ABSTRACT In this study, the corrosion and mechanical performance of hybrid aluminium matrix nanocomposites (HAMNCs) reinforced with titanium oxide (TiO2) and yttrium oxide (Y2O3) nanoparticles were investigated. A squeeze-casting process was used to develop five HAMNCs with wt.% of nanoparticles of 2.5, 5, 7.5, and 10. The corrosion resistance of HAMNCs was investigated during a 168-h salt spray test. XRD examined the crystallographic and elemental properties of the HAMNCs. FESEM was used to examine nanoparticle distribution and interaction in the matrix. The microhardness, compression strength and yield strength properties of the fabricated samples were examined. The introduction of nanoparticles at 5 wt.% TiO2 +5 wt.% Y2O3 (HAMNC6) in the Al matrix had the most outstanding properties (corrosion resistance, microhardness, compression strength, yield strength). The properties were shown to be inversely proportional with an increase in the wt.% of the nanoparticles. The SEM analysis of corroded surfaces revealed that TiO2 and Y2O3 nanoparticles were found near the grain boundaries of HAMNC6, causing small pits and minor cracks.