]{minimal} \\usepackage{amsmath} \\usepackage{wasysym} \\usepackage{amsfonts} \\usepackage{amssymb} \\usepackage{amsbsy} \\usepackage{mathrsfs} \\usepackage{upgreek} \\setlength{\\oddsidemargin}{-69pt} \\begin{document}$$\\upmu$$\\end{document}m. Using the hydrodynamic approach with the local mean energy approximation, along with simplified plasma chemistry, simulations have been performed under positive and negative ramp voltages, rising at 50, 25, 16.67, 12.5, and 10 kV/ns in synthetic air and in pure CO2\\documentclass[12pt]{minimal} \\usepackage{amsmath} \\usepackage{wasysym} \\usepackage{amsfonts} \\usepackage{amssymb} \\usepackage{amsbsy} \\usepackage{mathrsfs} \\usepackage{upgreek} \\setlength{\\oddsidemargin}{-69pt} \\begin{document}$$_{2}$$\\end{document}. Results on the developed electric field, electron densities, and propagation velocities are presented and discussed. Effects on the cathode sheath thickness scaling with voltage rate-of-rise have been additionally analyzed, the mechanisms behind these effects and their potential impacts are discussed. The work conducted in this study contributes towards an increased understanding of the gas discharge process, under fast-transients and nonuniform electric fields, with relevance to microelectromechanical, power, and pulsed power system design.

Experimental analysis of oil flow and drag torque generation in disengaged wet clutches

Fundamental knowledge of the oil flow in a disengaged wet clutch is essential for optimizing the cooling performance and the drag losses. However, no fundamental information on the oil flow and drag torque generation is available for dip-lubricated wet clutches. Therefore, the oil flow and drag torque generation in the sub-millimeter gap of a dip-lubricated wet clutch was experimentally investigated for three practically relevant oil levels. To enable optical access to the gap, transparent components were used. Further, a high-speed camera was used to capture the oil flow in the gap and grooving. Independent of the set oil level, the gap is oil-filled at low differential speeds, resulting in a single-phase flow. The drag torque increases approximately linearly with increasing differential speed due to the fluid shearing. In certain regions of the waffle grooving, air bubbles form locally. The air bubbles preferably occur in the grooves oriented in the radial direction, while the grooves oriented in the peripheral direction are filled with oil. Above a certain differential speed, the oil is continuously displaced from the gap, starting from the inside, due to the increasing centrifugal force. Consequently, the drag torque increases in a degressive manner until a maximum value is finally reached. The ongoing displacement of oil from the gap eventually results in a decrease in the drag torque. A steady drag torque is generated only when the oil is almost entirely displaced from the gap. Since the oil displacement from the gap already commences at a low differential speed, the cooling performance is limited for dip-lubricated wet clutches. The continuous displacement of oil from the gap can be held up, among other things, by increasing the oil level.

Trichel pulse characteristics and mechanism of negative corona discharge in sub-millimeter gaps

A negative corona discharge system of a needle-plate electrode suitable for sub-millimeter gaps is established to investigate Trichel pulse characteristics of negative corona discharge, in which an optical acquisition system is especially applied to timely observe a discharging corona. Electrostatics–hydrodynamics coupling simulations of air discharging in 100 μm-gaped needle-plate electrodes are performed to elucidate the micro-physical process of negative corona discharge. The impact ionization coefficient used for simulations and the experimentally recorded images of discharge corona are combined to characterize the active region of secondary electron emission. Dynamical distribution and transport of the charged particles are analyzed from multiphysics simulations to explain the microscopic mechanism for various stages of Trichel pulses. Even though the corona front near the plate electrode maintains a high rate of collision ionization and secondary electron excitation, the needle tip corona has not reached the threshold electric field of electron avalanche required for glow discharge, as manifested by discharge sawtooth waves comprised of corona and glow components. The amplitude and frequency of Trichel pulses increase, respectively, with impact ionization and secondary electron emission, which is evidently dependent on attachment coefficient and anion mobility. A higher attachment coefficient will lead to a significant reduction in amplitude of Trichel pulses. The present study provides a theoretical basis and experimental verification for micrometer discharges, which is the key point of insulation protections in microelectromechanical systems.

Discharge characteristics of positive and negative polarity streamers with submillimeter gap based on fractal theory

In order to study the characteristics of streamer discharge in sub-millimeter gap, an experimental system and an image acquisition system of positive and negative polarity streamer discharge in the gap of 100–500 μm at atmospheric pressure are built, and the initial breakdown voltages and breakdown images of positive and negative polarity streamer discharge in a gap range of 100–500 μm are collected, and the fractal dimension of the experimental discharge images is calculated by Matlab. The experimental analysis shows that the air breakdown discharge in the gap range of 100–500 μm still conforms to the stream theory, and the polarity effect between the breakdown voltage of positive and negative streamers and the fractal dimension of the discharge image is obvious. The influence of space charge and photoionization on the meandering degree and coverage of the discharge channel in stream theory increase with the increase of the gap, and jump at 300 μm. The fractal simulation of positive and negative streamer discharge with a gap of 500 μm is established by using WZ (Wiesmann-Zeller) model based on fractal theory in Matlab. It is found that the development probability index <i>η</i> is inversely proportional to the fractal dimension, and that the <i>η</i> is smaller in positive streamer than in negative streamer under the same discharge condition.

On the applicability of LDV profile-sensors for periodic open wet clutch flow scenarios

The present experimental study revolves around the applicability of a Bragg-shifted laser Doppler velocimetry profile sensor (LDV-PS) in use for open wet clutch flow scenarios, where sub-millimeter gap height and textured surfaces are present. It is shown that the LDV-PS is capable to determine angular-resolved 1D3C velocity information, with all complex flow structures, depicted properly that are present in a radial groove. For the flow measurements the sensor is tilted to pm 30^{circ } compared to the axial orientation to enable the opportunity to reconstruct angular-resolved 1D3C velocity fields from two consecutively conducted runs. This facilitates measurement results with high axial and angular resolution for the complete open clutch flow and proves for the first time, that a profile sensor is capable to extract 3C information with the mentioned method. The results show that all characteristic flow structures occurring in the investigated sub-millimeter rotor-stator gap flow can be recorded properly. This insight renders the LDV-PS a promising and straight-forward applicable means to support industry-relevant research so as to uncover formerly hidden flow features and thus contribute to advanced development approaches for the respectively considered applications.Graphical abstract

Flow-structure identification in a radially grooved open wet clutch by means of defocusing particle tracking velocimetry

The volumetric defocusing particle tracking velocimetry (DPTV) approach is applied to measure the flow in the sub-millimeter gap between the disks of a radially grooved open wet clutch. It is shown that DPTV is capable of determining the in-plane velocities with a spatial resolution of 12;upmu mathrm{m} along the optical axis, which is sufficient to capture the complex and small flow structures in the miniature clutch grooves. A Couette-like velocity profile is identified at sufficient distance from the grooves. Moreover, the evaluation of the volumetric flow information in the rotor-fixed frame of reference uncovers a vortical structure inside the groove, which resembles a cavity roller. This vortex is found to extend well into the gap, such that the gap flow is displaced towards the smooth stator wall. Hence, the wall shear stress at the stator significantly increases in the groove region by up to 15% as compared to the ideal linear velocity profile. Midway between the grooves, the wall shear stress is around 4% lower than the linear reference. Furthermore, significant amounts of positive radial fluxes are identified inside the groove of the rotor; their counterpart are negative fluxes in the smooth part of the gap. The interaction of the roller in the groove and the resulting manipulation of the velocity profile has a strong impact on the wall shear stress and therefore on the drag torque production. In summary, this DPTV study demonstrates the applicability of such particle imaging approaches to achieve new insights into physical mechanisms of sub-millimeter gap flow scenarios in technical applications. These results help to bring the design- and performance-optimization processes of such devices to a new level.Graphic abstract

Magnetic field mapping simulations of sub-mm period undulators for the next generation X-ray free electron lasers

There is a growing interest on the compact XFELs to be used in applications such as medical science (surgery, fat removal), material science and military. In order to build a compact XFEL, constructing an undulator with sub-millimeter period (λu) is mandatory. Many problems arise due to miniaturization of undulators; such as keeping the magnetic field high while still having a considerable gap to minimize beam scraping. In this work, RADIA program has been employed for the modeling of sub millimeter period undulators (20μm<λu<400μm) with three different magnet configuration; namely Up–Down​ (↑↓↑↓…), Halbach (Wiggler) (↑→↓←↑…) and Hybrid (→↑←↓→…). Effects of sub-millimeter undulator period and gap on the magnetic field pattern of the undulator have been discussed.

Segmented electrode formation of semiconductor detector based on printable electronics technology for a medical imaging scanner

We developed prototype CdTe detectors with segmented electrodes using inkjet drawing in ink containing Gold nanoparticles by exploiting the sintering process for metallization. The resulting electrode patterns demonstrated that the inkjet technology is capable of forming fine detection elements with submillimeter alignment and gaps of several tens of micrometers. Moreover, it was shown that they are suitable for the construction of medical imaging scanners. In addition, it was also demonstrated that the proposed approach is compatible with conventional processes with respect to detector performance. The developed prototype detectors achieved good energy resolution that was comparable to other detectors based on conventional methods. In particular, an energy resolution of 1.7 % was obtained at 662 keV for a detector with pixel sizes of 2×2 mm2. It was also determined that gold nanoparticle inks can be metallized at a relatively low cure temperature of approximately 200 °C and this feature facilitates the fabrication of detectors by employing CdTe, which is a heat-sensitive material.

Atomic measurements of high-intensity VHF-band radio-frequency fields with a Rydberg vapor-cell detector

We investigate and employ optical Rydberg resonances in an atomic vapor cell for measurements of high-intensity VHF-band radio frequency (rf) electric fields. An atomic vapor cell with integrated electrodes is used to generate high-intensity 50--500 MHz rf electric fields reaching $\ensuremath{\sim}5$ kV/m in a submillimeter gap. The fields are measured using Rydberg electromagnetically induced transparency as an optical readout of field-sensitive $30{D}_{J}$ and $35{D}_{J}$ Rydberg states of atoms within the gap. The rf electric field is determined by matching observed spectroscopic markers, including ac level shifts, even-harmonic rf sidebands, and rf-induced avoided crossings in the Rydberg manifold to calculated spectra derived from a nonperturbative Floquet theory. In our measurements, rf field frequencies and electric-field amplitudes are determined to an accuracy of $1.0%$ and $1.5%$, respectively. In the atom-field interaction, we observe a transition from a quantum regime, characterized by discrete even-harmonic Floquet states separated by an even multiple of the rf field frequency, into a semiclassical regime at very strong fields, in which the spectrum exhibits unresolved resonances whose strengths are smoothly modulated at a frequency of approximately five times the rf frequency. The underlying physics is explored.

Accelerated induction of in vitro apatite formation by parallel alignment of hydrothermally oxidized titanium substrates separated by sub-millimeter gaps

ABSTRACTAlthough autoclaving is a common sterilization method for biomedical devices, the ability to induce deposition of apatite particles on hydrothermally treated titanium is still not fully realized. This is because the induction ability is too weak to be evaluated via in vitro apatite formation in Kokubo’s simulated body fluid (SBF) by the conventional immersion method, i.e. using samples with open and smooth surface. This study reports on the surface structure of hydrothermally treated titanium and the ability to induce deposition of apatite particles on the surface of parallel confined spaces separated by sub-millimeter gaps in Kokubo’s SBF. Thin-film X-ray diffraction and analyses using Fourier transform infra-red (FT-IR) spectroscopy and Raman spectroscopy revealed that a nano-crystalline anatase-type titanium oxide layer was formed on titanium substrates after hydrothermal treatment at 150°C for 2 h. When growth of the titanium oxide layer was moderately suppressed, the hydrothermally treated titanium surface exhibited a characteristic interference color, silver or gold, which does not impair the esthetic appearance of the titanium-based implant. The ability to induce deposition of apatite particles on hydrothermally treated titanium was remarkably amplified by parallel alignment of substrates separated by sub-millimeter gaps.

Importance of Interfacial Interactions to Access Shear Elasticity of Liquids and Understand Flow Induced Birefringence from Liquid Crystals to Worm-Like Micellar Solutions

This work points out the importance of the substrate boundary conditions to lower the dissipation in the dynamic measurement and access the closest dynamic characteristics of liquids, in particular to access the low frequency shear elasticity. The liquid/surface interface is a source of dissipation that enters and impacts the measurement. Examples of steady-state shear flows or flow birefringence are presented to highlight the non-universality of the behavior with respect to the nature of the substrate or the sheared thickness. Additionally the present development completes and extends the identification of low frequency shear elasticity made at sub-millimeter gaps in various one-component liquids to salt-free aqueous solutions (CTAB-water (Hexadecyl-TrimethylAmmonium Bromide)).

Statistical Analysis of Pulsed Microdischarges and Ozone Generation in Dielectric Barrier Discharges

Pulsed microdischarges produced by dielectric barrier discharges (DBDs) in a submillimeter gap were investigated under 200 cycles of sinusoidal ac voltage at 5 kHz in this paper. The impulsive current in the external circuit was accurately measured by an oscilloscope with a bandwidth of 2.5 GHz and a maximum sampling rate of 40 GS/s to calculate the filamentary current in the discharge gap. The amplitude, pulse duration, and transferred charge of a single filamentary current and the microdischarge energy acquired over the 200 voltage cycles were statistically analyzed for different discharge gaps and gas pressures. The microdischarge parameters and ozone generation efficiencies for different conditions were compared. The ozone production efficiency was found to increase with increasing pressure from 1 to 2 bar absolute, and the gap length from 0.2 to 0.5 mm. The maximum ozone production efficiency achieved in the paper was 217 g/kWh, with a gap length of 0.5 mm, an absolute pressure of 2.0 bar, and an applied voltage of 5.5 kV at 5 kHz.

Error Analysis of Clay-Rock Water Content Estimation with Broadband High-Frequency Electromagnetic Sensors--Air Gap Effect.

Broadband electromagnetic frequency or time domain sensor techniques present high potential for quantitative water content monitoring in porous media. Prior to in situ application, the impact of the relationship between the broadband electromagnetic properties of the porous material (clay-rock) and the water content on the frequency or time domain sensor response is required. For this purpose, dielectric properties of intact clay rock samples experimental determined in the frequency range from 1 MHz to 10 GHz were used as input data in 3-D numerical frequency domain finite element field calculations to model the one port broadband frequency or time domain transfer function for a three rods based sensor embedded in the clay-rock. The sensor response in terms of the reflection factor was analyzed in time domain with classical travel time analysis in combination with an empirical model according to Topp equation, as well as the theoretical Lichtenecker and Rother model (LRM) to estimate the volumetric water content. The mixture equation considering the appropriate porosity of the investigated material provide a practical and efficient approach for water content estimation based on classical travel time analysis with the onset-method. The inflection method is not recommended for water content estimation in electrical dispersive and absorptive material. Moreover, the results clearly indicate that effects due to coupling of the sensor to the material cannot be neglected. Coupling problems caused by an air gap lead to dramatic effects on water content estimation, even for submillimeter gaps. Thus, the quantitative determination of the in situ water content requires careful sensor installation in order to reach a perfect probe clay rock coupling.

Optimizations for optical velocity measurements in narrow gaps

Measuring the flow velocity in small gaps or near a surface with a nonintrusive optical measurement technique is a challenging measurement task, as disturbing light reflections from the surface appear. However, these measurements are important, e.g., in order to understand and to design the leakage flow in the tip gap between the rotor blade end face and the housing of a turbomachine. Hence, methods to reduce the interfering light power and to correct measurement errors caused by it need to be developed and verified. Different alternatives of minimizing the interfering light power for optical flow measurements in small gaps are presented. By optimizing the beam shape of the applied illumination beam using a numerical diffraction simulation, the interfering light power is reduced by up to a factor of 100. In combination with a decrease of the reflection coefficient of the rotor blade surface, an additional reduction of the interfering light power below the used scattered light power is possible. Furthermore, a correction algorithm to decrease the measurement uncertainty of disturbed measurements is derived. These improvements enable optical three-dimensional three-component flow velocity measurements in submillimeter gaps or near a surface.

Transition to detonation of an expanding flame ring in a sub-millimeter gap

Deflagration-to-detonation transition of a flame ring circularly expanding in a 260 μm gap filled with stoichiometric ethylene/oxygen mixtures initially at atmospheric pressure and temperature has been experimentally visualized. The results show that DDT can occur under the influence of wall confinement even for an expanding flame. DDT could be observed at a distance as short as ∼70 mm from the ignition spot, which corresponds to ∼130 μs after the ignition spark voltage breakdown. Velocity overshoot of reaction front velocity exceeding Chapman–Jouguet velocity was characterized. Cell structures were observed on the reaction fronts after DDT occurred. The visualizations also showed that smooth circular flame developed right after ignition quickly evolved into wrinkled flame as the flame ring propagated outwards. Flame propagating velocity was accelerated from ∼600 m/s to ∼1000 m/s during the wrinkled flame stage. A series of local explosion on the flame ring was observed during the DDT process, and resulted in an abrupt surge on reaction front propagation velocity.

Around-the-objective total internal reflection fluorescence microscopy

Total internal reflection fluorescence (TIRF) microscopy uses the evanescent field on the aqueous side of a glass/aqueous interface to selectively illuminate fluorophores within approximately 100 nm of the interface. Applications of the method include epi-illumination TIRF, where the exciting light is refracted by the microscope objective to impinge on the interface at incidence angles beyond critical angle, and prism-based TIRF, where exciting light propagates to the interface externally to the microscope optics. The former has higher background autofluorescence from the glass elements of the objective where the exciting beam is focused, and the latter does not collect near-field emission from the fluorescent sample. Around-the-objective TIRF, developed here, creates the evanescent field by conditioning the exciting laser beam to propagate through the submillimeter gap created by the oil immersion high numerical aperture objective and the glass coverslip. The approach eliminates background light due to the admission of the laser excitation to the microscopic optics while collecting near-field emission from the dipoles excited by the approximately 50 nm deep evanescent field.

Images of Nanosecond Pulse-Driven Low Temperature Atmospheric Pressure Plasma Using Dielectric-Free Parallel Electrodes

Images of intensified charged coupled device and optical emission spectra are presented for a low temperature atmospheric pressure plasma jet, which is pulse-driven with a duration of 350 ns at a frequency of 40 kHz. He gas is injected with a gas flow rate of 5-30 L/min through two parallel electrodes that are exposed to the air and have a submillimeter gap. Driving voltage ranges from 400 to 600 V. The total power consumption is less than 2 W, and the plasma does not transit to an arc mode because of the short pulse duration.

Electrical breakdown of water in microgaps

Experimental and modeling studies on electrical breakdown in water in submillimeter gaps between pin and plane electrodes have been performed. Prebreakdown, breakdown and recovery of the water gaps were studied experimentally by using optical and electrical diagnostics with a temporal resolution on the order of one nanosecond. By using Mach–Zehnder interferometry, the electric field distribution in the prebreakdown phase was determined by means of the Kerr effect. Electric fields values in excess of the computed electric fields, which reach >4 MV cm−1 for applied electrical pulses of 20 ns duration, were recorded at the tip of the pin electrode, an effect which can be explained by a reduced permittivity of water at high electric fields. Breakdown of the gaps, streamer-to-arc transition, was recorded by means of high-speed electrical diagnostics, and through high-speed photography. It was shown, through simulations, that breakdown is initiated by field emission at the interface of preexisting microbubbles. Impact ionization within the micro-bubble's gas then contributes to plasma development. Experiments using pulse–probe methods and Schlieren diagnostics allowed us to follow the development of the disturbance caused by the breakdown over a time of more than milliseconds and to determine the recovery time of a water switch. In order to trigger water switches a trigger electrode with a triple point has been utilized. The results of this research have found application in the construction of compact pulse power generators for bioelectric applications.

Evolution of Discharge Structure in Capacitive Radio-Frequency Atmospheric Microplasmas

Conventional radio-frequency (rf) nonthermal atmospheric plasmas are generated in a millimeter gap. In this Letter, we present a self-consistent numerical study of rf atmospheric microplasmas in a submillimeter gap comparable to their sheath thickness. It is shown that the narrow electrode gap deforms the discharge structure, ultimately removing the bulk-plasma region and disabling electron trapping. Significantly, these properties permit rf atmospheric microplasmas to operate at very high current densities thus simultaneously achieving higher stability and greater chemical reactivity.