Stress Creep Research Articles

OXFORD-UMAT: An efficient and versatile crystal plasticity framework

The crystal plasticity-based finite element method is widely used, as it allows complex microstructures to be simulated and allows direct comparison with experiments. This paper presents the OXFORD-UMAT for Abaqus®, a novel crystal plasticity code that is publicly available online for researchers interested in using crystal plasticity. The model is able to simulate a wide range of materials and incorporates two different solvers based on the solution of slip increments and Cauchy stress with variants of state update procedures including explicit, semi-implicit, and fully-implicit for computational efficiency that can be set by the user based on the application. Constitutive laws are available for a range of materials with single or multiple phases for slip, creep, strain hardening, and back stress. The model includes geometrically necessary dislocations that can be computed using finite element interpolation functions by four alternative methods, including the total form with and without a correction for the dislocation flux, a widely used rate form, and a slip-gradient formulation. In addition, the initial strengthening and subsequent softening seen in irradiated materials can also be simulated with the model. The analysis is available in 2D (plane stress and plane strain) and 3D, including linear and quadratic elements. Here we include full derivations of the key equations used in the code and then demonstrate the capability of the code by modeling single-crystal and large-scale polycrystal cases. Comparison of OXFORD-UMAT with other available crystal plasticity codes for Abaqus® reveals the efficiency of the proposed approach, with the backup solver offering greater versatility for handling convergence issues commonly found in practical applications.

Creep stress analysis of functionally graded transversely isotropic piezoelectric disc with variable thickness under rotation

Materials exhibiting different piezoelectric properties throughout their volume are referred to as functionally graded piezoelectric materials (FGPM). Due to their graded composition, the characteristics of these materials can be customized to fit particular needs in a variety of applications. Functionally graded piezoelectric materials are beneficial in many technical applications because of their versatility that enables increased performance, efficiency, and adaptability in a variety of disciplines. The objective of the current study is to analyse creep stresses in an annular disc composed of transversely isotropic, functionally graded piezoelectric material with varying thickness parameters. Creep stresses are evaluated analytically using the approach of Seth's transition theory. By using the stress-strain relations, the equations for mechanical stresses and electrical displacement are determined. Substituting these relations into the equilibrium equation a nonlinear differential equation is obtained. The findings are presented both numerically and graphically, demonstrating how the thickness parameter affects the circumferential stresses in the intermediate surface of the rotating disc. The disc made of transversely isotropic piezoelectric material PZT-4 exhibits higher creep stresses than other materials under consideration according to all of the numerical discussions and calculations. This work may provide an effective methodology for the analysis of functionally graded piezoelectric rotating discs and contribute to theoretical research and engineering applications.

Evaluation of the off‐axis and on‐axis tensile creep behavior of glass‐fiber reinforced polymer unidirectional lamina

AbstractThe off‐axis creep behavior of glass‐fiber reinforced polymer (GFRP) unidirectional lamina is crucial for engineering structural applications. A unified prediction model for time‐dependent off‐axis and on‐axis tensile creep strain in GFRP lamina is developed. The model, analogous in form to the one‐parameter plasticity model, accounts for off‐axis creep deformation separately for elastic and plastic response stages, incorporating a correction term to describe on‐axis creep deformation. The accuracy of the model is confirmed through tensile creep tests on unidirectional lamina at angles of 0, 15, 30, 45, 60, and 90 degrees. The model successfully predicts of creep deformation in the elastic and plastic response stages, respectively. The effects of creep stress, creep time, and off‐axis angle on the creep behavior are investigated. The optimal test angles for predicting off‐axis creep behavior using only two off‐axis angles' creep tests are analyzed. The dominant factors of creep behavior at various off‐axis angles are evaluated. The findings of the study include recommendations for lay‐up configuration and engineering applications of GFRP composites.Highlights A unified creep strain prediction model for GFRP lamina was developed. Creep strain was calculated separately in elastic and plastic response stages. The link between stress, time, angle and creep behavior was determined. The optimal test angles for predicting off‐axis creep behavior were evaluated.

Effect of waste crab shell powder on matrix asphalt

Abstract In order to solve the problems of depleting petroleum asphalt resources and deteriorating pollution of marine products, a systematic study was carried out on the application prospect of waste crab shell (WS) powder as asphalt modifier. In this study, the physical properties of WS powder modified asphalt (WSA) were tested by blending different contents of WS powder into matrix asphalt; the high and low temperature rheological properties of WS powder modified asphalt were characterized by using Dynamic shear rheometer, Bending beam rheometer, and Multiple stress creep recovery test. In addition, the microscopic chemical properties and modification mechanism were analyzed by Differential scanning calorimetry, Fourier transform infrared spectroscopy, Atomic force microscopy, and Scanning electron microscope. It was shown that the WS powder enhanced the viscoelastic properties, temperature sensitivity properties, and permanent deformation resistance of asphalt. In addition, there was no obvious chemical reaction between the WS powder and the matrix asphalt, and no new chemical substances were generated; at the microscopic level, the WS powder and the matrix asphalt had good compatibility. In conclusion, the use of WS powder as a bio-based asphalt modifier to improve the resources and environmental issues have certain prospects.

Shear creep deformation of rock fracture distrubed by dynamic loading

The long-term stability of jointed rock masses is usually dominated by fault activation, which may be triggered by the dynamic disturbance generated by blasting during mining activities, leading to the occurrence of disasters such as landslides in open-pit and rockbursts in deep mining. The initial stress and dynamic disturbance are key factors that strongly affect the shear creep behavior of rock fractures. In this work, the shear failure instability of rock fractures of sandstone under creep-impact loading was experimentally investigated by using a creep-impact test machine, which allows for applying creep loading and an additional dynamic disturbance on rock fractures. Three stages of shear creep deformation, creep strain rate, and time-to-failure are examined under different creep stress levels and impact energies. Experimental results show that the tangential and normal creep rates increase with the increase of creep stress and impact energy, but the increment of tangential creep rate is higher than that of the normal creep rate. The time-to-failure of the creeping specimen is shortened under high creep stress and large impact energy, while the time-to-failure after the last dynamic disturbance of the specimen is determined by the total impact energy and creep stress level. By using high-speed photography, it is found that the failure types of rock depend on the magnitude of impact energy and creep stress level; that is, rock mainly slides with low stress levels and shears off with high stress levels. In addition, under different impact energy and creep stress levels, the variation of height is between 0.38 and 0.52, while the defined fracture factor, which describes the degree of failure of serrations, is between 0.30 and 0.54. The findings can provide deep insight into the fault sliding mechanism caused by mining activities, which provides theoretical support for the safe mining of ore in fault fracture zones.

Assessing pavement characteristics: An in-depth evaluation of waste engine oil and Buton rock asphalt composite modified asphalt and its mixture

To investigate the cooperative influence of waste engine oil (WEO) and Buton rock asphalt (BRA) on asphalt characteristics, the WEO/BRA composite modified asphalt and its mixture with varied dosages were prepared. The high-, moderate-, and low-temperature assessments of WEO/BRA composite modified asphalt were conducted through temperature sweep tests, multiple stress creep and recovery (MSCR), and bending beam rheometer (BBR) tests. The softening point difference was used to analyze the storage stability of composite modified asphalt. Based on the Fourier transform infrared spectroscopy (FTIR) and fluorescence microscope (FM) test, the microscopic feature and chemical constitution of WEO/BRA composite modified asphalt were analyzed. Rutting test, low-temperature bending test, immersed Marshall test, freeze-thaw splitting test, and four-point fatigue bending test were carried out to verify the pavement properties of the WEO/BRA composite modified asphalt mixture. The results indicated that WEO improved the capability in low-temperature conditions and fatigue properties of asphalt modified with BRA. BRA enhanced the high-temperature property of asphalt modified with WEO. The synergistic effect of WEO, BRA, and neat asphalt was a physical reaction, and these modifiers were uniformly distributed in the asphalt. Meanwhile, WEO/BRA composite modified asphalt had excellent storage stability for the single modified asphalt. The test results of the asphalt mixture verified the results, indicating that WEO/BRA composite modified asphalt can be considered a new green and durable asphalt pavement material.

Extraction solvents effect on asphalt binder properties

Asphalt industries are actively pursuing the integration of recycled asphalt pavement (RAP) into their constructions to promote sustainable pavement solutions amidst resource scarcity. However, challenges persist in the extraction and recovery processes, potentially affecting asphalt pavement performance assessments. This study investigates the impact of three common solvents—n-propyl bromide (nPB), trichloroethylene (TCE), and a toluene-ethanol blend (85 %/15 %)—on the rheological properties of recovered binders, particularly aiming to identify a substitute for TCE in light of its proposed ban by the Environmental Protection Agency (EPA) in the USA. Tests were conducted on six different performance-graded (PG) binders from diverse sources, assessing high-temperature properties using Dynamic Shear Rheometer (DSR) and Multiple Stress Creep Recovery (MSCR) tests, as well as low-temperature properties via Bending Beam Rheometer (BBR). Fourier Transform Infrared (FTIR) spectroscopy confirmed the absence of solvents in the recovered binders. Although minor variations were observed in measured properties between original and recovered binders due to solvent use, these differences did not affect the resulting performance grades. Thus, the toluene-ethanol blend can potentially substitute for TCE. However, it is noteworthy that the toluene-ethanol blend (85 %/15 %) displayed a slower solubility rate compared to nPB and TCE, underscoring the need for caution in its usage.

Functional and rheological investigations on hydrophilic nanoclay blended bitumen

Functional and rheological characteristics are two essential criteria for the success of any modifiers for the modification of bitumen. Recently, nanoclay has grabbed extensive attention as a key solution for enhancing the performance of bitumen. This study focuses on evaluating the dispersion, storage stability, high-temperature performance, and aging resistance potential properties of bitumen VG-30 modified with montmorillonite bentonite hydrophilic nanoclay (NC). Various proportions (0, 2, 4, 6, and 8% by weight of bitumen) of NC were blended with VG-30 using a high shear mixer (HSM). Various performance assessments, including kinematic viscosity by Brookfield Rotational Viscometer (BRV), multiple stress creep recovery (MSCR), high-temperature performance grade (PG), frequency sweep along with scanning electron microscopy (SEM) were conducted. SEM images and viscosity data analysis show that dispersion problem arises beyond 6% of NC addition while phase separation is in the acceptable range. Further, considerable increment in Superpave rutting parameter (G*/Sinδ) and recovery percentage (%R), and decrease in non-recoverable compliance (Jnr) was seen, resulted up to 30% improvement in rutting performance of the bitumen. Furthermore, the potential for aging resistivity resulted a significant drop in aging index (AI) values, suggesting that introducing NC to bitumen could significantly improve aging resistivity. Moreover, rheological approaches can be helpful to understand temperatures and frequency dependent aging behaviours of bitumen.

Determination of uniaxial creep properties using equivalent factors by sharp indentation

The uniaxial creep properties, including the creep coefficient and stress exponent, are crucial to characterize the creep behavior of materials. Instrumented sharp indentation test (ISIT) is a non-destructive technique to characterize the uniaxial creep properties using the stress equivalent factor and strain rate equivalent factor. However, the strain hardening exponent of tested material is ignored in the contact model, leading to inaccurate estimation of uniaxial creep coefficient. Based on finite element simulations, the effects of the strain hardening exponent on equivalent factors were investigated. The relationships between the equivalent factors, the strain hardening exponent, and the yield strain were established. Indentation and uniaxial tests on Pb95Sn5 and Sn99Cu1 were conducted to validate the established equivalent factors. Then those factors were used to determine the uniaxial creep coefficient of Pb95Sn5 and Sn99Cu1 by ISIT. This work demonstrates the feasibility of measuring uniaxial creep properties of work hardened material by ISIT.

Exploring the physicochemical and rheological properties of sustainable asphalt binders modified with lignin and high-viscosity additive

The primary objective of this investigation is to evaluate how the incorporation of lignin and high-viscosity modifiers impacts the performance of asphalt binders. Lignin-modified asphalt binder (LBA) and lignin-high viscosity modifier composite-modified asphalt binder (LHA) were created by blending 5 % and 15 % lignin, respectively. To understand the physicochemical interactions, Fourier transform infrared spectroscopy (FTIR), thermogravimetric analysis (TGA), and differential scanning calorimetry (DSC) were employed to analyze functional groups, thermal properties, and phase changes. Additionally, the linear rheological behavior and nonlinear rheological behavior were evaluated through frequency sweep and multiple stress creep recovery tests. The findings suggest that lignin blends physically with the asphalt binder and high-viscosity modifier without a chemical reaction. Although the onset pyrolysis temperature of lignin is significantly lower than that of asphalt binders, due to its relatively low content, the thermal decomposition of lignin-modified asphalt binders is primarily controlled by the asphalt binder itself and still exceeds the construction temperature. However, lignin incorporation increases the asphalt binder's glass transition temperature, potentially affecting low-temperature performance. Lignin significantly enhances the modulus in the high-frequency region of both unmodified and high-viscosity modified asphalt binder. However, it has a negative effect on the modulus in the low-frequency region of high-viscosity modified asphalt binder. Furthermore, nonlinear creep recovery test results demonstrate that lignin positively contributes to the deformation resistance of unmodified asphalt binder in a content-dependent manner, whereas it reduces the elastic behavior and deformation resistance of high-viscosity modified asphalt binder. In addition, low levels of lignin increase the stress sensitivity of binders, while high levels of lignin decrease it. Despite these effects, the performance of lignin and high-viscosity additive composite-modified asphalt binder remains superior to that of unmodified asphalt binder. These findings offer valuable insights into the combined use of lignin and polymers in asphalt binder modification.

Waste coffee biochar and bi-oil composite modified rejuvenated asphalt: Preparation, characterization, and performance evaluation

In the realm of sustainable road construction, bio-oil has emerged as a promising and eco-friendly alternative for rejuvenating aged asphalt. Nevertheless, challenges arise due to poor stability, diminished performance at elevated temperatures, and limited anti-aging properties. This study introduces an innovative approach by blending biochar, obtained from the pyrolysis of waste coffee grounds, into bio-oil to create a composite modified regenerator. Initially, the study conducts a microscopic characterization of the biochar using X-ray diffraction (XRD), scanning electron microscopy (SEM), and energy-dispersive X-ray spectroscopy (EDS). Subsequently, the rheological properties of this composite rejuvenated asphalt are evaluated across low, moderate, and high-temperature ranges using bending beam rheometer (BBR), linear amplitude sweep (LAS), and multiple stress creep and recovery (MSCR) tests. Departing from the traditional emphasis on initial property restoration, it further delves into performance alterations after re-aging of rejuvenated asphalt through temperature sweep (TS) and Fourier transform infrared spectroscopy (FTIR) tests, providing a comprehensive assessment of the anti-aging characteristics of rejuvenated asphalt. Additionally, gel permeation chromatography (GPC) is employed to quantitatively analyze the changes in asphalt molecular weight distribution. The microscopic characterization reveals the development of a rough and porous structure within the biochar, facilitating enhanced adhesion and interaction between the rejuvenator and the asphalt binder. Moreover, bio-oil rejuvenated asphalt exhibits excellent low-temperature crack resistance and moderate-temperature fatigue resistance. Following the incorporation of biochar, notable enhancements in high-temperature rutting resistance and anti-aging properties are observed, validating the efficacy of the biochar with bio-oil composite modified regenerator. To achieve optimal performance outcomes, a biochar content of 6 % (as a proportion of aged asphalt), corresponding to a 1:1 ratio of biochar to bio-oil, is recommended. Under this condition, the properties of the composite modified rejuvenated asphalt demonstrate comparability to those of the original asphalt. In summary, this research underscores the potential for integrating waste coffee biochar material into infrastructure development, thereby promoting circular economy principles and advancing more sustainable construction practices.

Creep stress analysis of Transversely Isotropic Rotating Disc Composed of Piezoelectric Material

If a crystal undergoes mechanical stress, then an electrical potential is developed across its sides; this phenomenon is called piezoelectricity, or the piezoelectric effect. Piezoelectric materials include quartz, zinc oxide (ZnO), lead zirconate titanate (PZT4), and Rochelle salt. There are numerous uses for piezoelectricity in signal and electrical transducers. In this work, transitional and creep stresses are evaluated in a thin disc made up of piezoelectric transversely isotropic solids subjected to rotation. The mathematical expressions of stress components are computed for the rotating disc by using Seth’s transition theory considering the rotation effect in circular disc. The electric displacement relations and various stress components are computed using Hooke’s Law. A non-homogeneous differential equation is obtained by using mathematical relations and the equilibrium equation. The theoretical solution of the differential equation is obtained under specified boundary conditions. Creep stresses are studied for the considered material. The obtained results are shown graphically, analyzed numerically, and concluded with a discussion of the results for transversely isotropic piezoelectric materials such as BaTiO3 and PZT-4, among others. On the basis of all the numerical discussions and graphs, it is concluded that discs composed of transversely isotropic piezoelectric (PZT4 and BaTiO3) materials are more stable than discs composed of transversely isotropic (magnesium and beryl).

Structural response of glass fiber-polymer composite bending-active elastica beam under long-term loading conditions

Bending-active elastica beams represent structural members which are initially installed as straight beams and then bent into arched shapes by applying horizontal displacements to one support. Designing such members for permanent structures made of fiber-polymer composites involves complex viscoelastic responses, which have not yet been thoroughly investigated. An experimental investigation of medium-scale bending-active elastica beams, consisting of pultruded glass fiber-polymer composite profiles, was thus conducted to investigate the long-term structural behavior of such members under imposed sustained bending and axial compression. The results revealed that viscoelastic responses are based on an interaction of stress relaxation and creep with their effects increased with increasing bending degree and time of exposure to sustained strains and stresses. The imposed horizontal displacement to one of the supports to maintain the bent beam shape induced sustained bending stresses in the beam. Beneficial relaxation of these stresses occurred with relaxation predicted to reach 12 % during a targeted 50-year design service life. Furthermore, the likelihood of the curved beam exhibiting in-plane deformations under sustained stresses enabled creep to occur simultaneously, with associated in-plane creep deformations and strength reduction. While creep deformations remained insignificant, progressive creep rupture occurred at highest bending degrees, exhibiting sequential creep rupture in the outer combined mat layers, delamination, crack opening and final fiber failure. Creep rupture can be prevented by postponing crack initiation in the combined mat layer beyond the targeted design service life. This can be achieved by limiting the bending degree to 50 % of the bending degree at which short-term crack initiation occurs.

High temperature tensile creep behavior and microstructure evolution of Ti60 alloy rolled sheet

In this work, the high temperature tensile creep test of 2mm Ti60 alloy rolled sheet was carried out, and the creep behavior and microstructure evolution were studied. The initial microstructure of the 2mm Ti60 alloy rolled sheet is mainly composed of primary α phase and secondary α phase, and there are many dislocations and dynamic recrystallization (DRX) inside the rolled sheet. According to Norton-Bailey law, the creep stress exponent at 600 °C is calculated to be 3.6, and creep activation energy at 200MPa is calculated to be 286.4kJ/mol. It implies that the creep mechanism of the rolled sheet includes dislocation slip and dislocation climb. The initial Ti60 alloy rolled sheet has the {0001}<10-10>α texture. Stretching along the RD makes the texture direction gradually change from B-type (<0001>//ND) to T-type (<0001>//TD). Whether it is the B-type texture or T-type texture, the (0001) plane of the α phase always exhibits a basal texture state parallel to the tensile stress direction, contributing a good tensile creep property of this alloy sheet.

Material volume reduction for creep testing using composite cantilevers and its application for residual life assessment

Digital image correlation (DIC) and finite element analysis (FEA) demonstrate that creep deformation in bending occurs primarily in ≈30 % of the cantilever volume near the fixed end, especially when the creep stress exponent ranges from 5 to 7. As an alternative approach to minimize the material volume required for testing, the concept of fabricating composite cantilevers is proposed and validated in this study. A composite cantilever sample consists of an “active” creeping portion (e.g., T22 boiler steel) and an additively extended “passive” non-creeping portion (e.g., IN718). The volume reduction process involved varying the length of the “active” section, a, while keeping the total length of the cantilever, L, constant. The DIC measurements conducted at 600 °C to assess the creep behavior of T22 steel revealed that analytical expressions for monolithic cantilevers could aptly predict the constitutive steady-state creep laws from the composite cantilevers if measurements are made in a region at a critical distance away from the interface. FEA indicates that accurate stress estimation enables predicting monolithic creep behavior using composite samples with “a/L” ratios of as small as 5 %. Using the developed approach, the loss of creep resistance of T11 boiler steel that was in service for ∼ 240,000 h was ascertained in high throughput fashion using a composite cantilever having only 30 vol % of the “active” material. Guidelines to minimize the volume fraction of the “active” portion in the composite cantilever and the implications of the observations for estimating the residual life of in-service high-temperature components are discussed.

Influence of bolt creep induced pre-tightening force relaxation on dynamic response of the bolted joint system

The bolted joint is an important link that affects the accuracy maintenance of the heavy-duty machine tool. Due to bolts of the crossbeam are under a preload of several hundred kN for an extended period, the bolt gradually creeps and elongates as the machine tool's service time increases. This relaxation of the preload results in a degradation of the bolted stiffness, weakening the dynamic response of the bolted joint system. To reveal that the degradation law of crossbeam bolting performance of the heavy-duty machine tool induced by bolt creep, based on the Norton-Bailey(NB) model, a method for analyzing the creep of bolts with precision threads is proposed, and the influence of thread geometry and friction coefficient on the creep stress relaxation of bolts is studied. Considering the interface contact, an interface contact stiffness model is derived based on fractal theory. The dynamic equation of the bolted beam system is established using the Matrix27 stiffness matrix. The dynamic response of the bolted system, resulting from the degradation of interface stiffness due to bolt creep, is analyzed. The results show that the stress relaxation of bolt creep is not only related to creep parameters, but also related to the mate-thread interaction. The dynamic model with Matrix27 stiffness matrix is comparable to experiment in calculation accuracy and efficiency, which provides technical guidance for machine tool dynamics analysis and effectively solves the scientific problem of beam bolting performance degradation during the service of heavy-duty machine tools.

Evaluation and comparison for higher temperature performance index of emulsified asphalt mastic using coal gangue powder

In order to investigate the rheological behavior and the influence of solid waste coal gangue powder on the high-temperature performance of cold recycled Emulsified Asphalt Mastics (EAM), Dynamic Shear Rheometer (DSR) and Multiple Stress Creep Recovery (MSCR) tests were conducted using three different fillers and four powder-to-binder ratios of EAM. Evaluation indexes such as rutting factor (G*/sinδ), improved rutting factor (G*/1−1/sinδ∙tanδ), Unrecoverable Creep Compliance (Jnr), Cumulative Strain (CS) and Creep Recovery Ratio (R) were used to analyze the influence of filler type and dosage on high temperature of EAM, and the effectiveness of these indexes to evaluate high temperature is considered. Moreover, atomic force microscopy experiments were carried out to study on interaction mechanism between the fillers and emulsified asphalt. Finally, grey relational analysis method was used for quantitative assessment of these indexes for EAM. The results indicate that all three fillers effectively improve the high-temperature performance, with a larger improvement observed as the filler dosage increases, among which the tunneling coal gangue powder is the most significant. Under a stress level of 0.1 KPa, the coal gangue filler mastic appears the best deformation recovery ability, whereas under a stress level of 3.2 KPa, the cement filler mastics appears the best deformation recovery ability. The additional fillers significantly influence the nano-scale surface morphology of the residues, and the tunneling coal gangue powder appears a stronger adsorption capacity for free polar components compared to the cement and limestone mineral powder. It is suggested that the Jnr and CS can be used as evaluation indexes of high temperature evaluation index of EAM, instead of G*/1−1/sinδ∙tanδ or G*/sinδ or R.

Rheological and mechanical evaluation of a novel fast curing cold asphalt concrete made with asphalt emulsion, by-products and magnetic induction

This work studies the feasibility of a new cold asphalt concrete with 5 % voids with fast curing, developed with asphalt emulsion and magnetic induction. Until now, it was impossible to produce fast curing cold asphalt concretes due to the impossibility of compacting and evaporating the water in the asphalt emulsion quickly. Therefore, the aim of this work is to solve the impossibility of compacting the cold asphalt concrete and thus reduce the long curing times. For this purpose, at laboratory level, an experimental cold asphalt concrete was designed with magnetic induction and compared with two reference hot asphalt concretes manufactured according to Spanish standards without magnetic induction (one with 50–70 grade bitumen and another with a PMB45/80–65 type polymer-modified bitumen). The research was carried out in two stages. First, the new cold asphalt concrete was rheologically characterized, the binder recovered from the asphalt concrete was analyzed according to the tests of ring and ball, penetration, dynamic shear rheometer (DSR) and multiple stress creep and recovery (MSCR). Secondly, the new cold concrete asphalt was mechanically characterized, the mechanical performance of the cold asphalt concrete was analyzed by evaluating stability and deformation, dry and wet indirect tensile strengths (ITS), wheel tracking test, stiffness modulus and resistance to raveling dry and wet conditions. Based on the rheological analysis results, the asphalt emulsion recovered from the cold asphalt concrete is extremely soft with a low softening point and a high penetration rate. On the other hand, the values of viscosity, phase angle, stiffness and non-recoverable creep compliance are between those of the bitumen 50/70 and the PMB45/80–65, but closer to bitumen 50/70. As for their mechanical performance, the novel cold asphalt concrete studied presents better resistance to water damage and particle loss, both in dry and wet conditions, but also high permanent deformations and low ITS, probably due to the fact that the residual binder of the emulsion used is softer than the others.

Development of SBS composite modified asphalt incorporating polydopamine-enhanced MoS2

This study investigated the development of a novel composite modified asphalt incorporating PDA-MoS2 into styrene-butadiene-styrene (SBS) modified asphalt. The successful synthesis of PDA-MoS2 was confirmed through various characterization techniques. The incorporation of PDA-MoS2 into SBS modified asphalt resulted in significant improvements in performance properties. With a PDA-MoS2 content of 0.7 wt%, the modified asphalt showed a notable 15.1% rise in softening point and a 24% drop in penetration in comparison to the control SBS modified asphalt. Dynamic Shear Rheometer tests revealed a 2.4-fold increase in the rutting factor at 60°C. Multiple Stress Creep Recovery tests demonstrated enhanced rutting resistance, with a 72.2% reduction in nonrecoverable creep compliance at 0.1 kPa stress level. Electrochemical measurements showed improved corrosion resistance, evidenced by lower current densities and higher charge transfer resistance. Microstructural analysis revealed well-dispersed PDA-MoS2 particles forming a compact network structure within the asphalt matrix. The hydrophilicity of the modified asphalt increased, with a 35.3% decrease in water contact angle. The synergistic effect between PDA-MoS2, SBS, and asphalt components, facilitated by enhanced interfacial interactions and chemical bonding, contributed to the observed performance improvements. The results indicate that PDA-MoS2 has the potential to improve the characteristics of SBS modified asphalt as a modifier.

A novel Ta-contained TiAl alloy with excellent high temperature performance designed for powder hot isostatic pressing

TiAl alloys offer strong potential for replacing conventional nickel-base alloys in structural applications at high temperatures, which requires good high temperature performance. This study analyzes the creep performance and thermal exposure characteristics for a powder hot isostatic pressing (P-HIP) Ta-contained TiAl alloy. The microstructure characteristics, creep performance, and thermal exposure properties of the nearly lamellar (NL) alloy with a size of about 145 μm were investigated. The alloy remains 0.72 % fracture strain at room temperature after exposure at 750 ℃ for 1000 h. The fitting results of creep curves show that the creep stress index n is 15.82 at 750 ℃, indicating the power law creep mechanism. By reducing the interfacial energy, Ta can facilitate the formation of metastable structures and achieve refinement. The enrichment of Ta element at the lamellar edge, both observed after thermal exposure and creep, inhibits the growth of lamellae and hinders the expansion of cavities due to its low diffusion rate, improving the thermal stabilities and creep performance. The P-HIP Ta-contained TiAl alloy shows exciting high temperature performance.