Background: The leaves and owers of Hibiscus rosa-sinensis have hair growth-promoting and anti-greying properties as well as excellent antimicrobial and antifungal activity. Active ingredients when added in shampoos which classify them as drugs. Medicated shampoos, in addition to cleansing and conditioning, deliver extra benets to the hair and scalp. Objectives:The objective of this study was to formulate a shampoo making use of the therapeutic activities of Hibiscus rosa-sinensis Linn. Methods: The study was carried out using standardized procedures at ST. WILFRED'S INSTITUTE OF PHARMACY, Panvel from 21 August 2021 to 21 December 2021. Our study included identication, quantitative analysis, extraction, pre-formulation studies, evaluation along with all other standard procedures required. Results: The alcoholic extracts of Hibiscus rosa-sinensis Linn. showed antimicrobial and antifungal activity. The formulated shampoo preparation passed all the recommended standard evaluation tests viz: Organoleptic properties, rheological evaluations, pH, percent solid test, foam producing, and foam retention capability, wetting time, surface tension, dirt dispersion, and cleansing action. Conclusion: The formulated shampoo revealed the ideal characteristics of the shampoo and is devoid of any harmful preservatives like paraben. It can be used as a safer alternative to its synthetic counterparts.