Microstructure Of Steel Research Articles

Microstructural Deformation and Fracture of Reduced Activation Ferritic-Martensitic Steel EK-181 under Different Heat Treatment Conditions

Abstract TEM studies were performed to examine the effect of holding of dispersion-strengthened heat-resistant reduced activation 12% chromium ferritic-martensitic steel EK-181 in static liquid lead for 3000 h at 600°C on the steel microstructure in comparison with the steel after conventional heat treatment by quenching and tempering at 720°C. It was found that the steel microstructure has good thermal stability under the specified experimental conditions. Microstructural deformation of EK-181 steel was studied in the neck region of tensile specimens tested at the temperatures 20, 680, 700, and 720°C with and without holding in liquid lead, and their fracture mechanisms were investigated. As a result of plastic deformation during tensile testing at room temperature, martensite plates and laths near the fracture surface are distorted and fragmented with the formation of new low-angle boundaries, and the dislocation density increases. At the deformation temperatures 680–720°C, nearly equiaxed ferrite grains are formed, the density and size of second-phase particles (M23C6 and MX) increases due to dynamic strain aging, and the dislocation density decreases locally. As the test temperature rises, the degree of martensite tempering increases. At T ≥ 700°C, some dynamic polygonization and dynamic recrystallization are observed. At elevated tension temperatures, ferrite coarsening is more significant in the specimens held in lead as compared to the conventionally treated material. The plastic deformation and fracture behavior of the steel are largely determined by the test temperature, rather than by the treatment mode.

Effect of ultrasonic impact treatment on surface residual stress, microstructure and electrochemical properties of the hot-rolled S355 steel

The effects of ultrasonic impact treatment (UIT) on the microstructure, corrosion resistance, and surface residual stress of hot-rolled S355 steel were investigated. In addition, the improving mechanism of the UIT induced corrosion resistance was discussed. The results show that the UIT can effectively improve the corrosion resistance of hot-rolled S355 steel, and corrosion current density reduction is demonstrated. Based on the corrosion morphology, it can be found that after the UIT the corrosion pits became shallower, the oxide layer becomes denser, and more flocculent structures appear on the surface as well as the appearance of dense irregular curved structures. Moreover, the residual tensile stress on the surface of the hot-rolled S355 steel is transformed into residual compressive stress after the UIT. The grains are refined, and the microhardness is increased, which implied that the significant plastic deformation has occurred on the surface of the hot-rolled S355 steel. The findings confirm that dense oxides could be generated on the surface of hot-rolled S355 steel treated by ultrasonic impact since the residual compressive stress is introduced, the plastic deformation is induced, and the grains are refined.

تأثير استعمال ليزر النيوديميوم ياك (Nd-YAG) على البنية الدقيقة وصلابة سطح الفولاذ AISI1012

The unique characteristics of the laser beam such as directionality, monochromaticity, and brightness make it a very important tool in the surface treatment engineering. The concentrated heat in the laser beam can be precisely directed toward the processed region on the surface. The laser beam power, beam size, and scanning velocity are easily controlled during the different processing methods. Laser surface modifications of metallic materials, such as laser surface melting, laser surface alloying, and laser cladding are some of the most important methods to improve the mechanical properties of the processed layer on the surface. A pulsed Nd-YAG laser surface melted specimens of low carbon steel with a maximum power of 90W at different processing parameters. The rapid melt and solidification of the treated layer produced a refinement in the microstructure. The original microstructure of this steel (Ferrite + Pearlite) has been transformed to new phases of martensitic and bainitic structures. The melted layer consists of the melted pool, the heat affected zone, and the substrate. The maximum hardness of the laser melted layer is more than 400 HV. The effect of different lasers such as high power CW CO2 laser on the mechanical properties and corrosion resistance of steel alloys will be carried out in future studies. Keywords: Nd-Yag Laser, Laser surface treatment, Microstructure and hardness of AISI1012 steel

A hot deformation constitutive model applicable for complete austenite and dynamic ferrite transformation interval

Dynamic ferrite transformation is a vital microstructure evolution mechanism for carbon alloy steels and an essential technology for manufacturing high-performance steel materials. In practice, carbon steel hot working processes are usually carried out at various temperatures, involving the evolutionary behavior of the single-phase austenite and the ferrite dynamic transformation process. Few models can simultaneously predict the microstructural state and deformation resistance in the single-phase austenitic interval and the dynamic ferrite transformation interval. The deformation mechanisms involve work-hardening, dynamic recovery, and dynamic recrystallization of austenite and ferrite phases, as well as the dynamic transformation of austenite to ferrite and coordinated deformation between the two phases. Therefore, this paper extends the application range of the model based on the viscoplastic unified constitutive model by considering the above deformation mechanisms. The constitutive model proposed in this paper applies to both the single-phase austenite interval and the dynamic ferrite transformation interval. Moreover, it can accurately predict carbon alloy steel's microstructure state and deformation resistance in different intervals. This paper can help to construct a hot deformation constitutive model in a wide range of deformation temperature intervals of steel materials.

Continuous cooling transformation in micro-alloyed medium-carbon steel and optimization of the forging process for half-shaft production

Abstract Micro-alloyed medium-carbon steel is increasingly used as a cost-effective alternative to quenched and tempered steel in the production of half-shaft components. Current research emphasizes controlling the microstructure during thermomechanical processing to achieve the desired structural properties after cooling. This study investigated the effect of continuous cooling transformation on the microstructure and mechanical properties of micro-alloyed medium-carbon steel. At a cooling rate of 0.5 °C s−1, only pearlite transformation occurred. At rates between 1 °C s−1 and 8 °C s−1, both bainite and martensite transformations were observed, while only martensite formed at rates exceeding 12 °C s−1. Subsequently, a four-factor, three-level orthogonal experiment was designed based on the actual production process for half shafts. The optimal forging parameters were identified as a heating temperature of 1000 °C, a deformation temperature of 920 °C, a deformation extent of 15%, and a cooling rate of 0.5 °C s−1. The study offered solutions to enhance microstructural uniformity and effectively manage abnormal bainite and martensite formations, thereby establishing a foundation for the high-quality application of micro-alloyed medium-carbon steel in half-shaft components.

Design of tri-phase lamellar architectures for enhanced ductility in ultra-strong steel

Achieving exceptional ductility in ultra-high strength steels has long been a formidable challenge, particularly when the yield strength reaches 2.0 GPa. In this study, we have designed an innovative tri-phase lamellar microstructure in medium Mn steel that successfully achieves both an ultrahigh yield strength of approximately 2.0 GPa and an impressive uniform elongation ranging from 22.5 % to 24.5 %. The ultra-high yield strength of this steel is primarily due to the ultrafine lamellar grain with high-density dislocations and HDI strengthening resulting from meticulously designed tri-phase lamellae. The remarkable ductility is attributed to the synergistic action of multiple plasticity mechanisms. The inherently excellent plasticity of the lamellar ferrite, in coordination with the lamellar martensite, generates significant HDI hardening, thereby suppressing the onset of necking in the early stages of deformation. During the mid-stage of deformation, high strain activates the transformation-induced plasticity effect in the highly stable austenite, which remains stable due to substantial HDI hardening and effectively mitigates strain localization. In the later stages of deformation, delamination cracking relieves stress accumulation at the interfaces, delaying material failure. These mechanisms elevate yield strength and uniform elongation product to 47.3 GPa·%, showcasing the tri-phase lamellar structure’s potential for ultrahigh-strength, high-ductility steels.

Investigation on microstructure and dynamic fracture behavior of high-strength steel welded by LAHW under different heat inputs

Investigation on microstructure and dynamic fracture behavior of high-strength steel welded by LAHW under different heat inputs

Influence of arc energy on the microstructure and corrosion behavior of ER2209 duplex stainless steel deposited on Q345B low-alloy steel by GMAW

In order to eliminate the complex effects of thermal cycling and the thermal effects of the next pass on multi-layer multi-pass welding of low-alloy steel and duplex stainless steel, ER2209 welding wire was single-layer single-pass deposited on the surface of Q345B hot-rolled plate by gas metal arc welding (GMAW). The microstructure and corrosion resistance of welded joints were studied by different arc energies. The results showed that the arc energy had a significant impact on the “tongue-shaped” morphology and the width of heat affect zone in the welded joint, which in turn affected the corrosion performance of the welded joints. Due to the least distribution of “tongue-shaped” morphology and minimum width of heat affected zone in the welded joint with arc energy of 0.645kJ/mm, it owned the best corrosion resistance. The weld metals of the welded joints were composed of ferrite and austenite phases. The ferrite phases were distributed along grain boundaries and intergranular. As the heat input increases, the distribution of ferrite phase along grain boundaries gradually decreased. The corrosion products and corrosion morphology of the welded joint were also investigated and the corrosion mechanism was discussed in detail. The research results of this article provide a theoretical basis for improving the corrosion performance of multi-layer multi-pass welded joints of low-alloy and duplex stainless dissimilar steels.

Interplay between deformation and fracture mechanism in gradient nanostructured austenitic stainless steel

The plastic deformation parameters are crucial for the grain size of gradient nanostructured (GNS) materials, and the multiscale grain structure within the GNS layer has a significant impact on fracture behavior. In this study, the detailed depth-dependent microstructures of GNS310S stainless steel fabricated by surface mechanical rolling treatment (SMRT) were investigated, and the relationship between the geometrically necessary dislocation (GND) density and the strain gradient was established through the local misorientation obtained by electron backscatter diffraction. The critical deformation parameters (strain gradient, shear strain, and strain rate) of SMRT-induced grain refinement at different scales were quantitatively evaluated. The tensile results show the yield strength and tensile strength of GNS310S are improved by 103 % and 23.1 % respectively compared to CG310S. Additionally, we elucidate the underlying tensile fracture mechanism of GNS310S stainless steel through detailed microstructural analysis. Due to the poor ductility of the near-equiaxed nanograins, cracking occurred on the surface of the SMRT specimen at low strain during the tensile testing. These cracks evolved into competitive shear offsets and multi-cracks with increased strain on the specimen surface, eventually leading to a hybrid fracture mode. In contrast, the subsurface nanotwinned lamellae layer displayed good ductility during tension, which can accommodate the deformation through lamellae widening and forming secondary twinning. This nanotwinned lamellae layer can suppress the inward propagation of surface cracks when the strain was not large. This work provides new insights into the fabricating parameters of the GNS stainless steel, as well as the deformation and fracture mechanisms.

Enhancing strength and toughness in a pearlitic rail steel via multi-alloying and accelerated cooling

The demand for higher speeds and heavier loads has emphasized the necessity to tackle the inherent trade-off between strength and toughness in pearlitic rail steels. Herein, the co-additions of Cr, Ni and Cu and accelerated cooling rate on the microstructure and mechanical properties of a medium carbon pearlitic steel were systematically investigated. In comparison with base alloy, the new steel exhibits smaller prior austenite grain size (PAGS) due to the drag effect of Cu and Ni solutes. The finer PAGS and lower C content increased the volume fraction of proeutectoid ferrite. The finer pearlitic nodule size (PNS) and pearlitic colony size (PCS) were attributed to the small PAGS and greater extent of undercooling due to the combined effect of multi-alloying and accelerated cooling. Additionally, the synergistic effects of multi-alloying and accelerated cooling rate decrease the pearlitic phase transformation temperature, accountable for the finer interlamellar spacing (IS). Compared with the base steel, the yield strength and ultimate tensile strength of the new steel increased from 587 MPa and 1069 MPa to 740MPa and 1178MPa, respectively, with a simultaneous increase of ductility from 12.4% to 14.7%. The strength increments are mainly attributed to the finer IS in the new steel. Meanwhile, the new steel possesses a higher impact toughness compared to the base steel due to the increased volume fraction of proeutectoid ferrite, and finer PNS and IS.

Effect of nitrogen on the microstructure and strengthening mechanism of high performance tinplate

In order to meet the high strength and high formability requirements of the tinplate market, the nitrogen strengthening method was used for the chemical composition of the tinplate, and the action mechanism of nitrogen on the full-process tinplate substrate was explored. The present study designed tinplate with different nitrogen contents (named as 20N steel and 150N steel), and conducted phase transformation research and recrystallization temperature tests. SEM, XRD, EBSD, TEM, chemical dissolution analysis and tensile tests were carried out, and the influence of annealing process on the microstructure, mechanical properties and precipitation of annealed sheet was also explained. With the increase of nitrogen content, the phase transformation temperature decreases, the hardness increases and the recrystallization temperature increases. The microstructures of 20N steel and 150N steel annealed at different annealing temperatures are composed of ferrite and cementite distributed in chains. At the same annealing temperature, the recrystallization degree of 20N steel is higher, the {111} texture accounts for a larger proportion, and the grain size is larger. With the increase of annealing temperature, the yield strength and tensile strength show a downward trend, while the elongation shows an upward trend. Compared with 20N steel, the yield strength and tensile strength of the 150N annealed sheet are significantly improved, and the elongation is slightly reduced. The calculation results show that the mechanism of nitrogen improving the strength of tinplate is mainly solid solution strengthening, and the improvement effect of fine grain strengthening and precipitation strengthening is weak.

Microstructure and mechanical properties of CP780 steel - 7075 aluminum alloy laser welded joint assisted by rotating magnetic field

Abstract This study uses a rotating magnetic field for laser welding on 1 mm thick CP780 high-strength steel and 1.5 mm thick 7075 aluminum alloy. The effects of different welding parameters (B = 0 mT, B = 65 mT with V = 0°/s, B = 65 mT with V = 10°/s) on the morphology, microstructure, and tensile properties of welded joints are analyzed. At B = 0 mT, the weld shape is V-shaped, with the intermetallic compounds primarily consisting of needle-like brittle Al-rich (Fe, Si)Al2 phase and fewer granular ductile Fe-rich (Fe, Si)Al phase, resulting in poor mechanical properties. With the application of the rotating magnetic field, the laser energy becomes more concentrated, forming a ‘T’ shape weld. The rotating magnetic field (B = 65 mT with V = 10°/s) generates a constantly changing Lorentz force, promoting molten pool flow and enhancing Fe diffusion within the weld. This process reduces needle-like brittle Al-rich (Fe, Si)Al2 phase and increases granular ductile Fe-rich (Fe, Si)Al phase. It also accelerates the weld cooling rate and inhibits the reaction time and grain growth of intermetallic compounds, thereby reducing the thickness and content of the intermediate transition layer and significantly improving mechanical properties. A comprehensive comparison shows that the best mechanical properties are achieved at B = 65 mT with V = 10°/s. This study offers new insights and a theoretical foundation for achieving cost-effective, high-performance welded joints in advanced high-strength steel and high-strength aluminum alloy for automobiles, thereby facilitating lightweight vehicle development.

Analyzing the permeability distribution of multilayered specimens using pulsed eddy-current testing with multi-scale 1D-ResNet

The mechanical properties of steel are determined by its microstructure, which is closely related to its permeability profile. In thermal processing, layered structures are formed in steel and different layers have different mechanical and magnetic properties. Therefore, it is crucial to propose a practical method to monitor the change of permeability profile along the depth, which can indicate the evolution of the microstructure of steel during thermal processing, such as hot rolling. This paper presents a method for determining the layered structure and permeability profile of the steel by using pulsed eddy current testing (PECT), which offers better penetration ability. An analytical model has been deduced for calculating the time-domain pulsed eddy current (PEC) response from a Hall sensor of a triple-layer conductor system based on the inverse Laplace transform. It is found the Tau (τ) curve is closely related to the permeability profile of the conductor. For the inverse solution, the Simultaneous Iterative Reconstruction Technique (SIRT) is utilized to determine the permeability profile of the multilayered specimens from the measured response. The approximate Jacobian matrix (sensitivity matrix) is obtained by the perturbation method based on the Tau curve. However, the permeability profile suffers from smoothing effect and sharp features are lost. Deep learning (DL) algorithm based on the Multi-Scale 1D-ResNet model is therefore introduced to address this issue. Numerical simulations and experiments have been performed to evaluate the proposed method for permeability profile estimation with various materials and thicknesses. The DL method can achieve an accurate estimation of the plate permeability profile with a relative error under 5%.

Enhancing mechanical properties and wear resistance of dual phase steel through surface mechanical attrition treatment

The study investigates the mechanical properties of dual-phase (DP) steel undergoing surface martensite transformation through Surface Mechanical Attrition Treatment, revealing phase transformation and grain refinement, increasing exponentially with treatment duration. After 40 min of SMAT, X-ray Diffraction (XRD) and Scanning Electron Microscopy (SEM) analyses revealed approximately 37% martensite and 63% ferrite phases, in contrast to 5% martensite and 95% ferrite phases in the as-received state. The surface hardness of the steel increased to 270 VH0.05 (up from 145 VH0.05), while the yield strength rose to 405 MPa (up from 258 MPa). Furthermore, a 60% reduction in the specific wear rate of the steel was achieved. This study highlights SMAT as an innovative method for tailoring the microstructure of steel and enhancing its mechanical properties through stress-induced phase transformation.

Study of the Martensitic Transformation of Steel During the Induction Hardening Process by means of Acoustic Emissions

Non-Destructive Testing (NDT) technology known as Acoustic Emission (AE) has been used to investigate the phase transformation of 42CrMo4 steel in a cylinder during an induction hardening process. The objective of this study is to characterize the martensitic transformation of the material using the data obtained by the AE sensor during the process. The heating process of the cylinder is carried out statically, focusing the heat on the area to be treated and then analyzing it. After quenching, destructive tests are carried out to determine the hardness and three-dimensional geometry of the steel microstructure after the process (hardness and X-ray diffraction tests). Once the microstructure of the material is known, it is possible to relate the results with the signals obtained by AE, making possible in future induction hardening processes the estimation of martensite by non-destructive techniques.

Effect of Trace Rare Earth Element Cerium (Ce) on Microstructure and Mechanical Properties of High Strength Marine Engineering Steel

In this paper, FH460 special steel with rare earth element cerium (Ce) was selected, and the control group without Ce was set up. By changing the content of Ce, the microstructure, phase transition point, and mechanical properties of the test steel were observed to study the effect of trace rare earth element Ce on the microstructure and mechanical properties of high-strength marine engineering steel. The morphology and energy spectrum of inclusions in three kinds of test steels were observed by SEM, and the morphological changes in inclusions in FH460 high-strength marine engineering steel after adding Ce were investigated. The fracture morphology and energy spectrum analysis were carried out by combining the tensile test at room temperature and the gradient low temperature impact toughness test, and the effect of trace Ce on the mechanical properties of the test steel was comprehensively analyzed. The results show that the addition of Ce changes the phase transformation temperature of Ac1 and Ac3, and refines the original microstructure of the test steel. SEM observation showed that the addition of Ce changed the long strip MnS and polygonal irregular Al2O3 inclusions into ellipsoids, which reduced the size of inclusions. The gradient low temperature impact test shows that with the decrease in temperature, the fracture dimple depth of the three test sheets of steel decreases, and the Ce-containing test steel forms a deep dimple centered on rare earth inclusions, which hinders the crack propagation and significantly improves the low temperature impact toughness of the test steel.

Deep learning-aided inverse analysis framework to accelerate the exploration of DP steel microstructures

Materials development requires numerous numbers of trial and error experiments. To reduce the experimental cost, numerical simulations which predict material microstructures and mechanical properties have a great potential to estimate the microstructures that should be produced for obtaining materials with the desired properties. There is a need to develop dual-phase (DP) steel with higher strength and ductility because DP steel is widely used due to its significant mechanical properties. DP steel consists of a soft phase (ferrite) and a hard phase (martensite), and the mechanical properties depend on the ratio of the two phases. The mechanical properties of DP steels are affected by the spatial distribution of martensite and ferrite, which requires a comprehensive consideration of a variety of microstructures. The problem is how to estimate microstructures of DP steel with the desired mechanical property because a comprehensive investigation of microstructures makes computational cost significantly expensive. For the purpose of reduction of the computational costs, we aim to develop a framework with low computational cost. The developed framework finds the optimal microstructure of DP steel by repeated random searches for a model that combines a generative adversarial network (GAN), which generates microstructures, and a convolutional neural network (CNN), which predicts the maximum stress and working limit strain from microstructures. Due to a low-dimensional search space provided by a latent variable of GAN, the proposed framework enables an efficient search for microstructures possible. To explore the desired microstructures under complex deformation modes, the multiple deformation modes are considered in this study. This framework is applicable not only for the microstructure of DP steel but also any other material microstructures. We are exhaustively able to explore the microstructure with desired properties of metallic or other composite materials in low-dimensional space thanks to this framework and contributes to accelerating materials development.

Investigating Microstructure and Wear Characteristics of Alloy Steels Used as Wear Plates in Ballast Cleaning Operation in Railways

Abstract Ballast cleaning machines play a pivotal role in maintaining the stability and safety of railway tracks by transferring and redistributing ballast on the tracks. However, the wear plates used in these machines are subjected to extreme conditions, making the assessment of their wear performance crucial. This study scrutinizes the wear performance of two distinct 31Ni10Cr3Mo6 based alloy steels used as wear plates in the ballast cleaning machines. The study compares the initial microstructure and wear properties of German grade steel (Plasser) wear plate with an indigenous grade steel (RDSO) used as an alternative. The results indicate that the indigenous wear plate consistently exhibits higher weight loss across various loading conditions, whereas the Plasser wear plate demonstrates superior wear resistance, particularly at higher loads. This enhanced performance is attributed to relatively larger amount of high-angle grain boundaries, small grain size, and variations in micro-alloying elements. The compositional analysis indicates low carbon content in both wear plates. The microstructural analysis shows that both samples have a single body-centered cubic crystal structure, with a randomly distributed heterogeneous ferritic and cementite phases in a lath-bainitic microstructure. This comprehensive study provides valuable insights into the wear behavior of these alloy steels, contributing to the optimization of alloying materials and desired microstructure for the wear plates in ballast cleaning machines.

Special Issue “Microstructure, Fatigue and Wear Properties of Steels”

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Phase transformation process and toughening mechanism of 12Cr1MoV heat-resistant steel for high-pressure boilers by external shower and internal spray heat treatment

To optimize the heat treatment process for 12Cr1MoV heat-resistant steel, this study designed a novel process of external shower and internal spray (ESIS), followed by air cooling. This new approach was simulated in the laboratory. The study focused on the variation in impact energy and the microstructural changes in the experimental steel subjected to different processes, specifically the T890 and T740 processes (where the numbers represent the termination temperature of ESIS). The phase transformation processes and toughening mechanisms of the steel after these treatments were thoroughly investigated. The theoretical analysis revealed that the microstructures of T890 and T740 steels consist of quasi-polygonal ferrite (QPF), granular bainite (GB), and pearlite. The QPF in T890 steel forms at a higher temperature compared to T740 steel, leading to a lower dislocation density and carbon content in QPF during the subsequent cooling phase. This results in the QPF in T890 steel having a hardness of 1.02 GPa lower than that of the QPF in T740 steel. The higher hardness of QPF in T740 steel correlates with reduced toughness and resistance to crack propagation. Under impact loading, the QPF in T740 steel exhibits insufficient crack propagation resistance to counteract the effects of microscopic defects within the tensile stress region of the fracture. Consequently, cracks preferentially propagate within the QPF, creating a relatively flat propagation path. In comparison, the fracture of T740 steel demonstrates a straighter propagation path in the tensile stress region than T890 steel, resulting in significantly lower impact energy for T740 steel.