This study investigates the electrical properties of a graphene oxide (GO) and nanocellulose (NC) composite using impedance spectroscopy, complemented by thorough characterization through Fourier-transform infrared spectroscopy (FTIR), X-ray photoelectron spectroscopy (XPS), Raman spectroscopy, and scanning electron microscopy (SEM). FTIR analysis revealed characteristic peaks corresponding to functional groups present in both GO and NC, providing insights into their chemical composition. XPS spectra exhibited distinctive peaks indicative of carbon and oxygen bonding states, elucidating the surface chemistry of the materials. Raman spectroscopy provided information on the structural order and defects within the samples, particularly highlighting the graphitic structure of GO. SEM images revealed the morphological features of the composite membrane, showcasing the distribution of NC particles and structural modifications induced by their incorporation. Impedance spectroscopy was utilized to investigate the electrical conductivity of the GO-NC composite. Results indicated a temperaturedependent behavior, with an increase in conductance observed as the temperature rose within the operational range of fuel cells. Remarkably, the addition of NC did not significantly alter the conductive behavior of the composite, suggesting compatibility and stability. In summary, this comprehensive characterization using multiple analytical techniques offers valuable insights into the electrical properties of the GO-NC composite. The findings suggest its potential for various applications requiring enhanced electrical conductivity, particularly in fuel cell technology.