Shale Beds Research Articles

Variation in Pore Structure and Associated Fractal Dimensions of Barakar and Barren Measures Carbon-Rich Gas Shales of Jharia Basin, India.

The carbon-rich Barakar and Barren Measures shale beds of the Jharia basin were evaluated for variation in pore size, pore structure, and fractal dimensions. The shale core samples were obtained from exploratory boreholes drilled at the Jharia basin. The shale samples were analyzed for organo-inorganic composition by FTIR, pore size, and pore structure using BET low-pressure N2 adsorption and pore geometry through FE-SEM photographs. The shale samples have significant carbon-rich content and are intercalated-banded in nature. The pore structures were evaluated through N2 isotherms and validated by SEM images, revealing the mixed contribution of organo-inorganic matter in pore formations controlled by geochemical alteration, diagenesis, and mineral interaction. The rough internal surfaces of the pore were evaluated by categorizing them into fractals D1, D2, and D3. It is observed that the D2 type of fractals is in abundance associated with mesopores. The positive trend of fractals with pore size, pore structure, depth, fixed carbon, and TOC suggests the influence of different parameters on the formation of pore internal rugged surfaces in shale beds. The FE-SEM images indicate shallow to deep pores with different pore structures with fair to good pore connectivity. In summary, the shale beds of Jharia have heterogeneous complex pore structures, a rough surface, and sorption mechanisms controlled by weathering/alteration, depositional conditions, and organo-inorganic content. In shale beds, gas storage and transport phenomena are directly related to pore size distribution, pore structure, and associated fractal dimensions. The calculated values using the proposed empirical models for porosity (EPOf) and permeability (EPEf) showed excellent linear correlation with the measured porosity (MPOc, R2 = 0.8577) and permeability (MPEc, R2 = 0.8577), which are close to measured values. The curve matching of EPOf with MPOc and EPEf with MPEc follows a similar path, validating the results and suitability of the models. Hence, the proposed models may be considered to estimate the porosity and permeability of shale and coal beds.

Palaeofloristics of Lower Gondwana exposure in Hingula area, Talcher Basin, Odisha, India: an inclusive study on biomarkers, megafloral and palynofloral assemblages

ABSTRACT This paper deals with an integrated work on the study of megafossils, palynoflora, and biomarkers in the Hingula Opencast Coal Project, Talcher Basin, Odisha, India. The macrofloral assemblage recovered from the lower grey shale bed of the investigated outcrop comprises Schizoneura gondwanensis, equisetaceous stem (Equisetales), Neomariopteris hughesii (Filicales), 19 species of Glossopteris, Vertebraria indica and stem cast (Glossopteridales). The megafloral assemblage and lithology (fine to medium-grained feldspathic grey shale) of the litho-column strongly suggest that the sediments belong to the Barakar Formation of late Early Permian (Artinskian-Kungurian) age. The palynofloral assemblage identified from the upper carbonaceous shale bed of the same outcrop is characterised by the dominance of Striatopodocarpites spp. and sub-dominance of Faunipollenites spp. Stratigraphically significant taxa of this palynoassemblage show its affinity towards the Late Permian (Wordian-Capitanian) age. The first-ever biomarker study of Talcher Basin has been undertaken as a part of the present investigation, which reveals the occurrence of short to long-chain hydrocarbons, indicating the presence of aquatic, microbial, and higher plant input. The predominance of n-C25 in most of the samples indicates moderate-to-high water levels. Similarly, the prevalence of pristane over phytane depicts suboxic to oxic basin conditions during deposition.

Foraminiferal Biostratigraphy of the Uppermost Cretaceous Period, Duhok Area, Kurdistan Region, North of Iraq

A relatively complete Late Maastrichtian succession of the upper part of the Shiranish Formation (Upper Cretaceous) in the Duhok area is investigated for the planktic foraminiferal assemblages. This studied interval consists mainly of bluish shale, marl, and thin beds of hard marly limestone all with grey-blue color. The upper contact of the Shiranish Formation is conformable with the overlies Danian Aaliji Formation. Based on the recorded planktic foraminifera and their ranges, the studied succession is subdivided into three main biozones of the latest Maastrichtian age, these zones are Pseudoguembelina hariaensis (CF3) Interval Zone, Pseudoguembelina palpebra (CF2) Interval Zone, and Plummerita hantkeninoides (CF1) Total Range Zone. These zones show continuous and complete Upper Cretaceous sediments, which are preserved in the Bade section of the Duhok area

Influence of the Weakening Effect of Drilling Fluid on Wellbore Stability in Anisotropic Shale Formation

For horizontal wells in Longmaxi Formation, oil-based drilling fluid that soaks for a long time is more likely to cause a wellbore collapse. Therefore, in this paper, the downhole core method of shale formation, in Longmaxi Formation, was adopted. First, rock samples were selected from different sampling angles and soaked with field drilling fluid. Second, a triaxial mechanics experiment was carried out. Based on the anisotropic wellbore stress distribution model, the stability of shale wellbore was calculated and analyzed. The results show that the compressive strength and cohesion of the shale are reduced after soaking in the drilling fluid. Hence, the reduction range of various sampling angles obviously differs as well. Shear failure occurs in vertical stratification; shear slip failure occurs along the weak plane, showing strong anisotropy. Combined with the experimental results, the collapse pressure is calculated, and it is found that the weakening effect of drilling fluid makes the overall collapse pressure rise by about 0.2 g/cm3. Finally, the shale bedding dip and dip direction have a great influence on the collapse pressure. The lower critical mud weight always takes the minimum value when the borehole axis is perpendicular to the bedding.

Constraints of sedimentary structures on key parameters of shale gas reservoirs: A case study of the Wufeng and Longmaxi formations of the Ordovician‐Silurian transition in Luzhou area, Sichuan Basin, southwestern China

There are various sedimentary structures developed in the black shales of the Upper Ordovician Wufeng Formation and the Lower Silurian Longmaxi Formation in Luzhou area, southern Sichuan Basin, southwestern China. In order to evaluate the controlling effects of sedimentary structures on the key parameters of shale reservoir properties, collected classification of sedimentary structures, scanning electron microscope observation, analysis of shale fabric and porosity characteristics, low‐pressure nitrogen adsorption, methane isothermal adsorption, and conventional triaxial compression test were carried out based on shale samples from Wells A‐H1, B‐H1, C‐H1 and D‐H1 in the study area. The sedimentary structures recorded in these shales are categorized into five types: homogeneous bedding, weak horizontal bedding, strong horizontal bedding, discontinuous ripple bedding, and gravel‐bearing massive bedding. In general, the palaeo‐hydrodynamics and oxygen content of water columns were weak when homogeneous bedding shale was deposited. The organic matter is the most abundant and the total organic carbon content is up to 4.01% on average. The average quartz content is 43.5%, and the brittleness index is the highest. The porosity and adsorption capacity were the highest, with an average of 4.57% and 79.5 scf/ton, respectively. Combined with its mechanical properties of low Poisson's ratio and high Young's modulus, homogeneous bedding sedimentary structure is associated with the shale units possessing the highest organic matter abundance, the strongest reservoir property, and the best fracability, which is the priority target for exploration and development of the Wufeng to lower Longmaxi Formation in the Sichuan Basin, southwestern China.

Experimental study on the effect of loading angle on crack propagation in bedding shale

The dynamic fracture of rock materials is a basic problem in the field of rock mechanics, while the dynamic fracture mechanism of shale is more complex due to its anisotropic characteristics. In order to study the effect of bedding angle on dynamic fracture process of shale, a split Hopkinson pressure bar (SHPB) system was used to carry out impact tests on notched semi-circular bend (NSCB) specimens of shale. Additionally, a crack propagation gauge (CPG) was set at the crack tip, and the whole fracture process of the shale NSCB specimen was studied with the help of a high-speed photography system and the digital image correlation (DIC) method. The loading rate and Mode-I dynamic fracture toughness of the shale NSCB samples were obtained by the method recommended by the International Society for Rock Mechanics (ISRM). And the crack initiation time and crack propagation speed of the shale NSCB samples can be accurately obtained by CPG. It is found from the experimental results that the Mode-I dynamic fracture toughness of the shale NSCB samples has significant anisotropy, and the loading angle has a positive correlation with the Mode-I dynamic fracture toughness. Although the crack propagation of the C-0sample is not affected by the bedding, its crack propagation needs to cut through the shale matrix, hence the C-0 and 90° shale specimens have a high Mode-I dynamic fracture toughness. When the impact velocity is low, the bending stress on the dangerous section affects the fracture direction of the shale specimen, but with less effect on the bedding. The crack propagation path finally closes to the notch direction. With the increase of impact velocity, stress concentration and micro cracks may exist along the weak plane of bedding due to its relatively low strength. With the increase of impact velocity, the cracks between the weak planes of bedding begin to extend, and the failure planes along the direction of bedding and notch occurred simultaneously.

Facies, magnetic susceptibility and timing of the Late Devonian Frasnian/Famennian boundary interval (Xom Nha Formation, Central Vietnam)

Upper Devonian carbonates deposited through the Frasnian/Famennian (F/F) stage boundary in the Xom Nha Formation, Central Vietnam, were studied. The section is mainly composed of fossiliferous, brecciated, and laminated limestone beds, while shale beds occur in a subordinate number. Microfacies generally suggests a hemipelagic setting on an outer shelf environment with low sedimentation rates. A sediment accumulation rate of 0.217 cm/kyrs for this section is calculated. The Xom Nha section does not exhibit characteristic black shales or black limestones through the F/F boundary, but instead shows a similar lithology in comparison to other F/F sections in Southeast Asia. The carbonates yielded abundant conodonts, which represent mainly cosmopolitan species but the section differs from most sections in Europe in showing relatively high numbers of Palmatolepis linguiformis species. Deposition through the F/F boundary interval reported here for the Xom Nha section appears to have occurred during a ~1.2 Ma, and shows well-defined climate cyclicity.

Organo-inorganic facets of shale gas reservoir of Jharia Basin of Damodar Valley, India

The Mahuda-Kapuria block of the Jharia Basin, Damodar Valley comprises thick shale sequences of Shibabudih (>180 m) in Barakar and Hariharpur shale (>40 m) in Barren Measures Formations. The ternary organic facies of maceral shown the trend of anoxification, resulting in higher maceration as a function of terrestrial-marshy depositional conditions. Subsequently, it supported the tissue preservation and carbon enrichment contributing to the formation of shale matrix. H/C vs O/C plot shown Type III/IV kerogen transformed from fluvio-humid to dry terrestrial depositional conditions followed by diagenesis, cata- and metagenesis processes. Also, the range values of Tmax (442–558 °C) and HI (25–345 mg HC/g TOC) confirms the significantly matured source rock having the input of dominantly type III/IV kerogen. The S1 and S2 specify (0.07–2.54 mg HC/g rock, 0.58–20.14 mg HC/g rock) the presence of substantial free/adsorbed hydrocarbon gases and uncracked hydrocarbon compounds. The large content of SiO2, Al2O3, and Fe2O3 account for 85–95 % of the samples point towards granitic source rock of sediments. The high CIA and low ICV values denote the compositional maturity of the shale due to conversion of feldspars to Al-bearing clays through intense geochemical weathering and alteration. The positive trend of organic weight with Langmuir volume (VL) and TOC specify the organic carbon present in shale mainly contributes to the formation of pore containing matrix system and adsorption of methane in shale pores. The mineralogy of shale directly controls the tensile strength, uniaxial compressive strength, Young's modulus, Poisson's ratio and brittleness of shale beds. Further, it is observed that the brittleness of shale beds exhibits higher axial strain with a small region of elastic behaviour by the influence of the hydrous property of kaolinite and illite. The proposed empirical EMBI for estimation of brittleness indicated moderate brittle characteristics of shale beds.

Analyses of depositional environments of the Marcellus formation in New York using biomarker and trace metal proxies

The purpose of this study was to observe how the composition of organic matter (OM) and the extent of anoxia during deposition within the Marcellus Formation in New York varied by distance from the sediment source in eastern New York. Lipid biomarkers (n-alkanes and fatty acids) in the extractable organic component (bitumen) of the shale samples were analyzed, and proxies such as the average chain length (ACL), aquatic to terrestrial ratio (ATR) and carbon preference index (CPI) of n-alkanes were calculated. Fatty acids were relatively non-abundant due to the age of the shale bed, but n-alkane distributions revealed that the primary component of the OM was terrigenous plants. The presence of shorter n-alkane chain lengths in the samples indicated that there was also a minor component of phytoplankton and algal (marine) sourced OM. Whole rock analyses were also conducted, and cerium anomalies were calculated as a proxy for anoxia. All samples had a negative anomaly value, indicating anoxic conditions during deposition. Two samples, however, contained values close to zero and thus were determined to have suboxic conditions. Anoxia and total organic matter (TOM) did not show any spatial trends across the basin, which may be caused by varying depths within the basin during deposition. A correlation between nickel concentrations and TOM was observed and indicates that algae was the primary source of the marine OM, which supports the lipid biomarker analysis. It was determined that the kerogen type of the Marcellus Formation in New York State is type III, consistent with a methane-forming shale bed.

Evaluation of the fracture mechanisms and criteria of bedding shale based on three-point bending experiment

Shale has remarkable bedding characteristics, and the key technology of shale gas extraction engineering is garnering great interest in the influence of bedding on the fracture mechanisms and fracture criteria of shale. Three-point bending tests combined with digital image correlation (DIC) were carried out on semicircular bend (SCB) specimens of shale with different bedding angles to investigate the influence of bedding on crack evolution. The results showed that the strain field of each bedding shale exhibited three stages during the three-point bending : uniform strain distribution, damage accumulation, and strain localization. In the stage of strain localization, each specimen first showed considerable tensile strain localization along a straight line extending from the tip of the prefabricated crack. With increasing loading, except for in the localized bands of the tensile strain, the maximum shear strain became aligned with the bedding orientation in the shale specimens, indicating that the original mode I cracks of the specimens were transformed into mixed-mode I/II cracks due to the influence of the bedding. A new fracture criterion (the generalized maximum circumferential stress criterion based on shale bedding, GMTS-SB) was deduced for predicting the propagation of a prefabricated mode I crack in bedding shale. The results calculated from the GMTS-SB were compared with the experimental results to evaluate the accuracy of the criterion. In the established GMTS-SB, the stress intensity factor is related to the specimen size, the load magnitude, and the bedding angle. This criterion also considers the influence of T-stress on the calculated result. For bedding shale, the GMTS-SB can effectively describe the crack angle and fracture resistance of a crack initiating along the bedding orientation.

Monitoring shale water uptake using 2D magnetic resonance relaxation correlation and SPRITE MRI

Fluid storage and transport in shale and clay formations is important in many areas of application, including hydrocarbon recovery from, and waste fluid storing in, these reservoirs. The multiscale heterogeneous nature of shales is largely responsible for these rocks being considered unconventional and complicated. Researchers often rely on imaging methods to provide spatial information to characterize their heterogeneity.SEM and nano-CT are powerful methods that have been used to give images of shale nanopores with fields of view (FOV) of 100 μm. However, this limited FOV has raised questions about the validity of simulations based on these methods to scale up and represent macroscopic shale properties. Here, we have used, for the first time, SPRITE Magnetic Resonance Imaging (MRI) methods to give core plug size shale images. The imaging method resolves water and oil signals to give separate images of each in shales.“As received” shale samples were used to acquire 1D and 3D oil and water images to characterize natural fluid distribution. Water uptake experiments were conducted to probe fluid displacement in shales. Measurements included gravimetric, Magnetic Resonance (MR) T1-T2∗ relaxation correlation, and SPRITE imaging methods. Water and oil images showed that sample scale heterogeneities are imposed by the shale beddings. Water uptake experiments (1) showed the capability of the T1-T2∗ method to identify MR signals from shale fracture water and matrix pore water, and (2) illustrated wettability control of spatial water distribution in shales during spontaneous imbibition.

An Analytical Model for Fracture Initiation of Radial Drilling-Fracturing in Shale Formations

Abstract Radial drilling-fracturing, the combination of radial drilling and hydraulic fracturing, can guide fractures toward the target area and effectively enhance the recovery of the low permeable reservoir. In this paper, based on the stress superposition principle, we establish an analytical model to predict fracture initiation pressure (FIP) and the shale failure mode for radial drilling-fracturing applied in shale formations. In contrast with the former studies, this model can additionally consider the failure from shale beddings and is more applicable in the shale reservoir. The model classifies the shale failure into three modes and, respectively, gives the criterion for each failure mode. Then, a series of sensitivity analyses is conducted by examining effects of various parameters. By analyzing the variation characteristic of the initiation pressures required for three failure modes, the main conclusions are as follows. Firstly, matrix failure and shear failure along bedding tend to take place when the azimuth of radial borehole is moderate. Small and large azimuths are favorable for the occurrence of tensile failure along bedding. Secondly, a high ratio of horizontal in situ stress predisposes shale to generate matrix failure, and bedding tensile failure and bedding shear failure are apt to occur when the ratio of horizontal in situ stress is low. Thirdly, with the increasing intersection angle of the radial borehole wall and bedding plane, the failure mode apt to occur changes from bedding tensile failure to bedding shear failure and then to matrix failure. Fourthly, shale prefers to yield bedding shear failure under a small Biot coefficient and generate the other two failure modes when Biot coefficient is large. Fifthly, permeability coefficient virtually has no influence on the failure mode of shale. The research clarifies the fracture initiation characteristics of radial drilling-fracturing in shale formations and provides a reference for the field application of radial drilling-fracturing.

Assessment of the interval heat flow and thermal resistance at the Faltu-1 well, Borno basin, NE Nigeria

The heat flowing through horizons in the Faltu-1 well, Borno Basin, NE Nigeria was calculated from their thermal conductivities and geothermal gradients with the aim of determining whether or not it is uniform, and if not, the depths where it is diverted, and the possible heat diversion process. The interval heat flow was assessed to be non-uniform. While fluid convection is adjudged to be the major heat diversion mechanism within the Chad Formation with minor heat refraction, the reversed is adjudged to be the situation for the underlying Kerri Kerri Formaton within which increasing sand content with depth is also predicted, with the lower interval predicted to be the Gombe Formation. Patterns of disruptions to the vertical heat flow within the Fika Formation were inferred to suggest rhythmic bedding of shale and sand beds that could serve as both source and reservoir rocks. Magmatic intrusions that impacted the maturation of organic matter into oil and gas also provided necessary entrapment structures and possible migration pathways. The Gongila and Bima Formations each has single disruption of the heat flows that are attributed to refraction. In the case of the Gongila Formation, the disruption is between the early-deposited more sandy and laterdeposited more shaley lithologies in the marine transgression of the area, while in the case of the Bima, it is between the more shaley Upper and more sandy Middle Bima Formations. Analysis of the Bullard plots also revealed disruptions to the vertical heat flow that are attributed either to convecting fluids or to heat refraction and diffraction. Two such disrupting heat advections were identified within the Chad Formation with the first being attributed to convection, while the other is attributed to a combination of both. Two similar disruptions for the Kerri Kerri Formation were attributed largely to lithological variations with minor contributions from convection of fluids. While unable to discern the rhythmic bedding, the five disruptions of the Bullard plot for the Fika Formation and one each for the Gongila and Bima Formations were interpreted to indicate similar features inferred from interval heat flow plots.
 Keywords: Interval heat flow, heat convection, heat diffraction, thermal resistivity, shaliness

Experimental investigation of shale breakdown pressure under liquid nitrogen pre-conditioning before nitrogen fracturing

Cryogenic fracturing with liquid nitrogen (LN2) offers the benefits of reducing the water consumption and adverse environmental impacts induced by water-based fracturing, as well as potentially enhancing the fracture complexity. We performed a series of laboratory experiments to explore the key mechanisms governing the breakdown pressures of shale during cryogenic fracturing. In this study, cylindrical shale samples were pre-conditioned by exposing a borehole to low-temperature LN2 for a certain time period, and then, the samples were fractured using gaseous N2 under triaxial stress and a high reservoir temperature. The effects of various key parameters on the breakdown pressure were investigated, including the duration of the low-temperature LN2 treatment, the confining pressure, the reservoir temperature, and the direction of the shale bedding relative to the borehole axis. The results demonstrate that the injection of low-temperature LN2 as a pre-fracturing fluid into a borehole can significantly reduce the breakdown pressure of the shale during subsequent nitrogen fracturing. This reduction in breakdown pressure can be further intensified by increasing the duration of the LN2 pre-conditioning. Without LN2 pre-conditioning, the breakdown pressure initially increases and then decreases with increasing reservoir temperature. When LN2 pre-conditioning is applied, the breakdown pressure keeps decreasing with increasing reservoir temperature. As the confining pressure increased, the breakdown pressure increased linearly in the tests with and without LN2 pre-conditioning. The experimental results demonstrate that LN2 pre-conditioning before N2 fracturing is a promising waterless fracturing technique that reduces the breakdown pressure and enhances the fracture complexity.

Multi-Level Detachment Deformation of the West Segment of the South Dabashan Fold-and-Thrust Belt, South China: Insights From Seismic-Reflection Profiling

The South Dabashan arcuate tectonic belt located at the northern margin of the Yangtze Block in South China, which primarily comprises a series of northwestern (NW)-trending foreland fold-and-thrust belts (FTBs), is useful for determining the intracontinental orogeny processes of the Yangtze Block. In this study, we integrated the latest pre-stack depth migration of three- and two-dimensional seismic profiles, drill hole, and outcrop data to explore the structural geometric and kinematic features of the west segment of the South Dabashan FTB. This belt is characterized by multi-level detachment structures due to the presence of three predominant sets of weak layers: the Lower Triassic Jialingjiang Formation gypsum interval, Silurian mudstone beds, and Cambrian shale beds. The belt is accordingly subdivided vertically into three structural deformation systems. The upper system appears above the Jialingjiang Formation gypsum layer and exhibits Jura-type folds, which were formed by alternating anticlines and synclines that are parallel to each other. The middle system comprises Silurian shale as the base and Jialingjiang Formation gypsum interval as the passive roof and exhibits NW-striking imbricate thrusts. The lower system is bounded by Cambrian and Silurian detachment layers, forming a duplex structure. The Sinian and Proterozoic basements below the Cambrian were not involved in deformation. The west segment of the South Dabashan FTB underwent four periods of tectonic evolution: Late Jurassic to Early Cretaceous, Late Cretaceous, Paleogene, and Neogene to Quaternary. The deformation was propagated southward in imbricate style, resulting in the passive uplifting of the overlying strata. Based on the magnetotelluric and deep seismic profile, the tectonic processes of the west segment of the South Dabashan FTB are inferred to be primarily controlled by the Yangtze Block northward subduction under the Qinling Orogenic Belt and the pro-wedge multi-level thrusting during the Late Jurassic to Cretaceous.

Trace elements geochemistry of the Golbanoo coal basin, Iran

ABSTRACT The Jurassic coal deposit in the Golbanoo area contains coal seams with thickness ranges from 5 cm to 1 m and is underlain and overlain by thin coaly shale, sandstone and siltstone beds. This study reports on the geochemical features of coals and non-coal rocks based on the 30 channel samples were collected and analyzed for trace elements using neutron activation analysis (INAA) and for major elements by X-ray fluorescence. The Al2O3, SiO2 and Fe2O3 concentrations are the main oxides. The amounts of trace elements (As, Ag, Br, Sb, Cr, Co, Sr, Zn, Ta, and ∑REE) in Golbanoo coal are high compared to world types of coal. The volcanic activity and their sulfide mineralization in study area is a favorable factor for accumulation of trace element in coal layers.

Early-Middle Frasnian (Late Devonian) carbon isotope Event in the Timan-Pechora Basin (Chernyshev Swell, Pymvashor River section, North Cis-Urals, Russia)

Details of the Early-Middle Frasnian boundary interval of the Pymvashor River section (Timan-Pechora Basin, Cis-Urals, in the far north of European Russia) are revealed by biostratigraphically constrained carbonate (δ13Ccarb) and organic carbon (δ13Corg) stable data. The studied interval corresponds to the lower part of the Domanik Formation, which consists of interbedded limestone and shale beds. Organic-rich black shale that lacks bioturbation and benthic organisms indicates an oxygen-depleted depositional environment. Detection of isorenieratene derivatives in organic matter indicates that anoxia was present in the photic zone during deposition. The Pymvashor River section contains δ13Ccarb and δ13Corg isotope records related to the Early-Middle Frasnian isotope Event. The similarity between the Cis-Uralian (this study) and the Chinese δ13Ccarb and δ13Corg oscillations, including the twostep pattern of the recorded major positive excursions, suggests a robust correlation of the Late Devonian Early- Middle Frasnian isotope Event and minor intra-event excursions. Magnitude of variations and values of δ13Corg and δ13Ccarb in the punctata Zone in the Pymvashor River section are minor than those observed in the North American, Polish, and Chinese successions. Such difference may reflect specific variation of the local environments.

Late Permian species diversity of the genus Glossopteris in and around Himgir, Ib River Basin, Odisha, India, with a clue on palaeoclimate and palaeoenvironment

The Ib River Basin, situated in the south-eastern part of the Mahanadi Master Basin, has always been in focus for its record of well-diversified Lower Gondwana plant mega fossils. A good number of plant mega fossils has been collected from a newly constructed road section near Himgir Village, Sundargarh District, Ib River Basin, Odisha, India (21°45′ 47″ N Latitude and 83° 42′ 28″ E Longitude). The collection of plant fossils from this locality represents the dominance of highly diversified Glossopteris genus (46 taxa) during the Late Permian time (Lopingian epoch). Altogether 46 species of genus Glossopteris were reported from two fossiliferous layers of the same ferruginous red shale bed. The majority of broad mesh form Glossopteris species along with few narrow and medium mesh forms, petiolate leaves and Glossopteris with thick midrib were reported from the upper floral zone, while the lower floral zone was dominated by narrow and medium mesh form species and leaves with thin midrib. A marked floral change has been noticed in these two fossiliferous horizons of this section, demonstrating the existence of two different floral zones in the rocks of Lower Kamthi Formation. The upper floral zone is assigned to the Changhsingian age, while the lower floral zone is of Wuchiapingian age. The existence of Late Permian floras, the absence of typical Triassic flora (Dicroidium flora) in the present fossil assemblage and the lithology of the area (covered by fossiliferous ferruginous red shale, ferruginous red sandstone, yellowish shale and pebbly conglomerate) demonstrate that the exposure belongs to the Lower Kamthi Formation. The presence of well-diversified fossil assemblage represents a thick swampy dense and deciduous forest of Glossopteris. The different morphological characteristics of plant fossils depict a warm, humid and temperate climate with intermittent rainfall and adequate light intensity at the time of deposition.

First record of late Campanian paleoceanographic and paleoclimatic changes, Arabian Platform, Mazidag-Mardin area, SE Turkey

The sedimentology, geochemistry and paleontology of the pelagic upper Campanian Maastrichtian Bozova Formation in the "Mazidag" (Mazıdağı) - Mardin area, SE Turkey, reveal paleoceanographic and paleoecological changes for the first time. A 119.25 m-thick composite stratigraphic section is characterized by alternating marls, clayey limestones, shales, and black shales; no coarse siliciclastic admixture or turbidite intercalations were recorded in the section. Biostratigraphic data indicate the presence of the Radotruncana calcarata Zone, and the UC15de/UC16 nannofossil zones. Stable isotope and elemental geochemical analyses have been carried out in the studied section. The isotope curves display similar patterns compared to reference curves from European and Chinese basins in the same interval. The prominent negative carbon isotope excursion determined in the upper interval can be correlated with the Late Campanian Event. Proxy elements display generally two relative rising trends in productivity from the lower part and the middle part of the succession. The lower part of the section records relatively more dysoxic/anoxic conditions and coincides with common black shale beds. The presence of both diverse planktonic foraminifera and calcareous nannofossils in the studied interval indicates a fully marine, warm-water, low-latitude Tethysian oceanic environment. In addition, the plant fossils derived from the nearby land mass indicate that a tropical humid climate was similar to that in northeast Australia. Therefore, warm water, tropical humid atmospheric conditions developed in the studied area causing the rise in productivity, precipitation and transportation of plant debris into offshore environments.

Velocity anisotropy and trend in Niger Delta, Nigeria

In geophysical data interpretation, matching the vertical velocity direction from seismic data with borehole-derived velocities is a challenging task because seismic-derived velocities are faster than borehole recorded velocities. This geophysical phenomenon is caused by velocity anisotropy. In this study, we used an empirical approach to estimate the degree of velocity anisotropy in the study area. The results showed that the delta anisotropy in sandstone beds varies from − 2.5% to 7.2% while most of them concentrate between 3.2% and 6.1%. The epsilon ranges between -6.4% and 9.3% while many of them concentrate between 3.2% and 7.2%. The gamma varies from − 6.3% to 7.3% while most of them concentrate between 1.2% and 5%. At shale beds, delta anisotropy varies from − 11.2% to 11.1% but most of them concentrate between 4.3% and 10.5%. The epsilon varies from − 7.2% to 14.5% while most of them concentrate between 4.5% and 10.5%. The gamma varies from 6.4% to 8.2% while majority of them concentrate between 2% and 5.3%. The results indicate that the study area is weakly to moderately anisotropic with shale beds having higher anisotropy values than sandstone beds. This probably results from preferential alignment of clay mineral orientations which also affect in situ velocity propagation. Three distinct velocity gradients (low, moderate and very high) were identified in the study area. These velocities vary erratically but showed northeast–southwest increase in velocities. Thus, the need to derive correction factors for individual wells for improved exploration success.