Single Photon Time Resolution Research Articles

Time-Resolving Characteristics of Pixel- and Charge-Division-Type Position-Sensitive SiPMs With Epitaxial Quenching Resistors

Silicon photomultipliers (SiPMs) with epitaxial quenching resistors (EQR SiPMs) are easier to fabricate with small microcells that provide a large fill factor and an adequate dynamic range. They are suitable for use as pixel-type and charge-division-type position-sensitive (PS) devices. In this paper, an EQR SiPM line array, with 0.12 $\times $ 0.12 mm2 active area and 120 microcells in one element, provided a single-photon time resolution (SPTR) of 36.9 ± 1.0 ps full-width at half-maximum. A tetra-lateral charge-division-type PS-SiPM demonstrated a lateral transmission time delay of 0.7 ps/ $\mu \text{m}$ . This linearity between the lateral transmission time delay and the relative distance from the light spot position to the opposite anodes may be used to quantify the position resolution for this type of PS-SiPM. The limiting factors which affect the time-resolving characteristics of EQR SiPM, such as electronic noise and lateral transmission time delay, were also discussed.

A comparative study of the time performance between NINO and FlexToT ASICs

Universitat de Barcelona (UB) and CIEMAT have designed the FlexToT ASIC for the front-end readout of SiPM-based scintillator detectors. This ASIC is aimed at time of flight (ToF) positron emission tomography (PET) applications. In this work we have evaluated the time performance of the FlexToT v2 ASIC compared to the NINO ASIC, a fast ASIC developped at CERN. NINO electronics give 64 ps sigma for single-photon time resolution (SPTR) and 93 ps FWHM for coincidence time resolution (CTR) with 2 × 2 × 5 mm3 LSO:Ce,Ca crystals and S13360-3050CS SiPMs. Using the same SiPMs and crystals, the FlexToT v2 ASIC yields 91 ps sigma for SPTR and 123 ps FWHM for CTR. Despite worse time performace than NINO, FlexToT v2 features lower power consumption (11 vs. 27 mW/ch) and linear ToT energy measurement.

Small FDIRC designs

In this article11The paper was presented at the RICH 2016 conference, Bled, Slovenia, September 2016. we explore the angular resolution limits attainable in small FDIRC designs taking advantage of the new highly pixelated detectors that are now available. Since the basic FDIRC design concept attains its particle separation performance mostly in the angular domain as measured by two-dimensional pixels, this paper relies primarily on a pixel-based analysis, with additional chromatic corrections using the time domain, requiring single photon timing resolution at a level of 100–200ps only. This approach differs from other modern DIRC design concepts such as TOP or TORCH detectors,22See presentation at this conference. whose separation performances rely more strongly on time-dependent analyses. We find excellent single photon resolution with a geometry where individual bars are coupled to a single plate, which is coupled in turn to a cylindrical lens focusing camera.

SiPM readout for the SHiP timing detector

The SHiP experiment is a new general purpose fixed target experiment proposed at the CERN SPS accelerator. A dedicated beam line in the North Area will be aimed at a fixed target station, followed by a magnetic shield to reduce beam induced background. The experiment will comprise a compact tau neutrino detector and a detector to search for hidden particles. Background rejection is ensured by use of background taggers and a dedicated timing detector. The timing detector will reduce combinatorial di-muon background by requiring incoming particles to be coincident in time within 100 ps. One option for the timing detector consists of columns of horizontal scintillating bars read-out on each end by Silicon Photomultiplier arrays. This study includes characterization of SiPMs from different manufacturers to be used in the timing detector in terms of Current-Voltage behavior, cross-talk probability, dark count rate and single photon timing resolution. Initial results of the time resolution of a EJ-200 scintillating bar read out on both ends by a single SiPM are presented.

Digital Signal Processing for SiPM Timing Resolution

Digital signal processing (DSP) is an emerging trend in experimental studies and applications of various detectors including SiPMs. In particular, the DSP is recognized as a promising approach to improve coincidence timing resolution (CTR) of fast SiPM-based scintillation detectors. Single photon timing resolution (SPTR) is one of the key parameters affecting CTR, especially important in a case when CTR is approaching to its ultimate limits as, for example, highly demanded in Time-of-Flight PET. To study SiPM timing resolution, we developed a special DSP software and applied it to both SPTR and CTR measurements. These measurements were carried out using 3x3 mm2 KETEK SiPM samples of timing optimized and standard designs with 405 nm picosecond laser for SPTR and with 3x3x5 mm3 LYSO crystals and 511 keV Na-22 source for CRT. Results of the study are useful for further improvements of DSP algorithms and SiPM designs for fast timing.

A comprehensive characterization of the time resolution of the Philips Digital Photon Counter

Photodetectors with excellent time resolution are becoming increasingly important in many applications in medicine, high energy- and nuclear physics applications, biology, and material science. Silicon photomultipliers (SiPM) are a novel class of solid-state photodetectors with good timing properties. While the time resolution of analog SiPMs has been analyzed by many groups, the time resolution of the digital photon counter (DPC) developed by Philips has not yet been fully characterised. Here, the timing capabilities of the DPC are studied using a femtosecond laser. The time resolution is determined for complete dies, single pixels, and individual single photon avalanche diodes (SPADs). The measurements cover a broad dynamic range, from intense illumination down to the single-photon level, and were performed at various temperatures between 0°C and 20°C. The measured single photon time resolution (SPTR) ranges from 101 ps FWHM for the DPC3200 sensor pixel to 247 ps FWHM for the DPC6400 sensor die. An extensive study of the single-SPAD time resolution, ranging from single photon to very high laser intensities (∼1000 photons per pulse), yielded a time resolution of 48 ps FWHM at the single-photon level.

Single photon time resolution of state of the art SiPMs

Comparison of the timing performance of different silicon photomultipliers (SiPMs) can be useful for applications that employ these devices. In our study, we characterize some of the currently available SiPMs to compare the single photon time resolution (SPTR) values measured using a 420 nm laser with a pulse width of 42 ps FWHM. SPTR values in the range of 175–330 ps FWHM were measured for most 3 × 3 mm2 and 4 × 4 mm2 devices and varied with the producer and the type of the SiPM. Factors influencing the SPTR including the area, cell to cell non-uniformity and the SPAD (single photon avalanche diode) jitter were investigated by the use of laser light focused at the level of a SPAD within a SiPM. The standard deviation of the SPTR values measured among different cells within a Hamamatsu Through Silicon Via SiPM was found to be less than 5 ps. When measured with focused laser the values of SPTR, the signal delay and the relative PDE were found to vary among different points within a SPAD of a SiPM. We found that such variation causes the values of SPTR measured with focused illumination to be better than when measured with diffuse illumination which probes the entire SiPM active surface. SPTR values close to 20 ps FWHM have been measured for standalone single SPADs produced by FBK after correcting for the laser jitter and the acquisition jitter. The performed tests helped us to understand the limits of the SPAD jitter. We infer that the dominant factor contributing to the degradation of the SPTR from the level of a SPAD to a SiPM is mostly driven by detector noise, if the influence of the signal delay time spread is reduced to a minimum.

State of the art timing in TOF-PET detectors with LuAG, GAGG and L(Y)SO scintillators of various sizes coupled to FBK-SiPMs

Time of flight (TOF) in positron emission tomography (PET) has experienced a revival of interest after its first introduction in the eighties. This is due to a significant progress in solid state photodetectors (SiPMs) and newly developed scintillators (LSO and its derivatives). Latest developments at Fondazione Bruno Kessler (FBK) lead to the NUV-HD SiPM with a very high photon detection efficiency of around 55%. Despite the large area of 4×4 mm2 it achieves a good single photon time resolution (SPTR) of 180±5ps FWHM. Coincidence time resolution (CTR) measurements using LSO:Ce codoped with Ca scintillators yield best values of 73±2ps FWHM for 2×2×3 mm3 and 117±3ps for 2×2×20 mm3 crystal sizes. Increasing the crystal cross-section from 2×2 mm2 to 3×3 mm2 a non negligible CTR deterioration of approximately 7ps FWHM is observed. Measurements with LSO:Ce codoped Ca and LYSO:Ce scintillators with various cross-sections (1×1 mm2 - 4×4 mm2) and lengths (3mm - 30mm) will be a basis for discussing on how the crystal geometry affects timing in TOF-PET. Special attention is given to SiPM parameters, e.g. SPTR and optical crosstalk, and their measured dependency on the crystal cross-section. Additionally, CTR measurements with LuAG:Ce, LuAG:Pr and GGAG:Ce samples are presented and the results are interpreted in terms of their scintillation properties, e.g. rise time, decay time, light yield and emission spectra.

Time-resolved single-photon detection module based on silicon photomultiplier: A novel building block for time-correlated measurement systems

We present the design and preliminary characterization of the first detection module based on Silicon Photomultiplier (SiPM) tailored for single-photon timing applications. The aim of this work is to demonstrate, thanks to the design of a suitable module, the possibility to easily exploit SiPM in many applications as an interesting detector featuring large active area, similarly to photomultipliers tubes, but keeping the advantages of solid state detectors (high quantum efficiency, low cost, compactness, robustness, low bias voltage, and insensitiveness to magnetic field). The module integrates a cooled SiPM with a total photosensitive area of 1 mm(2) together with the suitable avalanche signal read-out circuit, the signal conditioning, the biasing electronics, and a Peltier cooler driver for thermal stabilization. It is able to extract the single-photon timing information with resolution better than 100 ps full-width at half maximum. We verified the effective stabilization in response to external thermal perturbations, thus proving the complete insensitivity of the module to environment temperature variations, which represents a fundamental parameter to profitably use the instrument for real-field applications. We also characterized the single-photon timing resolution, the background noise due to both primary dark count generation and afterpulsing, the single-photon detection efficiency, and the instrument response function shape. The proposed module can become a reliable and cost-effective building block for time-correlated single-photon counting instruments in applications requiring high collection capability of isotropic light and detection efficiency (e.g., fluorescence decay measurements or time-domain diffuse optics systems).

In-depth study of single photon time resolution for the Philips digital silicon photomultiplier

The digital silicon photomultiplier (SiPM) has been commercialised by Philips as an innovative technology compared to analog silicon photomultiplier devices. The Philips digital SiPM, has a pair of time to digital converters (TDCs) connected to 12800 single photon avalanche diodes (SPADs). Detailed measurements were performed to understand the low photon time response of the Philips digital SiPM. The single photon time resolution (SPTR) of every single SPAD in a pixel consisting of 3200 SPADs was measured and an average value of 85 ps full width at half maximum (FWHM) was observed. Each SPAD sends the signal to the TDC with different signal propagation time, resulting in a so called trigger network skew. This distribution of the trigger network skew for a pixel (3200 SPADs) has been measured and a variation of 50 ps FWHM was extracted. The SPTR of the whole pixel is the combination of SPAD jitter, trigger network skew, and the SPAD non-uniformity. The SPTR of a complete pixel was 103 ps FWHM at 3.3 V above breakdown voltage. Further, the effect of the crosstalk at a low photon level has been studied, with the two photon time resolution degrading if the events are a combination of detected (true) photons and crosstalk events. Finally, the time response to multiple photons was investigated.

Measurement of intrinsic rise times for various L(Y)SO and LuAG scintillators with a general study of prompt photons to achieve 10 ps in TOF-PET

The coincidence time resolution (CTR) of scintillator based detectors commonly used in positron emission tomography is well known to be dependent on the scintillation decay time () and the number of photons detected (), i.e. . However, it is still an open question to what extent the scintillation rise time () and other fast or prompt photons, e.g. Cherenkov photons, at the beginning of the scintillation process influence the CTR. This paper presents measurements of the scintillation emission rate for different LSO type crystals, i.e. LSO:Ce, LYSO:Ce, LSO:Ce codoped Ca and LGSO:Ce. For the various LSO-type samples measured we find an average value of 70 ps for the scintillation rise time, although some crystals like LSO:Ce codoped Ca seem to have a much faster rise time in the order of 20 ps. Additional measurements for LuAG:Ce and LuAG:Pr show a rise time of 535 ps and 251 ps, respectively. For these crystals, prompt photons (Cherenkov) can be observed at the beginning of the scintillation event. Furthermore a significantly lower rise time value is observed when codoping with calcium. To quantitatively investigate the influence of the rise time to the time resolution we measured the CTR with the same L(Y)SO samples and compared the values to Monte Carlo simulations. Using the measured relative light yields, rise- and decay times of the scintillators we are able to quantitatively understand the measured CTRs in our simulations. Although the rise time is important to fully explain the CTR variation for the different samples tested we determined its influence on the CTR to be in the order of a few percent only. This result is surprising because, if only photonstatistics of the scintillation process is considered, the CTR would be proportional to the square root of the rise time. The unexpected small rise time influence on the CTR can be explained by the convolution of the scintillation rate with the single photon time resolution (SPTR) of the photodetector and the photon travel spread (PTS) in the crystal. The timing benefits of prompt photons at the beginning of the scintillation process (Cherenkov etc) are further studied, which leads to the conclusion that the scintillation rise time, SPTR and PTS have to be lowered simultaneously to fully profit from these fast photons in order to improve the CTR significantly.

Advances in digital SiPMs and their application in biomedical imaging

Similar to analog silicon photomultipliers (SiPMs), digital SiPMs (dSiPMs) essentially consist of an array of single-photon avalanche photodiodes (SPADs). Instead of a passive quench resistor, however, an active quenching circuit is locally integrated with each SPAD, making the sensor response faster and less sensitive to the gains of the individual SPADs. Moreover, additional circuits for the fully digital acquisition, processing, and readout of optical signals are integrated within the sensor. As a result, dSiPMs offer high photo-detection efficiency, high single-photon time resolution (SPTR), and high uniformity, as well as many practical advantages, such as a very compact form factor, low voltage operation, magnetic field compatibility, high stability of operation, low gain drift, and a high degree of scalability. At the same time, dSiPMs represent a new paradigm in low-level light sensing technology. That is, their fully digital operation makes them true photon counting devices, preserving at least partly the discrete spatio-temporal structure of the information embedded in the optical signal. This means that the operation of dSiPMs can be fully understood only in statistical terms, but also opens up novel possibilities for extracting information from the measured data. So far, the main driver behind the development of dSiPMs has been the detection of scintillation pulses in detectors for time-of-flight (TOF) positron emission tomography (PET). Several types of dSiPM have been developed in recent years. Moreover, first imaging devices based on dSiPMs have been realized by various groups. This review summarizes the main dSiPM concepts and technologies currently under development, provides an overview of the results obtained recently with dSiPMs-based PET and SPECT devices, and presents a critical outlook on the challenges and chances for dSiPMs in future radiomolecular imaging systems.

Spectrally Resolved Single-Photon Timing of Silicon Photomultipliers for Time-Domain Diffuse Spectroscopy

We characterized the single-photon timing response function of various silicon photomultipliers (SiPMs) over a broad (500-1100 nm) spectral range. We selected two SiPM manufacturers, and we investigated two active areas, i.e., a small (1-1.69 mm <sup xmlns:mml="http://www.w3.org/1998/Math/MathML" xmlns:xlink="http://www.w3.org/1999/xlink">2</sup> ) and a large (9 mm <sup xmlns:mml="http://www.w3.org/1998/Math/MathML" xmlns:xlink="http://www.w3.org/1999/xlink">2</sup> ) one, for each of them. We demonstrate that selected SiPMs are suitable for time-resolved diffuse optics (DO) applications where a very large detection area and sensitivity down to single photons are crucial to detecting the very faint return signal from biological tissues, like the brain, thus allowing replacement of photomultiplier tubes and opening the way to a novel generation of DO multichannel instrumentation. Due to our custom front-end electronics, we show the world's best single-photon timing resolution for SiPMs, namely, 57-ps full-width at half maximum for Hamamatsu 1.69 mm <sup xmlns:mml="http://www.w3.org/1998/Math/MathML" xmlns:xlink="http://www.w3.org/1999/xlink">2</sup> and 115 ps for Excelitas 9 mm <sup xmlns:mml="http://www.w3.org/1998/Math/MathML" xmlns:xlink="http://www.w3.org/1999/xlink">2</sup> . Even further, we provide a thorough spectral investigation of the full single-photon timing response function, also detailing diffusion tails' time constants and dynamic range. The achieved insight and the reported performance open the way to a widespread diffusion of SiPMs not just in many-photon regimes (e.g., PET) but at single-photon counting regimes like DO as well.

Time-based position estimation in monolithic scintillator detectors

Gamma-ray detectors based on bright monolithic scintillation crystals coupled to pixelated photodetectors are currently being considered for several applications in the medical imaging field. In a typical monolithic detector, both the light intensity and the time of arrival of the earliest scintillation photons can be recorded by each of the photosensor pixels every time a gamma interaction occurs. Generally, the time stamps are used to determine the gamma interaction time while the light intensities are used to estimate the 3D position of the interaction point. In this work we show that the spatio-temporal distribution of the time stamps also carries information on the location of the gamma interaction point and thus the time stamps can be used as explanatory variables for position estimation. We present a model for the spatial resolution obtainable when the interaction position is estimated using exclusively the time stamp of the first photon detected on each of the photosensor pixels. The model is shown to be in agreement with experimental measurements on a 16 mm × 16 mm × 10 mm LSO : Ce,0.2%Ca crystal coupled to a digital photon counter (DPC) array where a spatial resolution of 3 mm (root mean squared error) is obtained. Finally we discuss the effects of the main parameters such as scintillator rise and decay time, light output and photosensor single photon time resolution and pixel size.

Analysis of transit time spread on FBK silicon photomultipliers

In this paper we studied one of the aspects potentially limiting the single-photon time-resolution (SPTR) of the silicon photomultiplier (SiPM): the transit time spread (TTS). We illuminated the SiPM in different positions with a fast-pulsed laser collimated to a circular spot of 0.2 mm-diameter and acquired bi-dimensional maps of the avalanche-signal arrival time of RGB and RGB-HD SiPMs, produced at FBK. We studied the effect of both the number of bonding wires connecting the device to the package and the layout of the top-metal connection (on the device). We found that the TTS does not simply depend on the trace length between the cell and the bonding pad and it could vary in the range between tens of picoseconds (with 3 bonding connections) to more than one hundred of picoseconds (with one connection).

A compact high resolution flat panel PET detector based on the new 4-side buttable MPPC for biomedical applications

Compact high-resolution panel detectors using virtual pinhole (VP) PET geometry can be inserted into existing clinical or pre-clinical PET systems to improve regional spatial resolution and sensitivity. Here we describe a compact panel PET detector built using the new Though Silicon Via (TSV) multi-pixel photon counters (MPPC) detector. This insert provides high spatial resolution and good timing performance for multiple bio-medical applications. Because the TSV MPPC design eliminates wire bonding and has a package dimension which is very close to the MPPC׳s active area, it is 4-side buttable. The custom designed MPPC array (based on Hamamatsu S12641-PA-50(x)) used in the prototype is composed of 4×4 TSV-MPPC cells with a 4.46mm pitch in both directions. The detector module has 16×16 lutetium yttrium oxyorthosilicate (LYSO) crystal array, with each crystal measuring 0.92×0.92×3mm3 with 1.0mm pitch. The outer diameter of the detector block is 16.8×16.8mm2. Thirty-two such blocks will be arranged in a 4×8 array with 1mm gaps to form a panel detector with detection area around 7cm×14cm in the full-size detector. The flood histogram acquired with 68Ge source showed excellent crystal separation capability with all 256 crystals clearly resolved. The detector module׳s mean, standard deviation, minimum (best) and maximum (worst) energy resolution were 10.19%, ±0.68%, 8.36% and 13.45% FWHM, respectively. The measured coincidence time resolution between the block detector and a fast reference detector (around 200 ps single photon timing resolution) was 0.95ns. When tested with Siemens Cardinal electronics the performance of the detector blocks remain consistent. These results demonstrate that the TSV-MPPC is a promising photon sensor for use in a flat panel PET insert composed of many high resolution compact detector modules.

Quality control of the TSV multi-pixel photon counter arrays, and modules for the external plate of EndoTOF-PET ultrasound detector

The aim of the EndoTOFPET-US collaboration is to develop a multi-modal imaging tool combining ultrasound with time-of-flight positron emission tomography into an endoscopic imaging device. One of the objectives of this scanner is to reach a coincidence time resolution of 200ps full width at half maximum. The external detector is constructed with 256 matrices of 4×4 lutetium–yttrium oxyorthosilicate scintillating crystals, each with a size of 3.5×3.5×15mm3, coupled to 256 Hamamatsu TSV multi-pixel photon counter arrays (S12643-050CN). A full characterisation of these arrays has been performed in order to assure the quality of the arrays prior to the gluing to the crystal matrices. The breakdown voltage, dark count rate and single photon time resolution have been measured both at DESY and CERN. After this characterisation, the crystal matrices were glued to the multi-pixel photon counter arrays. The coincidence time resolution of each module has been measured at CERN using an ultra-fast amplifier-discriminator as the reference readout ASIC. Results of the characterisation of multi-pixel photon counter arrays and the crystal modules are presented here.

Analysis of single-photon time resolution of FBK silicon photomultipliers

We characterized and analyzed an important feature of silicon photomultipliers: the single-photon time resolution (SPTR). We characterized the SPTR of new RGB (Red–Green–Blue) type Silicon Photomultipliers and SPADs produced at FBK (Trento, Italy), studying its main limiting factors.We compared time resolution of 1×1mm2 and 3×3mm2 SiPMs and a single SiPM cell (i.e. a SPAD with integrated passive-quenching), employing a mode-locked pulsed laser with 2-ps wide pulses. We estimated the contribution of front-end electronic-noise, of cell-to-cell uniformity, and intrinsic cell time-resolution. At a single-cell level, we compared the results obtained with different layouts. With a circular cell with a top metallization covering part of the edge and enhancing the signal extraction, we reached ~20ps FWHM of time resolution.

Characterization of Single-Photon Time Resolution: From Single SPAD to Silicon Photomultiplier

In this paper, we report on the characterization of the single-photon time resolution (SPTR) of the RGB (Red-Green-Blue) type silicon photomultipliers (SiPM) produced at FBK. We measured and compared single-photon timing jitter of 1 ×1 mm <sup xmlns:mml="http://www.w3.org/1998/Math/MathML" xmlns:xlink="http://www.w3.org/1999/xlink">2</sup> and 3 ×3 mm <sup xmlns:mml="http://www.w3.org/1998/Math/MathML" xmlns:xlink="http://www.w3.org/1999/xlink">2</sup> SiPMs, and also of square SPADs with integrated passive quenching, identical to the cells composing the SiPMs. We reached a single-photon time resolution of about 180 ps full-width at half-maximum for 3 ×3 mm <sup xmlns:mml="http://www.w3.org/1998/Math/MathML" xmlns:xlink="http://www.w3.org/1999/xlink">2</sup> SiPM, 80 ps for 1 ×1 mm <sup xmlns:mml="http://www.w3.org/1998/Math/MathML" xmlns:xlink="http://www.w3.org/1999/xlink">2</sup> SiPM and less than 50 ps for single cells. From measurements with pinholes placed in front of 1 ×1 mm <sup xmlns:mml="http://www.w3.org/1998/Math/MathML" xmlns:xlink="http://www.w3.org/1999/xlink">2</sup> detector we see a very good cell-to-cell uniformity: it is not a limiting factor for time resolution. We also characterized the timing jitter of SiPMs as a function of the number of photons per laser pulse (N) finding that it does not decrease exactly with the square root of N because of the optical crosstalk between cells.

Systematic study of new types of Hamamatsu MPPCs read out with the NINO ASIC

Over the last decade there have been commercial TOF-PET scanners constructed using Photo-Multiplier Tubes (PMT) that have achieved ~500ps FWHM Coincidence Time Resolution (CTR). A new device known as the Silicon PhotoMultiplier (SiPM) has the potential to overcome some of the limitations of the PMT. Therefore implementing a SiPM based TOF-PET scanner is of high interest. Recently Philips has introduced a TOF-PET scanner that uses digital Silicon PhotoMultipliers (d-SiPMs) which has a CTR of 350ps. Here we will report on the timing performance of two Hamamatsu 3×3mm2 analogue-SiPMs read out with the NINO ASIC: this is an ultra-fast amplifier/discriminator with a differential architecture. The differential architecture is very important since the single-ended readout uses the ground as the signal return; as the ground is also the reference level for the discriminators, the result is high crosstalk and degraded time resolution. However differential readout allows the scaling up from a single cell to a multi-cell device with no loss of time resolution; this becomes increasingly important for the highly segmented detectors that are being built today, both for particle and for medical instrumentation.We obtained excellent results for both the Single Photon Time Resolution (SPTR) and for the CTR using a LYSO crystal of 15mm length. Such a crystal length has sufficient detection efficiency for 511keV gammas to make an excellent PET device. The results presented here are proof that a TOF-PET detector with a CTR of 175ps is indeed possible. This is the first step that defines the starting point of our SuperNINO project.