Typical Sandstone Research Articles

Efficacy of polyacrylate latex nanodispersions as consolidation agents in porous sandstones evaluated by synchrotron X-ray computed microtomography

This research describes the effects of two innovative aqueous polyacrylate polymers on the microstructure of porous stone materials. Such latex nanodispersions have been designed (with and without fluorination) as consolidation agents and tested on two types of sandstone, namely, Prague (Mšené) and Obernkirchen, largely used as building materials for valuable Cultural Heritage objects. Quantitative description of the polymer distribution within the specimens was obtained noninvasively by adopting synchrotron radiation computed microtomography. The propagation-based phase-contrast mode was adopted to test its effectiveness in enabling the recognition of the polymers in the two matrices, which is usually hampered by their low attenuation coefficient for X-rays. Quantitative image analysis revealed significant dissimilarities in total porosity, specific surface area of pores, connectivity density and fractal dimension as a consequence of the consolidation treatments. For instance, about 7% and 3% lower porosity values were found in the consolidated Prague and Obernkirchen sandstones, respectively, with the distribution shifted towards smaller pores. Furthermore, the simulation of water transport, based on the retrieved pore network, evidenced a decrease in water permeability and diffusivity of more than one order of magnitude in the treated samples; the effect was more pronounced along the direction of penetration of the consolidating agent. Overall, both latexes exhibited similar film-forming and pore-filling abilities. In general, the results highlighted the high potential of synchrotron-based 3D X-ray imaging for the quantitative assessments of the porous microstructure of consolidated building materials.

Experimental study of the influence of borehole parameters on prompt fission neutron uranium logging and its corrections

In prompt fission neutron uranium logging, borehole environmental parameters affect the measured results and must be corrected. In order to explore the influence of borehole parameters on the interpretation of logging results, this paper builds a sandstone type uranium ore block model to simulate the field production drilling device based on the “Epithermal/Thermal neutron counting rate ratio” (E/T) theory. The effects of borehole diameter, thickness of iron tube and well fluid on the decay rate of epithermal and thermal neutrons and their uncertainty correction methods were investigated. The results show that the effect of borehole diameter on E/T is negligible. The iron tube thickness has a certain effect on the moderation and absorption of epithermal and thermal neutrons, and its E/T increases slightly with increasing thickness. The influence of iron tube thickness on E/T is corrected and the relative uncertainty is less than 5%. The well fluid thickness also affects the decay rate of epithermal and thermal neutrons, and its E/T follows the law of negative exponential attenuation. The influence of well fluid thickness on E/T is corrected and the relative uncertainty is less than 5%. This study provides technical guidance for field well survey of uranium deposit.

A new criterion of rock burst proneness based on residual energy release rate index

The natural property of rock material, whether impact occurs, is the key influencing factor of the occurrence of rock burst disaster. To accurately assess rock burst proneness, this study focuses on typical sandstone as the research object. Uniaxial cyclic loading and unloading tests were conducted to measure the elastic strain energy accumulated in sandstone under different stress levels and a relationship between elastic strain energy and stress level was established. The results show that: (1) The peak stress under cyclic loading and unloading conditions is slightly lower than the uniaxial compressive strength. With an increase in the number of cycles, the internal damage of sandstone continues to accumulate, and the mechanical properties such as compressive strength continue to deteriorate; (2) With an increase in stress, the input strain energy, elastic strain energy, and dissipated strain energy also increase; (3) When the stress is low, the increase in elastic strain energy is large and shows a steady growth; with an increase in stress, the increase of elastic strain energy decreases; (4) The square of stress at any time has a good linear relationship with elastic strain energy. According to the relationship obtained from the test, the elastic strain energy at the peak stress time can be obtained; (5) A new criterion for assessing rock burst proneness is proposed: residual energy release rate index WT, which characterizes the energy release per unit time when the rock burst occurs. The intervals for evaluating the rock burst proneness of the residual energy release rate index WT are as follows: WT <0.025, indicating no rock burst proneness; 0.025≤ WT <0.15, indicating weak rock burst proneness; 0.15≤ WT <2, indicating medium rock burst proneness; WT >2, indicating strong rock burst proneness; and (6) The rationality of the proposed residual energy release rate index WT is verified by the multi-index method and the multi-sample method, and the proposed residual energy release rate index is used to determine the rock burst proneness of 10 kinds of rock samples. The evaluation accuracy is shown to be high, and it can reflect the actual rock burst proneness

STRATIGRAPHY, PETROLOGY AND FACIES ASSOCIATIONS OF THE QUATERNARY SPIN KAREZ GROUP, HANNA-SPIN KAREZ AREA, QUETTA DISTRICT, PAKISTAN

The Hanna-Spin Karez area which comprises the Quaternary succession of the Spin Karez Group is located adjacent to the junction of Sulaiman and Kirthar Fold-Thrust Belts (Quetta Syntaxes), southwest of the Zarghun Trough in the northwestern Balochistan, Pakistan. The area comprises over 800 m thick conformable succession of the Quaternary age, covering surface area of ~30 km2. The succession has been named as the Spin Karez Group, which are further subdivide from base to top into three distinct lithostratigraphic units as: Hanna Lake Conglomerate, Hanna Red Clays and Spin Karez Conglomerate. The Hanna Lake Conglomerate comprises 200 m thick succession of boulder-pebble conglomerate. The Hanna Red Clays comprise over 500 m thick succession of dominantly red claystone rarely interbedded with siltstone and very fine-grained sandstone. The Spin Karez Conglomerate is composed of over 100 m thick succession of well-stratified and moderately- to well-sorted cobble/pebble conglomerate with occasional sandstone/siltstone lenses. The Triassic to Pliocene age older successions from the region's north and west provided the polymictic conglomerate, boulder to pebble size limestone, sandstone, chert, and conglomerate fragments. The Spin Karez Group comprises 15 types of gravel, sandstone and mudstone facies, which were grouped into 5 facies associations. The facies associations include braided channel deposits (FA-1), sheet-flood deposits (FA-2), floodplain deposits (FA-3), marginal lacustrine deposits (FA-4) and open-water lacustrine deposits (FA-5). The Spin Karez group evolved in three phases: i) Deposition of the Hanna Lake conglomerate started with the proximal and distal braided channel systems in the northern and southern parts of the study area respectively; ii) Deposition of the Hanna Red clays deposited in shallow lake with episodic sub-aerial exposure, providing reddish colour to the mud-dominant facies; iii) The depositional basin, once again, transformed to braided channel system, of the Spin Karez conglomerate, which evolved over the shallow water lake deposits of the Hanna Red clays. The Spin Karez group was mainly controlled by continued subsidence and regional tectonics during the Quaternary period that accommodated the space for the small shallow basin (~30 km2) that stacked depositional systems.

Genetic mechanisms of high-quality tight siliciclastic reservoirs: A case study from the Upper Triassic Xujiahe Formation in the Yuanba area, Sichuan Basin, China

This study analyzed the petrological characteristics, diagenesis, pore types, and physical properties of the tight coarse-grained siliciclastic sequences in the third member of the Upper Triassic Xujiahe Formation (also referred to as the Xu-3 Member) in the western Yuanba area in the northeastern Sichuan Basin, China, based on the results of 242.61-m-long core description, 292 thin-section observations, scanning electron microscopy (SEM), and 292 physical property tests. The types and genetic mechanisms of high-quality tight coarse-grained siliciclastic reservoirs in this member was determined thereafter. The research objective is to guide the exploration and development of the tight coarse-grained siliciclastic sequences in the Xu-3 Member. The results of this study are as follows. Two types of high-quality reservoirs are developed in the coarse-grained siliciclastic sequences of the Xu-3 Member, namely the fractured fine-grained sandy conglomerate type and porous medium-grained calcarenaceous sandstone type. Hydrodynamic energy in the sedimentary environment is the key factor controlling the formation of high-quality reservoirs. These high-quality reservoirs are developed mainly in the transitional zone with moderately high hydrodynamic energy between delta-plain braided channels and delta-front subaqueous distributary channels. The dolomitic debris (gravel) content is the main factor affecting the reservoirs’ physical properties. The micritic algal debris and sandy debris in the dolomitic debris (or gravels) tend to recrystallize during burial, forming intercrystalline pores within. In the medium-grained calcarenaceous sandstones, intercrystalline pores in the dolomitic debris are formed at the early diagenetic stage, and a pore system consisting of structural fractures connecting intergranular pores, intergranular dissolution pores, and kaolinite intergranular micropores is developed at the late stage of diagenesis. The formation of intercrystalline pores in dolomite gravels and gravel-edge fractures, a pore system connected by gravel-edge and tectonic fractures, is closely related to the dolomite gravels in the sandy fine-grained conglomerates.

Petrophysical Analyses of Rock Construction Materials from a Roman Rural Settlement in Podšilo Bay on Rab Island (North-East Adriatic, Croatia).

This article presents the results of petrophysical analyses of limestones and sandstones used for the construction of the wall structures of a Roman rural settlement located in Podšilo Bay on Rab Island (Croatia). An on-site analysis of the walls indicated the use of different lithotypes, which is an uncommon case in the area. So far, no petrophysical properties of the applied materials have been tested, and their provenance has not been specified. The aim of this research was to determine their usability as construction materials in an attempt to determine the possible reasons behind the usage of multiple lithotypes and their suitability as building materials. The following procedure was used to address these issues: (1) determination of the petrographic characteristics of the rocks, (2) performance of tests to characterise the mechanical properties in a complex stress state of uniaxial tension followed by uniaxial and triaxial compression, and, finally, (3) determination of the internal structure of the rocks using methods based on X-ray imaging. Multi-proxy characteristics of the materials including numerous observations and methods were performed: optical microscopy used to characterise rock petrography and mineralogy, scanning electron microscopy (SEM) coupled with EDS, as well as grinding tests; furthermore, mechanical properties were determined on cylindrical samples in accordance with European standards. X-ray microtomography using the XμCT method enabled microscopic observations and determination of the orientation of discontinuities and the rock structure. The performed analyses allowed us to distinguish three lithological types of sandstone and two types of limestone among the examined stone blocks. Stone blocks of fine- and medium-grained sandstone with carbonate binders, as well as sparitic limestone and mudstone with calcite veins, were used to build the studied structures. The analysed blocks showed traces of partial edge processing. Despite the defects in the material structure identified using XμCT, all the types of rock were characterised by high or very high strength. High values of longitudinal wave velocity confirmed the good quality of the material. These results contribute to a better understanding of the construction process and the related technological choices, and they provide the first dataset which can be used for the reconstruction of the building's original appearance in the future.

Petrographic, Petrophysical, and Mechanical Characterisation of the Ultra- Tight Casa Cruz Sandstone, Moruga Formation, Southern Basin, Trinidad

Durability, compactness, and natural strength of sandstones are pivotal properties for its subsequent application as a building material. If a sandstone is tight and contains petroleum, then hydraulic fracturing is necessary to achieve commercial production. The Casa Cruz Sandstone Member, southern Trinidad, is currently being explored as a potential petroleum target and building material. This study investigates the petrographic, petrophysical, and mechanical characteristics of the Casa Cruz sandstone to understand the factors that control the quality of the sandstone and to determine the sandstone’s suitability as a natural resource. A thin-section analysis was performed to investigate the mineralogy, texture, and diagenesis of the sandstone. Permeability, porosity, density, P- and S-wave velocities, unconfined compressive strength (UCS) and confined compressive strength were measured. The elastic properties (Young’s modulus, shear modulus, bulk modulus, and Poisson’s ratio) were estimated from inversion of the P- and S-wave velocities. The results show that the Casa Cruz sandstone is one of the tightest sandstone types reported in the literature with porosity of 0.7% and permeability of 4.7 x 10-22 m2 (0.47 nD). Authigenic cementation and mechanical compaction are the main diagenetic processes that jointly controlled the quality of the sandstone. The sandstone was classified as a very strong (UCS of 128 MPa) quartz-arenite and is barren of petroleum and bioclasts. Brittle failure behaviour was exhibited, accompanied by axial splitting fractures and shear fractures under unconfined and confined conditions, respectively. The Casa Cruz sandstone is suggested to be an excellent building material as its petrophysical and mechanical properties are comparable to those of commercial industry grade of Westerly granite and Naparima Hill argillite.

Sandstone Provenance of Walanae Formation as a Parent Rock in Bulukumpa area, Bulukumba Regency, South Sulawesi

The Walanae Formation has a wide distribution in the southern arm of Sulawesi, this rock formation was deposited during the formation of the basin due to the Walanae strike-slip fault. The Walanae Formation in the study area comprises sedimentary rocks and pyroclastic rocks, which give different soil characteristics. This study aims to determine the types of sandstones, rocks of origin, and provenance of sandstones in the study area by using spot sampling at representative stations and petrographic analysis. The sandstones of the study area are divided into two groups based on Folk (1974), namely arkose lithic and feldspathic litharenite. Based on the type of quartz, rock fragments, and associated minerals, the origin of the sandstones in the study area are plutonic igneous rocks, volcanic rocks, sedimentary rocks, and metamorphic rocks. The results show that the types of provenance sandstones in the study area are magmatic arc and recycled orogenic.

Zhaman-Koitass granite-leukogranite massif (Northern Kazakhstan): U-Pb age, mineralogical and geochemical features, geodynamic analysis

Research subject. The Zhaman-Koitass granite-leucogranite massif of the Borovsk complex in Northern Kazakhstan. In the platform cover of the West Siberian plate, overlying granite-leucogranites, a large uranium deposit Semizbai of sandstone type is localized. Materials and methods. Geochemical, mineralogical, and geochronological studies of granite-leucogranites were conducted by X-ray fluorescence analysis, ICP-MS, electron probe microanalysis, scanning electron microscopy, and LA-ICP-MS (Analytical Center for multi-elemental and isotope research SB RAS). Results and conclusions. The Zhaman-Koitass massif is composed by A-type subalkaline leucogranites (SiO2 = 72.8–75.4 wt %, Na2O + K2O = 7.5–8.8 wt %, K2O/Na2O = 1.11–1.25, ∑REE = 120–231 ppm, (La/Yb)n = 10–22, Eu/Eu* = 0.2–0.4), which are characterized by titanite-ilmenite-magnetite accessory specialization. U-Pb isotope dating confirms the silurian age of the Zhaman-Koitass granite-leucogranites (426–420 Ma). The obtained geochronological data, along with the similarity of the chemical composition of the rocks, confirm that the granite-leucogranites of the Zhaman-Koitass massif belong to the Borovsk complex. The significant age interval between the ordovician granitoids of the krykkuduk complex (448 ± 2 Ma) and the silurian granite-leucogranites of the karabulak and borovsk complexes considered in the article (431–426 Ma) suggests a change in the geodynamic situation from suprasubduction to transform marginal-continental.

Provenance of the lower Cretaceous Lumshiwal Formation, Surghar Range, northwestern Indian Plate, Pakistan: Insights from new petrographical and geochemical analysis

This paper documents the provenance and palaeoclimatic conditions of the Cretaceous Lumshiwal Formation near the western margin of the Indian plate in the Surghar Range, northwest Pakistan. The combined techniques of petrography, X-ray diffraction (XRD), and bulk rock geochemistry were utilized to reveal the source and mineral-geochemical composition and sandstone type. The petrographic analysis of the sandstones confirms the dominance of quartz, feldspar, and rock fragments, with subordinate occurrences of muscovite, magnetite, and hematite. Heavy minerals consist of tourmaline, titanite (sphene), rutile, cassiterite, monazite, and zircon. The cementing material includes ferruginous clays, jarosite, glauconite, calcite, minor dolomite, gypsum, and silica. The modal composition plot of the sandstones falls into arkose to sub-arkose, with a few lithic arkose varieties. Lithic fragments mainly include granite, with a minor occurrence of granitic gneiss, chert, phyllite, and quartz mica schist. The discriminatory provenance diagram of the sandstones suggests a transitional continental provenance. The bulk rock geochemistry of the sandstones reveals the presence of SiO2, TiO2, Al2O3, Fe2O3, FeO, MnO, CaO, MgO, Na2O, K2O and P2O5. The petrographical mineral findings were corroborated with XRD, SEM, and bulk rock geochemistry analysis (major element concentrations and their ratios), which collectively all confirm a felsic igneous source. The tectonic discrimination diagram (SiO2-log K2O/Na2O wt %) implies a dominant influx of sediment sourced from the passive continental margin of the uplifted Gondwana Indian plate. Terrigenous sediments found in the Lumshiwal Formation are interpreted to have been derived from granites and granitic gneisses of the Indian Shield. The palaeo-weathering index, including the chemical index of alteration (CIA) and the chemical index of weathering (CIW) of the Lumshiwal Formation confirms a low to moderately weathered source area. The climate discrimination plot (SiO2 versus Al2O3 + Na2O + K2O) shows that humid to semi-humid climatic conditions during the deposition of the Lumshiwal Formation.

Importance of diagenetic heterogeneity in Chang 7 sandstones for modeling CO2-water-rock interactions

The diagenetic heterogeneity of the tight sandstone of Yanchang Formation in Ordos Basin is significant, and the surface area of reactive minerals varies greatly among different types of sandstones. Geochemical modeling was used to assess the impact of diagenetic heterogeneity on CO2-water-rock interactions in Chang 7 sandstones. Reactive surface area (RSA) for each mineral was determined using image analysis and the results were integrated into geochemical simulations of CO2-water-rock interactions to assess the mineralogical evolution of different diagenetic facies sandstones after CO2 injection. The simulation results show that the mineralogical evolution and porosity change of sandstones with different diagenetic facies are different under the same CO2-rich fluid environment, and the mineralization amount is also different. The results of this study show that even under similar sedimentary environment, tectonic location and burial-thermal history conditions, the differential response of different diagenetic facies to CO2-rich fluids cannot be ignored. It is necessary to consider the effect of diagenetic heterogeneity when evaluating CO2 sequestration at large scale.

TOWARDS ASSESSING SANDSTONE SURFACE MOISTURE AND DEGRADATION LEVEL FROM RADIOMETRICALLY CORRECTED TLS INTENSITY DATA

Abstract. Water is a prevalent deterioration agent for historic masonry works, especially those made of clay-bearing sandstones. To preserve cultural heritage made of sandstone, it is important to monitor, and then detect the regions with water retention or stone deterioration. To that aim, we investigate the prospects of terrestrial laser scanner (TLS) intensities for quantifying moisture in sandstone. Through a series of experiments following the drying processes of sandstone samples, we verify that TLS intensities can serve as moisture proxies for remote-sensing water retention. We identify the theoretically most suitable wavelengths, systematic effects requiring mitigation, and promising mitigation strategies. However, we also observe that the intensities are significantly affected by the type of sandstone and its level of degradation. Our results indicate that it is possible to distinguish different sandstones and levels of artificial degradation by observing and analyzing TLS-intensity time series during the drying process.

Characterizing rock transverse anisotropic spatial variations using digital drilling

Transverse anisotropy plays an important role in the engineering behavior of rock masses. This study examines the transverse anisotropic spatial variations and evaluates them using the coefficient of variation (CV) and anisotropy index (AI) through digital drilling tests. Four types of rocks, shale (SH), mudstone (MU), sandstone (SA), and schist (SC), are studied in four directions, revealing significant transverse anisotropy at the cutting point. The results demonstrate that the effect of the depth per rotation on the difference is weaker compared to the scaled weight and torque. The ranking of transverse anisotropy in the tested rocks is: MU > SA > SH > SC. Transverse anisotropy changes along the drilling depth vary across rock types. With the increase of drilling depth, SH experiences a decrease, rebound, and another decrease. MU shows an initial increase followed by a decrease. For SA, the degree of transverse anisotropy decreases and is sustained at a lower extent. SC exhibits slight fluctuations with the exception of the abrupt change. The time when the drilling bit is in perfect contact with the rock and the cutting efficiency in different drilling directions are the main factors causing the transverse anisotropy. The intricate evolution of transverse anisotropy should be worth investigating on a wider scale.

The Effect of Ultrasonic Alternating Loads on Restoration of Permeability of Sedimentary Rocks during Crude Paraffinic Oil Flow

This paper presents the results of experimental studies on the filtration of reservoir fluid through the rocks under the influence of nonlinear loads. A laboratory rig is assembled that allows for modeling the flow of fluid from the reservoir into the well during the propagation of elastic waves from the well. It is shown that depending on the permeability of the rock matrix as well as on the concentration of paraffins and asphaltenes in crude oil, the effect of the nonlinear load is different. Three types of sandstone are studied: low, medium, and high permeability. The greatest influence of nonlinear loads is observed in high-permeability sandstone. The effect manifests itself in fully unblocking the pore space from paraffins and asphaltenes accumulated in pore throats and restoring the oil permeability to its original value. In the case of medium-permeability sandstone subjected to nonlinear loads, blocking of the pore space is slow. In the case of low-permeability sandstone, the impact of nonlinear loads does not have a significant effect. When studying water filtration in the presence of residual oil saturation, the effect of nonlinear loads is observed as a mobilization of additional oil not previously involved in the filtration process, which also leads to an increase in the water permeability of the rock.

Pore-Scale Characterization of CO2 Trapping and Oil Displacement in Three-Phase Flow in a Heterogeneous Layered Sandstone

Summary Permeability variation in the vertical direction, a typical sandstone reservoir heterogeneity, can trap a large amount of oil in the low-permeability layer. We performed water-alternating-gas (WAG) injection and CO2 foam flooding on a specially constructed millimeter-sized layered sandstone and investigated fluid distribution using high-resolution X-ray microtomography. Based on the segmented images, CO2 capillary-trapping capacity, oil recovery, Euler number, shaper factor, capillary pressure, and fluid flow conductivity were calculated. Our results show that increasing the number of WAG cycles favored CO2 capillary trapping, and oil recovery was enhanced by the WAG strategy. However, there was still a significant amount of oil trapped in the low-permeability layer. After the WAG injection, the connectivity of the residual oil clusters decreased, the capillary pressure of the oil clusters increased, and oil flow conductivity decreased. This was not conducive to further oil recovery. The subsequent injection of CO2 foam effectively recovered the oil in the low-permeability layer. During the no-injection period, we observed a crossflow phenomenon caused by gravity segregation (the high-permeability layer was located below the low-permeability layer), i.e., oil in the low-permeability layer decreased while oil in the high-permeability layer increased, which is beneficial for subsequent oil production. Furthermore, CO2 moved upward driven by gravity, and although capillary barriers could prevent CO2 from escaping, subsequent water injection was essential to improve the stability of CO2 capillary trapping. This work accurately quantifies the distribution of oil and gas in high- and low-permeability layers, thus providing fundamental data for oil recovery and CO2 trapping in reservoirs with vertical heterogeneity. Although the sample used in the experiment was not natural reservoir rock, our results imply that when the permeability ratio between the two layers is greater than 2, sufficient attention must be paid to the fluid distribution differences caused by this layered heterogeneity. Different displacement strategies, such as WAG and CO2 foam flooding, or gravity differences between oil and gas can be used to enhance oil recovery.

Interpretasi Struktur Bawah Permukaan Menggunakan Data Anomali Medan Magnet Daerah Manifestasi Panas Bumi Sampuraga Kabupaten Mandailing Natal

This research was conducted to identify the distribution of magnetic field anomalies to determine the subsurface structure of the area around Sampuraga hot springs. Magnetic field data was measured using a magnetometer in an area with dimensions of 1400 m x 1100 m with 154 points. The measurement data is a total magnetic field, and to obtain magnetic field anomaly values, corrections are made for diurnal variation and IGRF correction. Magnetic field anomaly values range from 353,1 nT to 7622,0 nT. Magnetic field anomaly data were processed using the Oasis Montaj software by reducing to the poles, upward continuation, and 2D modeling. The 2D modeling results show three layers of soil in the study area. The upper part (first and second layers) is interpreted as a caprock. This layer consists of sedimentary rock types of sandstone and clay and igneous rock in the form of granite at a depth of up to 1700 m. The lower part (third layer) is interpreted as a reservoir. This layer consists of metasedimentary volcanic rock, clay alteration, andesitic lava, and dacitic lava with a depth of up to 2030 m from the ground surface. The results of this model also interpret the fault zone as an outflow zone so that it forms manifestations on the surface. These three geothermal system components show that the Sampuraga area can be further developed and explored.

Study on Brittleness Characteristics and Fracturing Crack Propagation Law of Deep Thin-Layer Tight Sandstone in Longdong, Changqing

Tight-sandstone oil and gas resources are the key areas of unconventional oil and gas resources exploration and development. Because tight-sandstone reservoirs usually have the characteristics of a low porosity and ultralow permeability, large-scale hydraulic fracturing is often required to form artificial fractures with a high conductivity to achieve efficient development. The brittleness of rock is the key mechanical factor for whether fracturing can form a complex fracture network. Previous scholars have carried out a lot of research on the brittleness characteristics of conglomerate and shale reservoirs, but there are few studies on the brittleness characteristics of sandstone with different types and different coring angles in tight-sandstone reservoirs and the fracture propagation law of sandstone with different brittleness characteristics. Based on this, this paper carried out a systematic triaxial compression and hydraulic fracturing experiment on the tight sandstone of Shan 1 and He 8 in the Longdong area of the Changqing oilfield. Combined with CT scanning cracks, the brittleness characteristics and fracturing crack propagation law of different types and different coring angles of sandstone under formation-confining pressure were clarified. The results show that there are great differences between different types of sandstone in the yield stage and the failure stage. The sandstone with a quartz content of 100% has the highest peak strength and a strong brittleness. Sandstones with a high content of natural fractures and dolomite have a lower peak strength and a weaker brittleness. There are also differences in the peak strength and fracture morphology of sandstone with different coring angles due to geological heterogeneity. The sandstone with a comprehensive brittleness index of 70.30 produces a more complex fracture network during triaxial compression and hydraulic fracturing than the sandstone with a comprehensive brittleness index of 14.15. The research results have important guiding significance for on-site fracturing construction of tight-sandstone reservoirs.

Evolution of residual strain and strain energy in rocks under various types of uniaxial cyclic loading-unloading

In the process of roadway excavation, the rock mass around the roadway is often subjected to cyclic loads, and the rock mechanical properties and strain energy evolution under cyclic loads are obviously different from those under compression, so it is urgent to carry out research on rock mechanical properties and strain energy evolution under cyclic loads. This study aims to investigate the evolution of residual strain and strain energy in rocks under uniaxial cyclic loading-unloading experiments (UCLUE). Four types of rocks, namely coal, white sandstone, red sandstone, and granite, were subjected to uniaxial compression experiments (UCE) and various uniaxial cyclic loading-unloading experiments (UEACLUE). The findings are as follows: analysis of UEACLUE revealed a gradual decrease in residual strain with an increasing number of cycles, leading to its eventual disappearance. However, if the cyclic loading-unloading (CLU) was continued beyond this point, the rocks displayed a reappearance of residual strain. The number of cycles required to eliminate residual strain was found to be inversely proportional to the peak strength of the rocks, while directly proportional to the upper limit value of UCLUE. Among the different stages of the uniaxial cyclic loading and unloading test, the plastic stage of white sandstone exhibited the largest disparity in dissipated strain energy, followed by the plastic stage of red sandstone, with coal displaying the smallest difference. Analysis of dissipated strain energy in the four types of uniaxial cyclic loading and unloading tests revealed differences of 0.00348 mJ▪mm−3, 0.03488 mJ▪mm−3, 0.02763 mJ▪mm−3, and 0.01619 mJ▪mm−3 in the plastic stage for the respective rock types. Furthermore, examination of the input strain energy density (ISED) and dissipated strain energy density (DSED) during the CLU process showed a linear relationship between these variables. Additionally, the investigation of ISED and DSED in other types of UCLUE demonstrated adherence to the cyclic-linear dissipation law (CLDL). The study of mechanical properties and strain energy evolution under CLU is of positive significance for the development of rock fatigue damage and rock damage mechanics.

Method of fabricating artificial rock specimens based on extrusion free forming (EFF) 3D printing

Three-dimensional (3D) printing technology has been widely used to create artificial rock samples in rock mechanics. While 3D printing can create complex fractures, the material still lacks sufficient similarity to natural rock. Extrusion free forming (EFF) is a 3D printing technique that uses clay as the printing material and cures the specimens through high-temperature sintering. In this study, we attempted to use the EFF technology to fabricate artificial rock specimens. The results show the physico-mechanical properties of the specimens are significantly affected by the sintering temperature, while the nozzle diameter and layer thickness also have a certain impact. The specimens are primarily composed of SiO2, with mineral compositions similar to that of natural rocks. The density, uniaxial compressive strength (UCS), elastic modulus, and tensile strength of the printed specimens fall in the range of 1.65–2.54 g/cm3, 16.46–50.49 MPa, 2.17–13.35 GPa, and 0.82–17.18 MPa, respectively. It is capable of simulating different types of rocks, especially mudstone, sandstone, limestone, and gneiss. However, the simulation of hard rocks with UCS exceeding 50 MPa still requires validation.

Study on Changes in Physical and Mechanical Properties and Integrity Decay of Sandstone Subjected to Freeze–Thaw Cycling

To investigate the effects of long-term freeze–thaw cycles on the physical and mechanical properties as well as the attenuation trend of rocks, this study conducted saturated freeze–thaw tests on coarse sandstone and fine sandstone samples collected from the slopes of Muli Coal Mine in Qinghai Province. The samples underwent different numbers of freeze–thaw cycles, and their porosity, longitudinal wave velocity, and uniaxial compression strength were studied. The variations in the physical and mechanical properties of the two types of sandstone with respect to the number of freeze–thaw cycles were analyzed. Take uniaxial compressive strength (UCS) as the integrity index, and decay laws of rock integrity were analyzed based on the decay equation suggested in previous studies. We found that the decay index λ, which is commonly assumed to be constant, varies with the number of freeze–thaw cycles. Furthermore, the λ values varied between different rock types. For fine sandstone, the λ decreases with an increase in the number of freeze–thaw cycles, ranging from 0.00385 to 0.005. However, for coarse sandstone, the λ initially decreases and then increases with an increase in the number of freeze–thaw cycles. The range of λ for coarse sandstone is between 0.00376 and 0.00481. Finally, we established a relationship between the decay index, porosity, and longitudinal wave velocity in the fine sandstones. This relationship provides a more straightforward way to evaluate the integrity of fine sandstones subjected to different numbers of freeze–thaw cycles.