ABSTRACT This study evaluates the performance and emission characteristics of diesel, fish biodiesel (comprising 20% fish oil and 80% diesel), and fish biodiesel using Fe and Zn-coated zeolite catalytic converters. The research aims to mitigate environmental challenges associated with diesel engines by exploring the efficacy of metal-doped zeolite catalysts in reducing harmful emissions. Fish biodiesel was derived from fish waste via transesterification and tested in a single-cylinder diesel engine. Key performance metrics, including Brake Specific Fuel Consumption, Brake Thermal Efficiency, Exhaust Gas Temperature, cylinder pressure, Heat Release Rate, and ignition delay, were measured. Emission characteristics such as carbon monoxide, hydrocarbon, nitrogen oxide, and smoke opacity were also analyzed. Results showed diesel had the lowest Specific fuel consumption, ranging from 730 g/kWh at 25% load to 320 g/kWh at full load. Fish biodiesel exhibited higher Specific fuel consumption, from 770 g/kWh to 350 g/kWh. Regarding emissions, the NOx of the biodiesel increased significantly compared to diesel; the use of a catalytic converter has reduced the NOx emission to a maximum extent of 37.5% at full load for a Fe-coated converter. The Zn-coated converter also improved emissions by up to 33% for NO but was slightly less effective than the Fe-coated converter. The study concludes that Fe-coated zeolite catalytic converters significantly enhance biodiesel-fueled diesel engines’ performance and emission characteristics. Both catalytic converters reduced the smoke emission significantly. These findings highlight the potential for developing more efficient and eco-friendly emission control technologies and promoting using renewable transportation fuels.