Shear Band Formation Research Articles

Novel Class of Crystal/Glass Ultrafine Nanolaminates with Large and Tunable Mechanical Properties.

The control of local heterogeneities in metallic glasses (MGs) represents an emerging field to improve their plasticity, preventing the propagation of catastrophic shear bands (SBs) responsible for the macroscopically brittle failure. To date, a nanoengineered approach aimed at finely tuning local heterogeneities controlling SB nucleation and propagation is still missing, hindering the potential to develop MGs with large and tunable strength/ductility balance and controlled deformation behavior. In this work, we exploited the potential of pulsed laser deposition (PLD) to synthesize a novel class of crystal/glass ultrafine nanolaminates (U-NLs) in which a ∼4 nm thick crystalline Al separates 6 and 9 nm thick Zr50Cu50 glass nanolayers, while reporting a high density of sharp interfaces and large chemical intermixing. In addition, we tune the morphology by synthesizing compact and nanogranular U-NLs, exploiting, respectively, atom-by-atom or cluster-assembled growth regimes. For compact U-NLs, we report high mass density (∼8.35 g/cm3) and enhanced and tunable mechanical behavior, reaching maximum values of hardness and yield strength of up to 9.3 and 3.6 GPa, respectively. In addition, we show up to 3.6% homogeneous elastoplastic deformation in compression as a result of SB blocking by the Al-rich sublayers. On the other hand, nanogranular U-NLs exhibit slightly lower yield strength (3.4 GPa) in combination with enhanced elastoplastic deformation (∼6%) followed by the formation of superficial SBs, which are not percolative even at deformations exceeding 15%, as a result of the larger free volume content within the cluster-assembled structure and the presence of crystal/glass nanointerfaces, enabling to accommodate SB events. Overall, we show how PLD enables the synthesis of crystal/glass U-NLs with ultimate control of local heterogeneities down to the atomic scale, providing new nanoengineered strategies capable of deep control of the deformation behavior, surpassing traditional trade-off between strength and ductility. Our approach can be extended to other combinations of metallic materials with clear interest for industrial applications such as structural coatings and microelectronics (MEMS and NEMS).

Hot deformation behavior and microstructural evolution of dual phase Ni48.6 Al10.3 Co17 Cr7.5 Fe9 Ti5.8 Ta0.6 Mo0.8 W0.4 high entropy alloy

The present study reports the hot deformation behavior, microstructural evolution, and the alloying effects of refractory elements (Ta, Mo, W) in Ni48.6 Al10.3 Co17 Cr7.5 Fe9 Ti5.8 Ta0.6 Mo0.8 W0.4 (at. %) high entropy alloy (HEA). The vacuum arc melted specimens were characterized using a scanning electron microscope, X-ray diffractometer, and Differential scanning calorimetry, which revealed the two-phase structure consisting of γ′ precipitates embedded in the γ matrix. The Energy Dispersive Spectroscopy analysis in a scanning electron microscope revealed that Mo and W partitioned into the dendritic region (KMo = 1.23 and KW = 1.28) while Ta is found to be partitioned in the interdendritic region composed of mostly γ′ precipitates (KTa = 0.67). Further, the specimens were subjected to hot deformation in the 800 °C - 1100 °C temperature range at the strain rate of 0.01s−1. The maximum flow strength was around 278 MPa and 183 MPa at 1050 °C and 1100 °C, respectively. The flow behavior is correlated with the microstructure evolution, which is characterized using electron backscattered diffraction (EBSD). In the cases of hot deformation below 1000 °C, localized plastic flow in the form of shear bands developed in coarse grain microstructure, whereas fine grains evolved due to dynamic recrystallization (DRX) in the sample deformed above 1000 °C. Further, the role of refractory elements in retaining high-temperature flow strength has been discussed.

Atomistically informed mesoscale modelling of deformation behavior of bulk metallic glasses

Both atomistic and mesoscale simulation techniques have been extensively employed to gain fundamental understanding of the structures, deformation mechanisms, and structure-property relationships in bulk metallic glasses (BMGs), each with its unique strengths and limitations. Nevertheless, there is a limited degree of synergistic integration between the two approaches. In this study, we extract key properties of shear transformation zones (STZs) directly from the atomistic simulations, including their size, number of shear modes, eigenstrain, and most importantly, the activation energy barrier spectrum as a function of cooling history and strain rate. We then incorporate these STZ properties into a heterogeneously randomized STZ dynamic model implemented in a kinetic Monte Carlo algorithm to study parametrically the deformation microstructure, shear band formation and stress-strain behavior of BMGs. Two important characteristics of STZ activation that dictate the strength and ductility of a glass are identified. One is the average of the activation energy barrier spectrum (approximated by a Gaussian distribution), determined by the glass composition and processing history such as the cooling rate. The other is the amount of shift of the Gaussian distribution towards smaller activation energy barrier values during deformation, which is determined by the initial structural states and strain rate during deformation, and exhibits a saturation value. These findings have allowed us to gain important fundamental insights into the correlation between the degree of shear-induced softening and the general deformation behavior of BMGs, leading to a better understanding of the correlation between the processing history/loading condition and the mechanical behavior.

Numerical modeling of shear band effect on Goss grain recrystallization in electrical steels: Crystal plasticity finite element and phase field modeling

This study investigates the effect of shear band evolution on the nucleation of Goss {110}<001> texture during the primary recrystallization of 3.24 wt% Si grain-oriented electrical steel. Nucleation at the early stage of primary recrystallization of the steel is explored both experimentally and numerically. The experimental approach involves cold rolling the steel specimens to obtain a thickness reduction ratio of 76 % and then applying heat treatment to them at 600 °C for less than 1 min. The numerical simulation employes crystal plasticity (CP) finite element model (FEM) to simulate the plastic deformation induced by the dislocation slips on predefined slip systems and non-crystallographic shear bands during cold rolling. Based on the CPFEM results, the generalized strain energy release maximization (GSERM) model is used to predict the preferential orientation probability of recrystallized nuclei for the steel by considering shear band formation. Subsequently, the microstructure evolution during the early stage of primary recrystallization of the steel is simulated using the phase field model (PFM). The developed CP model successfully predicted shear band activation and evolution in the γ-fibers centered on the {111}<112> texture component. The model also demonstrated that shear bands would be the preferred nucleation sites at the early stage of primary recrystallization because of their high stored energy. Moreover, by coupling with the GSERM model, the PFM could reproduce the nucleation of Goss grains at the beginning of primary recrystallization in shear bands.

Tailored gradient nanocrystallization in bulk metallic glass via ultrasonic vibrations

To advance materials with superior performance, the construction of gradient structures has emerged as a promising strategy. In this study, a gradient nanocrystalline-amorphous structure was induced in Zr46Cu46Al8 bulk metallic glass (BMG) through ultrasonic vibration (UV) treatment. Applying a 20 kHz ultrasonic cyclic loading in the elastic regime, controllable gradient structures with varying crystallized volume fractions can be achieved in less than 2 s by adjusting the input UV energy. In contrast to traditional methods of inducing structural gradients in BMGs, this novel approach offers distinct advantages: it is exceptionally rapid, requires minimal stress, and allows for easy tuning of the extent of structural gradients through precise adjustment of processing parameters. Nanoindentation tests reveal higher hardness near the struck surface, attributed to a greater degree of nanocrystal formation, which gradually diminishes with depth. As a result of the gradient dispersion of nanocrystals, an increased plasticity was found after UV treatment, characterized by the formation of multiple shear bands. Microstructural investigations suggest that UV-induced nanocrystallization originates from local atomic rearrangements in phase-separated Cu-rich regions with high diffusional mobility. Our study underscores the tunability of structural gradients and corresponding performance improvements in BMGs through ultrasonic energy modulation, offering valuable insights for designing advanced metallic materials with tailored mechanical properties.

Critical temperature-dependent shear band formation in CoCrNi alloy under high-temperature dynamic compression

In numerous engineering applications, the occurrence of highly rapid loading conditions, coupled with significant temperature rise, is prevalent. Under these harsh conditions, shear localization is a prominent material failure mechanism, which may result in catastrophic failure. Generally, materials possessing higher strength, limited work hardening rate, and lower thermal conductivity are more prone to mechanical instability. However, in the current study, a cryo-rolled CoCrNi alloy, characterized by much higher strength and limited work hardening, shows remarkable room and high-temperature mechanical performance under impact loading except at one temperature domain∼600 °C where this material displays mechanical instability by exhibiting adiabetic shearband. To shed light and understand this abnormal mechanical response, an in-depth microstructural study revealed that the ASB formation is closely linked to the recrystallization behavior of this alloy that is invariantly related to the stored energy of cold work, test temperature, and strain rate. Uniquely, the amplified nano-twinning activity at high strain rate and critical temperature promoted the fragmentation of grains and facilitated recrystallization, respectively. Once the recrystallization is completed, the alloy regains work hardening ability even at very high test temperatures, reaching 900 °C due to the deformation of the newly recrystallized matrix. The present work is valuable in delineating the alloy's application domain for rigorous impact and crash-worthiness applications, as there exists a dearth of literature on this material for dynamic scenarios.

Brittle Damage Processes Around Equi‐Dimensional Pores or Cavities in Rocks: Implications for the Brittle‐Ductile Transition

AbstractIn the Earth's upper crust, rocks deform mostly by means of brittle fracturing processes. At the micro‐scale these processes involve the formation and growth of microcracks in the vicinity of defects such as open fissures, pores and other cavities. Large defects can produce strong enough perturbations of the stress field to activate and/or intensify brittle damage around them. Here we considered the ideal cases of smooth cylindrical and spherical pores inside an infinite solid body subjected to remote triaxial compressive stresses (i.e., the intermediate and minimum principal stresses are assumed equal). We first established the resulting local stress field around one of those large pores and then verified whether certain brittle damage processes could be activated in these conditions. We mainly considered the formation of tensile microcracks and micro shear bands. The former requires the presence of tensile stresses in some regions around the pore, while the latter needs sufficiently large shear stresses on pre‐existing optimally inclined microcracks to overcome their frictional resistance to sliding. We find that shear driven deformation remains localized in the vicinity of the pore. On the other hand, dilatational, tensile cracks can propagate large distances away from the pore but cannot form at and above some threshold ratio of the least to the largest principal stresses. Faulting associated with interacting tensile cracks is therefore suppressed with increasing depth. Our analysis leads to conclusions generally consistent with published experimental observations and provides some clues to discuss the physical cause of the brittle‐ductile transition in rocks.

Tailoring Mechanical Properties and Shear Band Propagation in ZrCu Metallic Glass Nanolaminates Through Chemical Heterogeneities and Interface Density

The design of high‐performance structural thin films consistently seeks to achieve a delicate equilibrium by balancing outstanding mechanical properties like yield strength, ductility, and substrate adhesion, which are often mutually exclusive. Metallic glasses (MGs) with their amorphous structure have superior strength, but usually poor ductility with catastrophic failure induced by shear bands (SBs) formation. Herein, we introduce an innovative approach by synthesizing MGs characterized by large and tunable mechanical properties, pioneering a nanoengineering design based on the control of nanoscale chemical/structural heterogeneities. This is realized through a simplified model Zr24Cu76/Zr61Cu39, fully amorphous nanocomposite with controlled nanoscale periodicity (Λ, from 400 down to 5 nm), local chemistry, and glass–glass interfaces, while focusing in‐depth on the SB nucleation/propagation processes. The nanolaminates enable a fine control of the mechanical properties, and an onset of crack formation/percolation (&gt;1.9 and 3.3%, respectively) far above the monolithic counterparts. Moreover, we show that SB propagation induces large chemical intermixing, enabling a brittle‐to‐ductile transition when Λ ≤ 50 nm, reaching remarkably large plastic deformation of 16% in compression and yield strength ≈2 GPa. Overall, the nanoengineered control of local heterogeneities leads to ultimate and tunable mechanical properties opening up a new approach for strong and ductile materials.

Investigation of the Shear Mechanism at Sand-Concrete Interface under the Influence of the Concave Groove Angle of the Contact Surface

A “random-type” sand–concrete interface shear test was developed based on the sand cone method, with a focus on the most commonly encountered triangular contact surface morphology. A “regular-type” triangular interface, matched in roughness to the “random-type”, was meticulously designed. This “regular-type” interface features five distinct triangular groove inclinations: 18°, 33°, 50°, 70°, and 90°. A series of sand–concrete interface direct shear tests were conducted under consistent compaction conditions to investigate the impact of varying compaction densities and triangular groove inclinations on the shear strength at the interface. Particle flow simulations were utilized to examine the morphology of the shear band and the characteristics of particle migration influenced by the triangular contact surface. This analysis is aimed at elucidating the influence of the inclination of the triangular groove on the shear failure mechanism at the sand–concrete interface. The findings indicate that: (1) The morphology of the interface significantly impacts the shear strength of the sand–concrete interface, while the shape of the stress-displacement curve experiences minimal alteration. (2) At smaller inclination angles, particle contact forces are arranged in a wave-like configuration around the sawtooth tip, resulting in a non-uniform stress distribution along the sawtooth slope. However, as the inclination angle grows, the stress concentration at the sawtooth tip diminishes, and the stress distribution across the sawtooth slope becomes more consistent. (3) Particle migration is significantly influenced by the sawtooth’s inclination angle. At lower angles, particles climb the structure’s tip through sliding and rolling. As the angle increases, particle motion shifts to shear, accompanied by a transition in friction from surface friction to internal shear friction. This leads to the formation of a wider shear band and an increase in shear strength.

Experimental study and numerical simulation verification of the macro- and micromechanical properties of the sandstone–concrete interface under freeze–thaw cycles

In cold-region tunnel engineering, the bonding surface between concrete and surrounding rock is highly susceptible to engineering disasters such as the cracking of support structures under the influence of freeze-thaw cycles, which severely affects the stability of tunnel engineering. This study investigates the macroscopic and microscopic mechanical properties of the sandstone–concrete interface under freeze–thaw cycles and reveals the microdamage and fracture evolutionary laws during the freeze–thaw loading process via the coupled expansion of water–ice particle phase changes via particle flow numerical simulation methods, aiming to provide theoretical support for the design and construction of rock–soil and tunnel engineering in high-altitude frozen soil areas. The results indicate that the interface strength characteristics of the sandstone–concrete specimens exhibit a stable decreasing trend with an increase in the number of freeze-thaw cycles and a decrease in roughness. Taking the most unfavorable condition as an example, the exacerbation of freeze-thaw deterioration resulted in shear strength reductions of 16.53%, 27.01%, and 37.17% for specimens (JRC=3.727), while an increase in roughness led to shear strength increases of 11.00% and 15.14% for specimens (NT=60 cycles). The acoustic emission characteristics during the loading process of the sandstone–concrete interface specimens reflect the microcracking evolutionary activity of the specimens quite well, and setting 1.0 as the recommended value for the precursor determination of the b-value and CV(k) index is most reasonable. Under freeze-thaw cycles, cracks first initiate partial microcracks at the interface and on the outer side of the specimen, primarily dominated by tensile cracks and evolving with a "slow–fast" trend toward both sides of the interface. Under shear stress, particles at the interface first undergo slip dislocation due to their lower bonding strength, generating cracks, subsequently inducing significant displacement of particles on both sides of the interface, resulting in crack propagation toward both sides of the interface, ultimately penetrating and forming shear bands leading to macroscopic failure.

Tensile deformation of metallic glass and shape memory alloy nanolaminates

Mechanical deformation of Cu50Zr50 metallic glasses (MGs) with CuZr B2 layers was explored using tensile tests under iso-strain and iso-stress conditions using molecular dynamics simulations. Atomic structure identification was conducted through machine learning techniques, enabling a distinct examination of the deformation exhibited by each phase. Our results revealed early-stage plasticity driven primarily by shear transformation zones at the amorphous/crystalline interface, rather than shear band formation and propagation observed in the monolithic MG, leading to nanolaminates with enhanced strength. Furthermore, under iso-strain deformation, B2 layers underwent martensitic transformation promoted by the nucleation of voids. However, void growth quickly supersedes these effects under both iso-strain and iso-stress conditions, culminating in sample fracture. In summary, this work advances our understanding of amorphous/crystalline nanolaminates, providing valuable insights into their mechanical complexities.

Crystal plasticity modeling and analysis for the transition from intergranular to transgranular failure in nickel-based alloy Inconel 740H at elevated temperature

The precipitation-strengthened Nickel-based alloy Inconel® 740H® (IN740H) exhibits increased ductility at higher applied strain rates during quasi-static tensile tests at an elevated temperature of 760 °C. The examination of fracture surfaces in this context reveals a noteworthy transition of underlying fracture mechanisms from transgranular to intergranular fracture as the applied strain rate decreases from 1×10−3/s to 0.83×10−4/s. To thoroughly understand the mechanical response of IN740H under these conditions, this study develops a crystal plasticity finite element (CPFE) model. This model incorporates various deformation mechanisms including dislocation slips, climb, and grain boundary sliding, which are relevant to the test conditions. The model is calibrated using data from both tensile tests at different strain rates and creep tests across a broad stress range at 760 °C, enabling the accurate determination of model parameters for each mechanism. Simulation results well captured the experimental observations of different failure modes. At higher strain rates, the model shows a dominance of dislocation slip leading to heterogeneous plastic deformation and formation of transgranular shear bands causing the failure, while at lower strain rates, an increased activity of grain boundary sliding causes grain boundaries crack leading to intergranular failure.

A preliminary investigation on the mechanical behaviour of a stiff Italian clay in the context of hydrogen storage

The large-scale use of renewable energy sources is closely linked to the ability to store excess energy generated during periods of overproduction for use when demand is at a peak. Storing green energy is therefore a key component in the move towards a carbon-neutral economy. Underground hydrogen storage in depleted oil and gas reservoirs may provide an efficient long-term solution. Cyclic injection and production of hydrogen alter the chemo-hydro-mechanical conditions of the reservoir and caprocks, and possible geomechanical consequences of such alterations must be preliminarily assessed for safe storage operations. This study aims at exploring the possible effects of cyclic mechanical loads, such as those that might be induced by hydrogen storage and production, on the mechanical behaviour of a clayey caprock. A series of triaxial tests, both monotonic and cyclic, were carried out on undisturbed samples of a stiff Italian clay cored from a caprock formation overlying a hydrocarbon reservoir. The results show that the material response is characterized by the distinctive stress-strain behaviour of stiff clays, with a rather high fragility, which was found to be highly dependent on the loading strain rate. During laboratory experiments conducted at frequencies larger than in situ ones, cyclic loading under stress control causes a gradual degradation of the material structure leading to the formation of a clear shear band followed by a reduction in shear strength. Eventually, failure occurs as the peak shear strength approaches the applied load. The progressive destructuration also implies a reduction in P- and S-wave propagation velocities and a significant change in the signal shape, which is therefore a promising parameter for monitoring the material degradation process.

Increase in interplanar distances and formation of amorphous shear bands in deformed diamond

Amorphous transformation-deformation bands have been observed in diamond under cyclic loading (at planetary ball milling) near the graphite-diamond equilibrium line at temperatures below the Debye temperature. The maximum stresses and temperature in the diamond do not exceed 6 GPa and 420 K, respectively. These bands add to the set of plastic deformation mechanisms in diamond. TEM methods and conventional X-rays were used to investigate the mechanisms of plastic deformation of diamond. The observed mechanisms include amorphous deformation bands, bond breaking, twin formation, and phase transitions of diamond-lonsdaleite and diamond-onions. The increased interplanar distances provide evidence of the plastic deformation mechanism due to bond breaking. The distances of 0.222 and 0.255 nm are significantly larger than the initial value of 0.206 nm, which is characteristic of d111 diamond. This increase in distance cannot be attributed to lattice expansion caused by point defects, but rather to the breakage of interatomic bonds.

Strength and Fracture Toughness of Type 304 and 316 Austenitic Stainless Steels at 4.2 K

The tensile properties and fracture toughness of type 304L, 316L and 316LN austenitic stainless steels and their weldments at cryogenic temperatures have been summarized in the literature. Rolled plates showed a trade-off relationship between 0.2% proof stress and planestrain fracture toughness with those at 4.2 K. The 0.2% proof stress increases with increasing C+N content, and the fracture toughness depends on their austenite stability to α’-martensitic transformation at the crack tip. The formation of shear bands at low strains is directly related to fracture toughness. The stacking fault energy represents the shear-band formation as well as slip deformation manner, so alloy design with higher Ni, Mn, and Mo contents in the chemical composition range of 316LN would be desirable to improve fracture toughness due to higher stacking fault energy.

A strong and ductile biocompatible Ti40Zr25Nb25Ta5Mo5 high entropy alloy

A non-equiatomic high entropy alloy (HEA) Ti40Nb25Zr25Ta5Mo5 (at.%) was designed by replacing 5% Ta with 5% Mo in a precursor Ti40Nb25Zr25Ta10 HEA for improved mechanical properties and reduced density. The Ti40Nb25Zr25Ta5Mo5 HEA fabricated by copper mould casting exhibited a nearly equiaxed grain structure (grain size: 96 ± 16 μm), but within each equiaxed grain, dendritic structures are discernible in the backscattered electron imaging mode. These dendrites are enriched in Ta, Nb and Mo, while the inter-dendritic regions contain higher Zr and Ti. The as-cast HEA achieved tensile yield strength (σ0.2) of 976 ± 8 MPa and strain to fracture (εf) of 16.80 ± 1.86%, well above the minimum requirements of σ0.2 and εf for medical-grade titanium alloy Ti–6Al–4V (759 MPa and 10%). The formation of microscale and nanoscale shear bands and the presence of significant dislocations in the shear band boundary region played a key role in allowing this as-cast HEA to achieve the excellent combination of tensile strength and ductility. Furthermore, the HEA exhibited a lower wear rate, lower coefficient of friction and much higher corrosion resistance in Hank's solution (electrochemical assessments) than Ti–6Al–4V, making it a promising alternative biomedical alloy.

Study on strain localization of frozen sand based on uniaxial compression test and discrete element simulation

Strain localization has always been an important subject in frozen soil mechanics and engineering. To evaluate the development of local strain and the formation of shear bands in frozen soil, uniaxial compression tests have been conducted on frozen sand at various temperatures and particle grades. The strain localization evolution law of the frozen soil is analyzed utilizing the digital image correlation (DIC) method. The test results reveal that the entire process of shear band generation, development, and formation in frozen soil can be well captured. Within the testing temperature and particle grade range in this study, in comparison to particle grade, temperature exerts a more pronounced influence on the shear band angle which increases as temperature decreases. It is discovered that the width of the shear band increases with the decrease in temperature and the increase in mean particle diameter d50. Subsequently, a discrete element method (DEM) model is developed to examine the microscopic mechanical characteristics of frozen sand in uniaxial compression tests. The reliability of the DEM model is verified through comparative analysis with test results. Besides, the development law of the strain localization of the frozen soil obtained by the numerical simulation is revealed based on the quantitative analysis of the rotational angle, bonding state, and displacement of the soil particle during the shearing process.

Localization patterns emerging in CPTu tests in a saturated natural clay soil

In this work, the mechanics of cone penetration during CPTu tests in Osaka clay, a natural structured silty clay, was investigated with the Particle Finite Element Method (PFEM). To describe the behavior of the soil, the FD_MILAN model, recently proposed by the Authors, was adopted. The model, based on the multiplicative decomposition of the deformation gradient, incorporates a scalar internal variable, the bond strength Pt, to quantify the effects of structure. The macroscopic description of mechanical destructuration effects is provided by the hardening law of Pt, according to which the bond strength decreases monotonically with accumulated plastic deformations. The brittle behavior resulting from the softening process associated to destructuration make the soil quite susceptible to the spontaneous development of strain localization in the form of shear bands. In order to deal with strain localization phenomena, the model is equipped with a non-local version of the hardening laws, incorporating a material constant – the characteristic length ℓc – which provides the material with an internal length scale. The objective of this work was to get some insight on the effects of the characteristic length and of the initial degree of structure on: the kinematics of the soil deformation around the advancing cone tip; the evolution of soil structure with accumulated plastic deformations; the excess pore pressure field generated in the soil as a result of the hydro-mechanical coupling between the solid skeleton and the pore water, and the net cone resistance measured at the base of the cone. The results of the PFEM simulations show that the deformations around the piezocone are strongly affected by the characteristic length. For heavily structured soils, when ℓc is relatively small with respect to cone radius, the accumulated plastic deviatoric deformation field is characterized by clearly visible shear bands while, as ℓc increases, the detection of localized deformation regions becomes more difficult, if not impossible. This depends on the fact that, for large values of ℓc, the shear band width may be of comparable size to the cone radius. In all cases, the soil around the advancing piezocone is subjected to a very strong destructuration process, which leads to the complete loss of bond strength in a large region around the cone tip and shaft. As a consequence, the use of conventional Nc values from the literature in the interpretation of the CPTu test performed in heavily structured soils could provide undrained strength values closer to the ultimate undrained shear strength. At the same time, the use of empirical correlation to estimate the yield stress in oedometric conditions would lead to a significant underestimation of the overconsolidation ratio.

Slow Fatigue and Highly Delayed Yielding via Shear Banding in Oscillatory Shear.

We study theoretically the dynamical process of yielding in cyclically sheared amorphous materials, within a thermal elastoplastic model and the soft glassy rheology model. Within both models we find an initially slow accumulation, over many cycles after the inception of shear, of low levels of damage in the form strain heterogeneity across the sample. This slow fatigue then suddenly gives way to catastrophic yielding and material failure. Strong strain localization in the form of shear banding is key to the failure mechanism. We characterize in detail the dependence of the number of cycles N^{*} before failure on the amplitude of imposed strain, the working temperature, and the degree to which the sample is annealed prior to shear. We discuss our finding with reference to existing experiments and particle simulations, and suggest new ones to test our predictions.

Effect of grain size on the recrystallization kinetics and crystallographic texture of unidirectionally rolled Ti-15V-3Cr-3Al-3Sn alloy

In the present work, Ti-15V-3Cr-3Al-3Sn (Ti-15333) samples were solution annealed (SA) at two different temperatures (800 °C for 30 minutes and 1000 °C for 15 minutes) to investigate the effect of initial grain size (GS) on the cold rolling and recrystallization behavior. Average grain size (AGS) for samples SA at 800 °C and 1000 °C was 87±7.82 μm and 177±4.36 μm, respectively. Both the samples were cold rolled unidirectionally (UDR) upto 80 % thickness reduction, subsequently followed recrystallization at 780 °C. UDR samples showed elongated grain structure with a preferential formation of shear bands (SBs) in some grains. Formation of SBs was more prominent in coarse AGS sample and these bands were also found to be orientation sensitive. The frequency of occurrence of SBs was more in γ-fiber (ND//<111>) grains and Dillamore’s plastic instability criterion was used to explain their preferential occurrence in γ-fiber. Recrystallization was done at 780 °C, for various time periods ranging from 30 s to 30 minutes). 80 % UDR samples showed the formation of strong α- and γ-fibers in both the cases. Full recrystallization was attained within 10 minutes for the initial fine grained 80% UDR sample, and it exhibited a continuous γ-fiber texture. In contrast, initial coarse grained 80% UDR sample took 20 minutes to achieve complete recrystallization, and it showed a discontinuous γ-fiber texture. Notably, the {111}<112> texture component of the γ-fiber was prominently evident in both cases, while the α-fiber was entirely absent for both conditions.