Composite Structures Research Articles

Preparation and formation mechanism of (W) WC/Fe bundle reinforced iron matrix composites

To address the issue of strength and toughness inversion in traditional metal matrix composites, which are reinforced by uniformly distributed ceramic particles, this research developed a novel space bundle configuration of reinforced iron matrix composite using tungsten wire (W) and tungsten carbide (WC). This composite was prepared using a lost foam casting process combined with in-situ reaction. Microstructural analysis revealed that WC particles are distributed along the tungsten wire, with larger particles at the center and smaller ones at the edges. The formation of the reinforcement occurs in two stages: first, a solid-liquid reaction between the solid tungsten wire and molten iron during the lost foam casting process, promoting WC formation at high temperatures and carbon potential; second, an in situ solid-solid reaction where Fe diffuses and Fe3W3C decomposes, forming a composite structure of WC and α-Fe. The composite obtained at 1100°C for 9 hours exhibited a compressive strength of 836.59 MPa and a fracture strain of 18.69%, representing increases of 48.46% and 48.69% respectively compared to grey cast iron (GCI). The (W) WC/Fe bundle reinforcement effectively enhances the strength and toughness of the composite through the high volume fraction and gradient distribution of WC particles, combined with the synergistic effect of α-Fe. This research provides a new strategy for improving the mechanical properties of composite materials and resolving the issue of strength-toughness inversion.

Laser and thermal control over structure and magnetic properties of PrDy-FeCo-B microwires

Magnetic microcombs are necessary in microrobotics, MEMS technologies, actuator and magnetic flow analyzer industries. Usually, magnetic microcombs are artificial linear magnets of periodic shape. We propose another type of microcombs based of microwires, where periodicity of magnetization is caused by equidistant alternation of natural domains. We have demonstrated the presence of quasi-periodic radial magnetization and the effect of temperature and magnetic field on magnetic relief in PrDyFeCoB microwires. Accurate analysis of chemical, phase and structural composition of the microwires allowed us to reveal necessary conditions for the creation of periodical magnetic relief. Annealing affects magnetic relief and changes structure of initially amorphous microwires. Crystal structure of inclusions enriched with Fe and Co instead of Dy and Pr is body-centered cubic (BCC), while the bulk of the microwire has tetragonal structure. We have found laser stimulated amorphization of surface of PrDy-FeCo-B microwires. Partial restoration of the amorphous structure in polycrystalline microwires under single laser pulse of irradiation of 1mJ power and 120 ns duration has been found in 1–2 μm depth.

Fabricating sandwich composite tubes using a new thermal expansion technique: Materials preparation and energy absorption characteristics

The extensive application of hollow composite structures in engineering increasingly demands innovations in highly efficient and economical manufacturing processes as well as materials to achieve lightweighting and enhance mechanical performance. To address the limitations of traditional molding processes in fabricating hollow composite structures with intricate geometries, this study proposes a novel thermal expansion molding technique. This method eliminates the need to remove the mandrel after molding, making it exceptionally suitable for the molding of foam sandwich composite structures. Leveraging this new technique, lightweight sandwich composite tubes filled with polymethacrylimide (PMI) foam and thermal expansion foam were successfully fabricated. Considering the importance of crashworthiness for automotive applications, detailed experimental studies were conducted to investigate the crushing performance of the sandwich composite tubes prepared using this technology. Experimental results reveal that the synergistic effect between the multi-component materials within the sandwich composite tubes confers surprising energy absorption characteristics and crushing stability to the structure. The sandwich composite tubes prepared by this innovative thermal expansion process exhibit promising prospects as crashworthy structures for automotive lightweighting applications, and this method provides critical inspiration for the fabrication of composite structures with complex shapes.

Arbuscular mycorrhizal fungi affected soft wheat quality properties and nutritional index by regulating the composition and secondary structure of protein

Arbuscular mycorrhizal fungi (AMF) inoculation has important regulatory influence on plant growth and nitrogen uptake, which are intimately associated with soft wheat yield and quality. The study aimed to investigate the impact of AMF inoculation on soft wheat grain yield, protein compositions, protein quality, secondary structure of gluten, dough properties and biscuits baking quality. In this study, AMF inoculation significantly increased grain yield. AMF inoculation decreased grain protein content by 5.1%, glutenin content by 8.5%, GMP by 14.3%, and HMW-GS by 8.8% compared with CK. Conversely, AMF inoculation increased the ratio of gliadin/glutenin. Further analysis showed AMF treatment had a looser gluten network than CK, significantly reduced β-sheet and β-turn content, while α-helix content increased. The nutritional index of grain protein was slightly reduced under AMF inoculation, yet the biological value was improved. Reduced wet gluten content, gluten performance index and dough development time under AMF treatment through regulation of soft wheat protein composition and gluten protein structure. Therefore, biscuits in AMF treatment showed reduced thickness, hardness, significantly greater spread ratio and sensory score compared with CK. These indicate that AMF application would be a beneficial agronomic practice to synergistically optimize yield and grain quality in soft wheat.

Effectiveness of Computer Application in Improving Reading Skills in Chinese Language and Towards Post-Attitudes as Home-based Learning

Background: As technology continues to advance, language acquisition methodologies have increasingly been integrated into computer-assisted language learning (CALL) systems. In the context of Chinese language acquisition, characters are structured in three phases: the overall character, its components, and its strokes. Proficiency in identifying and distinguishing individual characters hinges upon understanding their structural composition. Objective: This study aims to explore the impact of a computer application on Chinese language reading skills and students' perceptions regarding the utilization of computer applications for home-based learning. Method: A total of 60 students engaged in home-based learning using a designated computer application were involved in the study. Employing a quantitative approach with a quasi-experimental design, the study assessed the effects of the intervention. Results and Conclusion: Following one month of home-based learning through computer applications, participants exhibited higher gain scores in reading skill tests, albeit the differences were not statistically significant. Students expressed a preference for and perceived greater ease in acquiring reading skills through computer applications compared to traditional methods. Furthermore, the integration of computer applications in teaching and learning processes demonstrated the potential to enhance students' motivation, interest, and confidence in language acquisition, albeit without a notable impact on attention levels. The study underscores the pedagogical promise of Computer-Assisted Language Learning (CALL) and advocates for further research endeavors in this domain.

Concerns and Safety Evaluation Indicators for Compatibility Study of Injections with Prefilled Syringe

Abstract: Prefilled syringe is a multi-component injector drug packaging system in which liquid drugs are directly loaded for direct use by patients. It has two functions, drug storage and regular injection, which belongs to high-risk pharmaceutical packaging containers. In recent years, more and more injections have been packaged with prefilled syringes worldwide. However, no guidelines about compatibility of chemical injections and prefilled syringes was set up. In current review, studies related to the compatibility study was summarized. Structural composition, material composition and production technology are analyzed first. After that, extraction test, interaction study and safety study are summarized. Glass components, plastic components, seal elastomer components, other components and materials, adsorption test and physical properties are the main focusing points. Based on the studies mentioned above, together with the results of extraction test, migration test and adsorption test, safety evaluation indexes could be formed. The current review aims to provide strategies for the setting up of compatibility study guidelines.

КЕРАМИКАЛЫҚ ЖОЛ ТӨСЕНІШТЕРДІ ӨНДІРУДЕГІ КЕРАМИКАЛЫҚ МАССА КОМПОЗИЦИЯСЫН ЖЕТІЛДІРУ

The article presents the results of a study of the chemical and mineralogical composition of the raw material components in the ceramic mass and provides techniques for the technology of laying ceramic material by vibropressing using talc rock in the mass and methods for determining the composition of clay raw materials. Formulations for the production of ceramic road surfaces, taking into account the factors of preference for mixtures to improve the properties of the finished product as a molding, drying and ceramic material, have been studied in two different components. It was found that the introduction of talc into the ceramic composition has an effect on the formation of high-temperature augite and amphibole phases and the intensification of the formation of minerals in clay, on the formation of high-temperature phases - sanidine, ackermanite elements. This process leads to an increase in the physical and mechanical properties of the resulting samples.The main patterns of formation of the structure and phase of ceramic compositions by firing in the temperature range 1000оC-1100оC were studied by isothermal control.In this pattern, sintering processes with solid and solid liquid-phase syntheses were carried out to ensure the phase - mineral composition, the study clarified the production of high-strength and frost-resistant ceramic pavement. In order to be used in the improvement of the city territory (sidewalks, alleys, park areas, playgrounds, etc.), the possibility of obtaining ceramic road surfaces that meet environmental and operational requirements has been proven. It has been established that one of the priority properties of ceramic road surfaces is a significant abundance of their porosity (25-30%), which allows you to quickly absorb moisture from precipitation (rain, sleet, etc.) and filter water through the body into the ground.Such properties of ceramic paving stones prevent the accumulation of moisture on the surface of the roadway and create comfortable conditions during pedestrian movement, reducing the likelihood of ice formation on the surface of the paving stones in the cold season.

Effects of Varying Nano-Montmorillonoid Content on the Epoxy Dielectric Conductivity

This study investigates the correlation between the interface structure and macroscopic dielectric properties of polymer-based nanocomposite materials. Utilizing bisphenol-A (BPA) epoxy resin (EP) as the polymer matrix and the commonly employed layered phyllosilicate montmorillonoid (MMT) as the nanometer-scale dispersive phase, nano-MMT/EP composites were synthesized using composite technology. The microstructure of the composite samples was characterized through XRD, FTIR, SEM, and TEM. Changes in the morphology of the nanocomposite interface were observed with varying MMT content, subsequently impacting dielectric polarization and loss. Experimental measurements of the dielectric spectrum of the nano-MMT/EP were conducted, and the influence of the material interface, at different nano-MMT contents, on the dielectric relaxation was analyzed. The study delves into the effect of the nanocomposite interface structure on ion dissociation and migration barriers, exploring the ionic conductivity of nano-MMT/EP. Lastly, an analysis of the impact of different nano-MMT contents on the dielectric conductivity is presented. From the experimental results, the arranging regularity of polymer molecules in the interface area raises. In the matrix, the ion migration barriers decrease significantly. The higher the MMT content in the interface, the lower the migration barrier is. Until the MMT content exceeds the threshold, the agglomerated micro-particles form, which decreases the polymers’ space distribution regularity, and the ions migration barrier raises. According to the changes in the rule of the ions migration barrier with the composite interface structure content, the reason for dielectric conductivity changes can be judged.

Electrically switchable behavior in coupled EIT-like meta-molecule and Fabry-Pérot cavity

Abstract In this paper, we propose a microstrip Fabry-Pérot (FP) cavity embedded with an active electromagnetically-induced-transparency-like (EIT-like) meta-molecule to investigate the electrically switchable behavior. The phenomenon of EIT is achieved by coupling a “bright” comb-line resonator with a “dark” split-ring resonator. The FP cavity is fabricated by etching two narrow slots on a microstrip line. With two different resonance mechanisms working together, the proposed composite EIT-cavity design is shown to exhibit the enhanced EIT-like transmission characteristics, accompanied by two sharp Fano-type line-shapes. By incorporating PIN diodes into the composite EIT-cavity structure, we can dramatically modulate the transmission spectrum via external DC voltage. In particular, we show the multi-band unity modulations through biasing the proposed active samples. Moreover, the slow light on-to-off switching processes are also obtained with modifying the state of PIN diode from dielectric to conductive. Our results may open important opportunities for fabricating dynamic functional photonic devices in the future.

Sedimentary exhalative Pb-Zn deposit model of the Ban Lin – Phia Dam ore range, Vietnam

Purpose. The aim of this study is to construct a typical ore model for Pb-Zn ore range in Ban Lin – Phia Dam and to compare it with the existing ones. The model is constructed based on three main elements of the mineral generation process, such as formation environment, generated-ore fluid source, and deposited-ore mechanism. The obtained results are aimed at determining and predicting the resource of sedimentary exhalative (SEDEX) Pb-Zn ore deposit in Vietnam. Methods. To comprehend the characteristics of the SEDEX Pb-Zn ore deposits in the Ban Lin – Phia Dam area, we employ a combination of approaches that include mineralography to determine the composition and tectonic structure of rocks and ore, inclusion analysis to determine the temperature and inclusion composition, Pb isotopic analysis and stable S isotopic analysis to explore the environment and sources of ore-forming materials. Findings. The sedimentary exhalative (SEDEX) Pb-Zn ore deposit arises from the dissolution of metal-rich salt deposits due to heating at shallow depths (several kilometers). Subsequently, this fluid migrates through faults and fractures to preferred locations where galena and sphalerite precipitate alongside sedimentary basin deposition. Originality. SEDEX ore deposits have been extensively studied in various regions of the world. Although there are multiple theories regarding their origin, including explosion, biological debris accumulation, and surface replacement, each model has its own distinct advantages and limitations in explaining the genesis and development of SEDEX ore deposits. Practical implications. The acquired findings are intended to identify and predict the resources of sedimentary exhalative Pb-Zn ore deposits in Vietnam.

Tuning ferroelectric domains and polarization properties of flexible BiFeO3 thin films by phase transition engineering

In the present investigation, thin films of flexible (Bi1-xSmx)(Fe0.95Mn0.05)O3 (denoted as BSFM0, BSFM4, BSFM8, and BSFM12 for x=0 %, 4 %, 8 %, and 12 %, respectively) were synthesized on metallic Ni-Cr substrates via the sol-gel technique. A comprehensive examination was conducted to elucidate the influence of varying concentrations of Sm3+ substitution on the phase constitution, oxygen vacancy concentration, and leakage behavior of the (Bi1-xSmx)(Fe0.95Mn0.05)O3 films. Utilizing X-ray diffraction (XRD) and Raman spectrometry, it was ascertained that all films exhibited a composite structure comprising orthorhombic (Pnma) and rhombohedral (R3c) phases. An augmentation in Sm3+ doping led to a non-monotonic variation in the R3c phase content, initially increasing and subsequently decreasing, while the nonpolar Pnma phase demonstrated a progressive enhancement. The distorted R3c phase was found to promote the flipping of the domain architecture, thereby augmenting the polarization attributes. Notably, at a Sm doping level of 4 %, the maximum polarization (Pmax) attained was 95 μC/cm2, with a remnant polarization (Pr) of 78 μC/cm2. The incorporation of a judicious amount of Sm was observed to curtail film leakage and decelerate the aging phenomenon. The compositional stability of this doping level was evaluated across a frequency spectrum of 0.1–12 kHz and a temperature gradient of 25–200 °C, revealing no propensity for degradation under conditions of polarization, a holding duration of 104 s, or fatigue scenarios involving a curvature of 5 mm and 108 switching cycles subjected to 103 instances of bending. These findings provide innovative insights for the development of next-generation lead-free transducer apparatus and flexible information storage mediums.

Robust topology optimization of multi-material structures with overhang angle constraints using the material field series-expansion method

This paper presents a novel topology optimization method to enhance the manufacturability and practicality of multi-material structures. Traditional topology optimization techniques excel at generating high-performance designs, but the performance of these designs is often compromised due to the load perturbations encountered in real-world applications or post-processing for additive manufacturing (AM). This work addresses this challenge by incorporating three key features directly into the optimization process. First, the method integrates overhang angle constraints, ensuring designs are inherently manufacturable with AM. Second, it utilizes the material field series-expansion method for a significant reduction in design variables while simultaneously providing a clear and efficient description of material distribution within the optimized designs. Finally, to enhance design robustness under real-world scenarios with uncertain loads, the method employs Monte Carlo simulation, which is decoupled from the optimization process to reduce the computational cost. Numerical examples demonstrate the efficiency and effectiveness of the proposed method in generating robust designs of multi-material structures well-suited for AM. The proposed framework offers a promising pathway for the realization of complex, high-performance composite structures.

Herbivore regulation of savanna vegetation: Structural complexity, diversity, and the complexity–diversity relationship

AbstractLarge mammalian herbivores exert strong top‐down control on plants, which in turn influence most ecological processes. Accordingly, the decline, displacement, or extinction of wild large herbivores in African savannas is expected to alter the physical structure of vegetation, the diversity of plant communities, and downstream ecosystem functions. However, herbivore impacts on vegetation comprise both direct and indirect effects and often depend on herbivore body size and plant type. Understanding how herbivores affect savanna vegetation requires disaggregating the effects of different herbivores and the responses of different plants, as well as accounting for both the structural complexity and composition of plant assemblages. We combined high‐resolution Light Detection and Ranging (LiDAR) with field measurements from size‐selective herbivore exclosures in Kenya to determine how herbivores affect the diversity and physical structure of vegetation, how these impacts vary with body size and plant type, and whether there are predictable associations between plant diversity and structural complexity. Herbivores generally reduced the diversity and abundance of both overstory and understory plants, though the magnitude of these impacts varied substantially as a function of body size and plant type: only megaherbivores (elephants and giraffes) affected tree cover, whereas medium‐ and small‐bodied herbivores had stronger effects on herbaceous diversity and abundance. We also found evidence that herbivores altered the strength and direction of interactions between trees and herbaceous plants, with signatures of facilitation in the presence of herbivores and of competition in their absence. While megaherbivores uniquely affected tree structure, medium‐ and small‐bodied species had stronger (and complementary) effects on metrics of herbaceous vegetation structure. Plant structural responses to herbivore exclusion were species‐specific: of five dominant tree species, just three exhibited significant individual morphological variation across exclosure treatments, and the size class of herbivores responsible for these effects varied across species. Irrespective of exclosure treatment, more species‐rich plant communities were more structurally complex. We conclude that the diversity and architecture of savanna vegetation depend on consumptive and nonconsumptive plant–herbivore interactions; the roles of herbivore diversity, body size, and plant traits in mediating those interactions; and a positive feedback between plant diversity and structural complexity.

Damage identification in composite structures using high-speed 3D digital image correlation and wavelet analysis of mode shapes

ABSTRACT In this study, the damage identification procedure combining the advantages of high-speed 3D digital image correlation (DIC) that is used for modal analysis and wavelet-based processing algorithm is presented. The proposed procedure has been successfully validated on sandwich composite structures with internal damage of a core and impact damage, and its performance was demonstrated by detection, localisation, and identification of shapes of damage in tested structures, comparable to the results from scanning laser Doppler vibrometry (SLDV). The effectiveness in damage identification was achieved by the development of processing algorithm of acquired mode shapes, which uses a 2D double-density directional wavelet transform with increased sensitivity with entropic weights allowing to automatically select those wavelet coefficients and mode shapes, which are most sensitive to damage. The procedure presented in this paper demonstrates the performance of 3D DIC for damage identification as a cost-effective alternative to the procedures based on SLDV measurements.

Experimental study on shear mechanism of a new TU-type connector at HSS-UHPC interface

To maximize the benefits of high-strength steel (HSS) and ultra-high performance concrete (UHPC) composite structures, proper connections at HSS-UHPC interfaces are essential. Due to the significant variations in material strengths and component dimensions, traditional shear connectors could be unsuitable for HSS-UHPC interfaces. This study proposes a new TU-type connector (T-shaped rib with U-shaped holes), which has the advantages of high shear and tensile capacity, good slip capacity, low height limitation, and easy installation. Firstly, eighteen push-out tests of HSS TU-type connectors embedded in UHPC were performed to investigate the effect of connector heights and the contribution of connector flanges. The failure process, including the yielding of hole walls, the fracture of connector webs, and the development of fracture surfaces was discussed. Besides, the microstructures involving smooth areas, lamellar structures, and dimples on the fracture surfaces were presented by scanning electron microscope (SEM), and the effect of flange foam blocks on the out-of-plane displacements of UHPC slabs was investigated by digital image correlation (DIC). Secondly, the shear force–displacement curves and the load–strain relations of steel plates and rebars were discussed. In addition, the effects of considered parameters on shear capacity, peak slips, and shear stiffness were investigated. Finally, a strut-and-tie model was established to reveal the shear mechanism of TU-type connectors. Based on the principle of virtual work, the shear capacity equations of TU-type connectors were proposed.

Origin and characteristics of collapsible soils state of the art report

This study establishes a foundational framework addressing challenges, implications, and potential remedies related to collapsible soils. Serving as a cornerstone for global exploration, it emphasizes the importance of understanding geological, structural, and mechanical characteristics for early identification and proactive mitigation. The study underscores the significance of preventing structural damages in regions prone to collapsible soils, discussing their diverse types and origins, structural composition, and mechanical behavior. A detailed exploration highlights their prevalence in semi-arid and arid regions, emphasizing distinct geological features associated with their occurrence.

Controllable Synthesis of Hollow Dodecahedral Si@C Core-Shell Structures for Ultrastable Lithium-Ion Batteries.

Silicon (Si) has attracted considerable attention as a promising alternative to graphite in lithium-ion batteries (LIBs) because of its high theoretical capacity and voltage. However, the durability and cycling stability of Si-based composites have emerged as major obstacles to their widespread adoption as LIBs anode materials. To tackle these challenges, a hollow core-shell dodecahedra structure of a Si-based composite (HD-Si@C) is developed through a novel double-layer in situ growth approach. This innovative design ensures that the nano-sized Si particles are evenly distributed within a hollow carbon shell, effectively addressing issues like Si fragmentation, volume expansion, and detachment from the carbon layer during cycles. The HD-Si@C composite demonstrates remarkable structural integrity as a LIBs anode, resulting in exceptional electrochemical performance and promising practical applications, as evidenced by tests in pouch-type full cells. Notably, the composite shows outstanding cycling stability, retaining 85% of its initial capacity (713 mAh g-1) even after 3000 cycles at a high current rate of 5000mA g-1. Additionally, the material achieves a gravimetric energy density of 369Wh kg-1, showcasing its potential for efficient energy storage solutions. This research signifies a significant step toward realizing the practical utilization of Si-based materials in the next generation of LIBs.

Bioinspired surface modification of mussel shells and their application as a biogenic filler in polypropylene composites

This study explores the potential of mussel shells (MS) as biogenic fillers in polymer composites. The chemical composition and crystal structures of MS were characterised. To improve MS filler dispersion and adhesion within a polypropylene (PP) matrix, three surface modification methods were evaluated: polydopamine (PDA) coating, maleic anhydride-grafted polypropylene (MAPP) modification, and PDA/MAPP co-modification. The PDA coating, inspired by the adhesive properties of mussel foot proteins, successfully functionalized the MS surface, as confirmed by X-ray photoelectron spectroscopy (XPS). Thermodynamic analysis, based on contact angle measurements, revealed that MAPP and PDA/MAPP modifications reduced surface energies and potential energy differences. These changes enhanced filler dispersion and interfacial bonding by increasing hydrophobicity and reducing agglomeration in the PP matrix. Consequently, PP composites with 20% PDA/MAPP-modified MS fillers exhibited a 2.9% increase in tensile strength and a 7.5% increase in flexural strength compared to neat PP. Scanning electron microscopy (SEM) also showed reduced filler-matrix debonding and fewer voids. The proposed mechanism attributes these macroscopic property enhancements to the ability of the PDA coating to facilitate chemical and hydrogen bonding between MS fillers and MAPP.

Evolution characteristics and molecular constraints of microbial communities during coal biogasification.

This study investigates the production of biomethane, and variation in microbial community and coal molecular structures using gas chromatography, 16S rRNA high-throughput sequencing and Fourier transform infrared spectroscopy. Additionally, the factors influencing microbial community structure at a molecular level are discussed. The results demonstrate that bituminous coal exhibits a higher biomethane yield than anthracite coal. In bituminous coal samples, Escherichia and Proteiniphilum are the predominant bacteria at day 0, while Macellibacteroides dominates from days 5 to 35. Methanofollis is the dominated archaea during days 0 to 15, followed by Methanosarcina on day 35. In anthracite coal samples, Soehngenia is the dominant bacterial genus at day 0; however, it transitions to mainly Soehngenia and Aminobacterium within days 5-15 before evolving into Acetomicrobium on day 35. Methanocorpusculum is predominantly found in archaeal communities during days 0-15 but shifts to Methanosarcina on day 35. Alpha diversity analysis reveals that bacterial communities have higher species abundance and diversity compared to archaeal communities. Redundancy analysis indicates a significant correlation between coal molecular structure and bacterial community composition (P value < 0.05), whereas no correlation exists with archaeal community composition (P value > 0.05). The research findings provide theoretical support for revealing the biological gasification mechanisms of coal.

Development of sustainable flame-retardant bio-based hydrogel composites from hemp/wool nonwovens with chitosan-banana sap hydrogel

Flame retardant (FR) finishing is crucial for developing protective textiles, traditionally relying on halogen, phosphorus, and phosphorus-nitrogen chemistries, which have limitations like toxicity and fabric stiffening. Innovative approaches such as nanotechnology, plasma treatments, and natural resource-based finishes are being explored to achieve sustainable FR textiles. This study presents the development and comprehensive characterization of hydrogel composites made from nonwoven fabrics composed of various hemp/wool blends (70/30, 80/20, and 90/10). The nonwoven fabrics were treated with a chitosan hydrogel incorporating banana sap to enhance their properties. Scanning electron microscope (SEM) examined the surface morphology and structural integrity of the composites, while Fourier transform infrared spectroscopy (FTIR) identified chemical interactions and functional groups. Differential scanning calorimeter (DSC) revealed thermal properties, water absorbency tests demonstrated hydrophilicity, mechanical testing assessed tensile strength, and vertical flammability tests evaluated fire resistance. SEM and FTIR revealed a successful coating of chitosan hydrogel with banana sap inclusions onto the hemp/wool nonwoven fabric, forming a composite structure. DSC analysis suggests higher chitosan content and hemp fiber ratio (like 70/30) lead to increased thermal stability of hydrogel composites. Higher chitosan concentrations in the hydrogel significantly improve the flame-retardant properties of hemp/wool nonwoven fabrics by reducing char length and enhancing protective char layer formation, with banana sap further promoting charring. These results indicate that the developed composite can be effectively used in flame-retardant textiles.