Specular Surfaces Research Articles

3D shape measurement of discontinuous specular objects based on advanced PMD with bi-telecentric lens.

This paper presents an advanced phase measuring deflectometry (PMD) method based on a novel mathematical model to obtain three dimensional (3D) shape of discontinuous specular object using a bi-telecentric lens. The proposed method uses an LCD screen, a flat beam splitter, a camera with a bi-telecentric lens, and a translating stage. The LCD screen is used to display sinusoidal fringe patterns and can be moved by the stage to two different positions along the normal direction of a reference plane. The camera captures the deformed fringe patterns reflected by the measured specular surface. The splitter realizes the fringe patterns displaying and imaging from the same direction. Using the proposed advanced PMD method, the depth data can be directly calculated from absolute phase, instead of integrating gradient data. In order to calibrate the relative orientation of the LCD screen and the camera, an auxiliary plane mirror is used to reflect the pattern on the LCD screen three times. After the geometric calibration, 3D shape data of the measured specular objects are calculated from the phase differences between the reference plane and the reflected surface. The experimental results show that 3D shape of discontinuous specular object can be effectively and accurately measured from absolute phase data by the proposed advanced PMD method.

A calibration method for fringe reflection technique based on the analytical phase–slope description

The fringe reflection technique (FRT) has been one of the most popular methods to measure the shape of specular surface these years. The existing system calibration methods of FRT usually contain two parts, which are camera calibration and geometric calibration. In geometric calibration, the liquid crystal display (LCD) screen position calibration is one of the most difficult steps among all the calibration procedures, and its accuracy is affected by the factors such as the imaging aberration, the plane mirror flatness, and LCD screen pixel size accuracy. In this paper, based on the deduction of FRT analytical phase–slope description, we present a novel calibration method with no requirement to calibrate the position of LCD screen. On the other hand, the system can be arbitrarily arranged, and the imaging system can either be telecentric or non-telecentric. In our experiment of measuring the 5000mm radius sphere mirror, the proposed calibration method achieves 2.5 times smaller measurement error than the geometric calibration method. In the wafer surface measuring experiment, the measurement result with the proposed calibration method is closer to the interferometer result than the geometric calibration method.

Dynamically imaging collision electrochemistry of single electrochemiluminescence nano-emitters.

The quest for new techniques to measure single nanomaterials is a great impetus to research efforts to understand individual behaviours. Here, we develop an electrochemiluminescence (ECL) microscopy for visualization of stochastic collision electrochemistry of single nano-emitters without the interference of current and optical background. This design uses a water-immersion objective to capture the ECL emission of nanoparticles near the specular electrode surface for enhancing light collection efficiency. The approach enables us to trace the collision trajectory of multiple nanoparticles and spatially distinguish simultaneous collisions. Results reveal that collision types, frequencies and ECL intensities significantly depend on surface natures, particle concentrations, and diffusion fluxes. By recording successive collisions, we develop a "relay probe" sensing platform for long-term research. This imaging technique displays great potential for applications in single-particle electrochemical and analytical research.

Nonlinear phase error compensation for fringe deflectometry measuring system

Fringe deflectometry technique (FDT) plays a more and more important role in specular surface measurement due to its large slope measurement range. However, its accuracy is heavily dependent on the quality of the extracted phase. The gamma effect of liquid crystal display (LCD) and CCD introduces significant phase distortion, resulting in a periodical phase error and measurement error. A mathematical model is established to illustrate phase error introduced by gamma effect, and an optimal algorithm based on four-time four-step phase-shifting (FFPS) is proposed to retrieve phase. Simulation results prove that FFPS phase retrieval method can compensate for the phase error caused by the nonlinearity of the LCD and CCD point-by-point, thus it is immune not only to calibration error, but also to the non-unitary of the gamma effect spatially and temporally. Experimental results are also presented to verify the performance of the proposed method.

Characterization and data-driven modeling of a retro-reflective coating in Radiance

Retro-reflective coatings applied to blinds of reduced geometric complexity promise to provide view to the outside while effectively controlling solar gains and glare. To characterize the reflection characteristics of such coatings over the entire solar spectrum, a novel extension to a scanning gonio-photometer is developed. The extended instrument is tested and applied to measure a coating's Bidirectional Reflection Distribution Function including the region of the retro-reflected peak. The measured datasets are compiled into a data-driven reflection model for the daylight simulation software Radiance. This model is applied to illustrate the coating's effect in a comparison to purely diffuse and specular surface finishes on geometrically identical, flat blinds. Daylight supply, the probability of glare, and solar gains are assessed for an exemplary, South-oriented office under sunny sky conditions. The results indicate the potential of the coating to effectively shade direct sunlight even if applied on blinds with minimalistic geometries. The modeling technique is shown to be a general means to replicate the irregular optical properties of the coating, which cannot be represented by the standard models in daylight simulation software.

Three-Dimensional Shape Measurements of Specular Objects Using Phase-Measuring Deflectometry.

The fast development in the fields of integrated circuits, photovoltaics, the automobile industry, advanced manufacturing, and astronomy have led to the importance and necessity of quickly and accurately obtaining three-dimensional (3D) shape data of specular surfaces for quality control and function evaluation. Owing to the advantages of a large dynamic range, non-contact operation, full-field and fast acquisition, high accuracy, and automatic data processing, phase-measuring deflectometry (PMD, also called fringe reflection profilometry) has been widely studied and applied in many fields. Phase information coded in the reflected fringe patterns relates to the local slope and height of the measured specular objects. The 3D shape is obtained by integrating the local gradient data or directly calculating the depth data from the phase information. We present a review of the relevant techniques regarding classical PMD. The improved PMD technique is then used to measure specular objects having discontinuous and/or isolated surfaces. Some influential factors on the measured results are presented. The challenges and future research directions are discussed to further advance PMD techniques. Finally, the application fields of PMD are briefly introduced.

Comparative study of radiometric and calorimetric methods for total hemispherical emissivity measurements

Accurate knowledge of infrared emissivity is important in applications such as surface temperature measurements by infrared thermography or thermal balance for building walls. A comparison of total hemispherical emissivity measurement was performed by two laboratories: the Laboratoire National de Metrologie et d’Essais (LNE) and the Centre d’Etudes et de Recherche en Thermique, Environnement et Systemes (CERTES). Both laboratories performed emissivity measurements on four samples, chosen to cover a large range of emissivity values and angular reflectance behaviors. The samples were polished aluminum (highly specular, low emissivity), bulk PVC (slightly specular, high emissivity), sandblasted aluminum (diffuse surface, medium emissivity), and aluminum paint (slightly specular surface, medium emissivity). Results obtained using five measurement techniques were compared. LNE used a calorimetric method for direct total hemispherical emissivity measurement [1], an absolute reflectometric measurement method [2], and a relative reflectometric measurement method. CERTES used two total hemispherical directional reflectometric measurement methods [3, 4]. For indirect techniques by reflectance measurements, the total hemispherical emissivity values were calculated from directional hemispherical reflectance measurement results using spectral integration when required and directional to hemispherical extrapolation. Results were compared, taking into account measurement uncertainties; an added uncertainty was introduced to account for heterogeneity over the surfaces of the samples and between samples. All techniques gave large relative uncertainties for a low emissive and very specular material (polished aluminum), and results were quite scattered. All the indirect techniques by reflectance measurement gave results within ±0.01 for a high emissivity material. A commercial aluminum paint appears to be a good candidate for producing samples with medium level of emissivity (about 0.4) and with good uniformity of emissivity values (within ±0.015).

Performance analysis and evaluation of direct phase measuring deflectometry

Three-dimensional (3D) shape measurement of specular objects plays an important role in intelligent manufacturing applications. Phase measuring deflectometry (PMD)-based methods are widely used to obtain the 3D shapes of specular surfaces because they offer the advantages of a large dynamic range, high measurement accuracy, full-field and noncontact operation, and automatic data processing. To enable measurement of specular objects with discontinuous and/or isolated surfaces, a direct PMD (DPMD) method has been developed to build a direct relationship between phase and depth. In this paper, a new virtual measurement system is presented and is used to optimize the system parameters and evaluate the system's performance in DPMD applications. Four system parameters are analyzed to obtain accurate measurement results. Experiments are performed using simulated and actual data and the results confirm the effects of these four parameters on the measurement results. Researchers can therefore select suitable system parameters for actual DPMD (including PMD) measurement systems to obtain the 3D shapes of specular objects with high accuracy.

Effect of intermediate layers on atomic layer deposition-aluminum oxide protected silver mirrors

This work investigates intermediate materials deposited between silver (Ag) thin-film mirrors and an aluminum oxide (AlOx) barrier overlayer and compares the effects on mirror durability to environmental stresses. Physical vapor deposition of various fluorides, oxides, and nitrides in combination with AlOx by atomic layer deposition (ALD) is used to develop several coating recipes. Ag-AlOx samples with different intermediate materials undergo aggressive high-temperature (80°C), high-humidity (80%) (HTHH) testing for 10 days. Reflectivity of mirror samples is measured before and after HTHH testing, and image processing techniques are used to analyze the specular surface of the samples after HTHH testing. Among the seven intermediate materials used in this work, TiN, MgAl2O4, NiO, and Al2O3 intermediate layers offer more robust protection against chemical corrosion and moisture when compared with samples with no intermediate layer. In addition, results show that the performance of the ALD-AlOx barrier overlayer depends significantly on the ALD-growth process temperature. Because higher durability is observed in samples with less transparent TiN and NiO layers, we propose a figure of merit based on post-HTHH testing reflectivity change and specular reflective mirror surface area remaining after HTHH testing to judge overall barrier performance.

Ductile mode grinding of reaction-bonded silicon carbide mirrors.

The demand for reaction-bonded silicon carbide (RB-SiC) mirrors has escalated recently with the rapid development of space optical remote sensors used in astronomy or Earth observation. However, RB-SiC is difficult to machine due to its high hardness. This study intends to perform ductile mode grinding to RB-SiC, which produces superior surface integrity and fewer subsurface damages, thus minimizing the workload of subsequent lapping and polishing. For this purpose, a modified theoretical model for grain depth of cut of grinding wheels is presented, which correlates various processing parameters and the material characteristics (i.e., elastic module) of a wheel's bonding matrix and workpiece. Ductile mode grinding can be achieved as the grain depth of cut of wheels decreases to be less than the critical cut depth of workpieces. The theoretical model gives a roadmap to optimize the grinding parameters for ductile mode grinding of RB-SiC and other ultra-hard brittle materials. Its feasibility was validated by experiments. With the optimized grinding parameters for RB-SiC, the ductile mode grinding produced highly specular surfaces (with roughness of ∼2.2-2.8 nm Ra), which means the material removal mechanism of RB-SiC is dominated by plastic deformation rather than brittle fracture. Contrast experiments were also conducted on fused silica, using the same grinding parameters; this produced only very rough surfaces, which further validated the feasibility of the proposed model.

Fabrication, structural evaluation, optical and photoelectrochemical properties of soft lithography based 1D/2D surface patterned indium titanium oxide sol-gel thin film

For the first time, we report on successful fabrication of 1-dimensional (1D) nanoprism and 2-dimensional (2D) nanocone shaped surface patterned amorphous indium titanium oxide (INTO) sol-gel based mesoporous thin films on glass by soft lithography. Structural evaluation of the surface patterns over amorphous thin film surfaces was performed by atomic force and transmission electron microscopes as well as X-ray diffraction study. Chemical bonding/oxidation state of constituent elements in INTO film matrix was analyzed by FTIR and X-ray photoelectron spectroscopies. Maximum optical absorption and minimum specular surface reflection in visible region were noticed in 2D patterned film. The thin film with physical thickness over 100 nm was mesoporous in nature (~14% porosity) as measured by spectroscopic ellipsometer. A significant improvement in photoelectrochemical (PEC) activity was found in 2D patterned film under visible light that could be associated with the enhancement in light absorption/trapping by the periodic nanocones. Moreover, the existence of mesopores could provide excess active sites for electrolyte diffusion and mass transportation. Thus, the mesoporous 2D patterned thin film could have substantial opportunity in solar energy conversion. The facile technique could create an avenue for fabrication of complexed surface patterned thin films with improved PEC property.

Full-field 3D shape measurement of discontinuous specular objects by direct phase measuring deflectometry

AbstarctWith the advent of intelligent manufacturing, phase measuring deflectometry (PMD) has been widely studied for the measurement of the three-dimensional (3D) shape of specular objects. However, existing PMDs cannot measure objects having discontinuous specular surfaces. This paper presents a new direct PMD (DPMD) method that measures the full-field 3D shape of complicated specular objects. A mathematical model is derived to directly relate an absolute phase map to depth data, instead of the gradient. Two relevant parameters are calibrated using a machine vision-based method. On the basis of the derived model, a full-field 3D measuring system was developed. The accuracy of the system was evaluated using a mirror with known positions along an accurate translating stage. The 3D shape of a monolithic multi-mirror array having multiple specular surfaces was measured. Experimental results show that the proposed DPMD method can obtain the full-field 3D shape of specular objects having isolated and/or discontinuous surfaces accurately and effectively.

Multiple cues for visual perception of mirror and glass materials

The visual system can easily distinguish between a "mirror" object, which has a perfect specular surface like a polished metal, and a "glass" object, which has a transparent and refraction medium like ice under natural illumination, although an observer just observes a complex distorted image on the object surfaces from the surrounding illumination. In order to identify the visual cues to distinguish mirror and glass materials, we investigated a relationship between observers' performances and static/dynamic cues in visual stimulus.. Three randomly-bumped (potato-shape) objects were modeled by Blender 2.77 and were rendered as mirror and glass material objects by Mitsuba renderer (Jacob, 2010) under five real-world illuminations (Debevec, 2000; Adams et al., 2016). To examine both static and dynamic effects, we presented the static objects as image or the horizontally rotating objects as a video. The observer's task was to identify its material (mirror or glass) in a 2AFC paradigm. In this result, we found that a luminance distribution along a vertical direction in the image was significantly correlated with the performance in the static condition, and a ratio between positive and negative values of motion components along the object rotating direction in the video was significantly correlated with the performance in the dynamic condition. Moreover, for the stimuli color, which inverted from positive to negative values, the observers relatively more depended on a dynamic cue. This result can be caused by a decrease of a reliability of the static cue by the color inversion. These results suggest that the visual system effectively and comprehensively uses multiple cues in order to distinguish several materials in various contexts. Meeting abstract presented at VSS 2017

Transport phenomena in a slim vertical atmospheric pressure chemical vapor deposition reactor utilizing natural convection

The gas flow, heat and species transport in a slim vertical silicon chemical vapor deposition reactor for Minimal Fab were evaluated by a numerical analysis. The influences of the inlet gas flow condition on the gas flow direction and the gas phase temperature in the reactor were studied. When the gas flow rate was minimized, natural convection transports the precursor of trichlorosilane gas to the wafer surface. Because the wafer rotation, even very slow at 4rpm, adjusted the gas flow to shrink the hot region height above the wafer, the gas phase reaction was moderated for preparing the specular surface of the epitaxial film.

High-precision measurement of low reflectivity specular object based on phase measuring deflectometry

Phase measuring deflectometry (PMD) is a robust, noncoherent technique for the characterization of specular surface. For measuring high specular reflectivity surface, PMD can deliver micron radian range local gradient. However, when the measured surface has low specular reflectivity, the accuracy of the measured gradient is low since the captured fringe pattern shows low signal to noise ratio. The phase error characteristics in PMD system when testing low reflectivity surfaces are analyzed. The analysis illustrates that the random phase error increases rapidly while the nonlinear error drops slowly with the decreasing of the tested surface reflectivity. In order to attain high precision measurement of low reflectivity specular surface, a robust error reduction method based on wavelet de-noising is proposed to reduce the phase error. This error reduction method is compared with several other normally used methods in both simulation and experiment work. The method based on the wavelet de-noising shows better performance when measuring the low reflectivity specular surface.

Optical fringe-reflection deflectometry with sparse representation

Optical fringe-reflection deflectometry is a surprisingly attractive scratch detection technique for specular surfaces owing to its unparalleled local sensibility. Full-field surface topography is obtained from a measured normal field using gradient integration. However, there may not be an ideal measured gradient field for deflectometry reconstruction in practice. Both the non-integrability condition and various kinds of image noise distributions, which are present in the indirect measured gradient field, may lead to ambiguity about the scratches on specular surfaces. In order to reduce misjudgment of scratches, sparse representation is introduced into the Southwell curl equation for deflectometry. The curl can be represented as a linear combination of the given redundant dictionary for curl and the sparsest solution for gradient refinement. The non-integrability condition and noise permutation can be overcome with sparse representation for gradient refinement. Numerical simulations demonstrate that the accuracy rate of judgment of scratches can be enhanced with sparse representation compared to the standard least-squares integration. Preliminary experiments are performed with the application of practical measured deflectometric data to verify the validity of the algorithm.

Detecting dings and dents on specular car body surfaces based on optical flow

This paper introduces a new approach to detect defects cataloged as dings and dents on car body surfaces, which is currently one of the most important issues facing quality control in the automotive industry. Using well-known optical flow algorithms and the deflectometry principle, the method proposed in this work is able to detect all kind of anomalies on specular surfaces. Hence, our method consists of two main steps: first, in the pre-processing step, light patterns projected on the body surface sweep uniformly the area of inspection, whilst a new image fusion law, based on optical flow, is used to obtain a resulting fused image holding the information of all variations suffered by the projected patterns during the sweeping process, indicating the presence of anomalies; second, a new post-processing step is proposed that avoids the need of using pre-computed reference backgrounds in order to differentiate defects from other body features such as style-lines. To that end, the image background of the resulting fused image is estimated in the first place through a method based on blurring the image according to the direction of each pixel. Afterwards, the estimated image background is used in a new subtraction law through which defects are well differentiated from other surface deformations, allowing the detection of defects in the entire illuminated area. In addition, since our approach, together with the system used, computes defects in less than 15s, it satisfies the assembly plants time requirements. Experimental results presented in this paper are obtained from the industrial automatic quality control system QEyeTunnel employed in the production line at the Mercedes-Benz factory in Vitoria, Spain. A complete analysis of the algorithm performance will be shown here, together with several tests proving the robustness and reliability of our proposal.

Photometric Stereo by Hemispherical Metric Embedding

Photometric Stereo methods seek to reconstruct the 3d shape of an object from motionless images obtained with varying illumination. Most existing methods solve a restricted problem where the physical reflectance model, such as Lambertian reflectance, is known in advance. In contrast, we do not restrict ourselves to a specific reflectance model. Instead, we offer a method that works on a wide variety of reflectances. Our approach uses a simple yet uncommonly used property of the problem - the sought after normals are points on a unit hemisphere. We present a novel embedding method that maps pixels to normals on the unit hemisphere. Our experiments demonstrate that this approach outperforms existing manifold learning methods for the task of hemisphere embedding. We further show successful reconstructions of objects from a wide variety of reflectances including smooth, rough, diffuse and specular surfaces, even in the presence of significant attached shadows. Finally, we empirically prove that under these challenging settings we obtain more accurate shape reconstructions than existing methods.

A Novel Active Imaging Model to Design Visual Systems: A Case of Inspection System for Specular Surfaces.

The use of visual information is a very well known input from different kinds of sensors. However, most of the perception problems are individually modeled and tackled. It is necessary to provide a general imaging model that allows us to parametrize different input systems as well as their problems and possible solutions. In this paper, we present an active vision model considering the imaging system as a whole (including camera, lighting system, object to be perceived) in order to propose solutions to automated visual systems that present problems that we perceive. As a concrete case study, we instantiate the model in a real application and still challenging problem: automated visual inspection. It is one of the most used quality control systems to detect defects on manufactured objects. However, it presents problems for specular products. We model these perception problems taking into account environmental conditions and camera parameters that allow a system to properly perceive the specific object characteristics to determine defects on surfaces. The validation of the model has been carried out using simulations providing an efficient way to perform a large set of tests (different environment conditions and camera parameters) as a previous step of experimentation in real manufacturing environments, which more complex in terms of instrumentation and more expensive. Results prove the success of the model application adjusting scale, viewpoint and lighting conditions to detect structural and color defects on specular surfaces.

Envisat RA-2 Individual Echoes: A Unique Dataset for a Better Understanding of Inland Water Altimetry Potentialities

The exploitation of synthetic aperture properties in nadir-looking radars is opening new scenarios in the framework of satellite radar altimetry. Both recent and upcoming missions including Cryosat-2, Sentinel-3, Sentinel-6 and SWOT take benefit from the coherent processing of radar data, aimed at improving range measurements in particular contexts, such as ice, open ocean, coastal zone, and even inland waters. This work investigates the possibilities offered by current and future satellite radar altimetry missions for the study of inland water bodies, probing into the peculiarities of the expected radar returns and their potential usage. In this regard, signals collected by the RA-2 instrument (Radar Altimeter 2) onboard the Envisat mission offer an unprecedented possibility, even with a relatively low pulse repetition frequency, to analyze the peculiarities of actual signals for detecting and ranging small water surfaces. In particular, the RA-2 instrument offers a global archive of Individual Echoes (IEs), collected at the native sampling rate of 1795 Hz, in addition to the 18 Hz data obtained by incoherent averaging, which are typically delivered to the users as standard products. RA-2 shares with future radar platforms such as Sentinel-6 a continuous and interleaved working modality, as was recommended by the scientific community in designing next missions’ requirements. This is a further reason to consider the usage of RA-2 IEs as particularly attractive. Whilst only available for a small percentage of the earth’s surface, sufficient IE data exist to study the height retrieval capability of these echoes, in particular for what concerns small water bodies, where we show that enough coherence is exhibited for focusing relatively narrow surfaces and range them correctly. A peculiar aspect of this work lies in the assumption that most of the returned echoes (in RA-2 IEs) are specular. A theoretical framework is developed according to this assumption, which is validated by investigating real RA-2 data and observing their related specular features. In particular, we discuss how specular echoes are expected to be very common in inland altimetry, and are most often associated with small to medium size lakes and rivers. This paper illustrates the expected electromagnetic behavior of specular water targets by exploiting the classical radar cross-section (RCS) theory for specular surfaces. Results from the model are compared with real IE data in three selected case studies, regarding two rivers of variable width and one flood plain, in order to check different hydrological regimes. The model very closely matches the data in all cases, making the results of this validation activity very promising. In particular, we demonstrate the feasibility of using satellite radar altimetry in rivers much smaller than what was considered possible until now.