The area involved in this study is Sirt basin, which is located in the north central part of Libya within the bounder's 27N-33N and 16E-22E. The study involves the analysis of gravity and magnetic data to delineate structures and faults and to locate any major structures. The produced Bouguer gravity map shows prominent NW-SE and N-NW trends. Isostatic residual map is characterized by a dominant NW– SE trend in the study area. This is clearly evident in the isostatic residual. The main trending anomalies are in the northern and southeastern parts of the study area with NW-SE orientation. A strong NW-SE trend is truncated by E-W trending in the southeastern and southwestern parts of the area. This is consistent with change of tectonic zones. The magnetic expression in the northern part of Ajdabiya trough is characterized by NW-SE trending structures which coincide with late Cretaceous structures of the Sirt basin, while the southern part is characterised by NE-SW trending features which coincide with a late Paleozoic trend. The northern part of the Ajdabiya trough is separated from the southern part by a prominent NE-SW lineament that is expressed in both the gravity and magnetic data. It is interpreted as a basement fault, which separates a thicker southern crust from a thinner northern crust. The high gravity anomaly within the northern part of the Ajdabiya trough is interpreted as a result of mantle upwelling which caused thinning of the continental crust beneath the northern part of the Ajdabiya trough. The Total horizontal derivative results of Gravity, 3D Euler Deconvolution of gravity and magnetic data magnetic anomalies produced features trending similar to the positions of tectonic and geological information from the Sirt basin. High gradient values delineate NNW-SSE to N-S and NW-SE trends which mark the faulted southwestern, southern, northern and central boundaries of the basin, respectively. New faults with orientations NNW-SSE trends along the southwestern flank of the Sirt basin and is truncated by E-W faults dividing it into segments. Strong N-S lineaments occur over the southern and central part of study area and are well indicated by the 3D Euler Deconvolution. From this study the 3D Euler Deconvolution provides very useful information of the rift structures.