Rupture Properties Research Articles

Effect of carbon content on the microstructure and stress rupture properties of a 4th-generation nickel-based single crystal superalloy

The balance between the stress rupture properties and castability of a 4th-generation Ni-based single crystal superalloy can be achieved by addition of appropriate carbon content. In this work, the effects of carbon content on the microstructure and stress rupture properties of a 4th-generation Ni-based single crystal superalloy were investigated in detail. The results showed that minor carbon addition could aggravate the dendrite segregation, while the addition of carbon had no obvious effect on the rafting and distortion of γ′ phase during stress rupture deformation. At 760 °C/810 MPa and 1100 °C/210 MPa, the stress rupture lives of the three experimental alloys initially increased and subsequently decreased with the increasing carbon content. However, under condition of 1140 °C/137 MPa, the increased carbon content resulted in the reduction of the stress rupture lives of alloy. It was discovered that minor carbon elements addition (0.045 wt%) can promote formation of interfacial dislocation networks and improve creep resistance at high temperatures. At intermediate temperature, the introduction of carbon could reduce the stacking fault (SF) energy of γ matrix, thus facilitating the formation of SFs in γ matrix. The M6Cgranular carbides precipitated at high temperature, which was considered to be beneficial to stress rupture properties.

Rupture Mechanics of Blood Clots: Influence of Fibrin Network Structure on the Rupture Resistance

Embolization is a leading cause of mortality, yet we know little about clot rupture mechanics. Fibrin provides the main structural and mechanical stability to blood clots. Previous studies have shown that altering the concentration of coagulation activators (thrombin or tissue factor (TF)) has a significant impact on fibrin structure and viscoelastic properties, but their effects on rupture properties are mostly unknown. Toughness, which corresponds to the ability to resist rupture, is independent of viscoelastic properties. We used varying TF concentrations to alter the structure and toughness of human plasma clots. We performed single-edge notch rupture tests to examine fibrin toughness under a constant strain rate and we assessed viscoelastic mechanics using rheology. We utilized fluorescent confocal and scanning electron microscopy (SEM) to quantify the fibrin network structure under varying TF concentrations. Our results revealed that increased TF concentration resulted in increased number of fibrin fibers with a reduction in network pore size, thinner and shorter fibrin fibers. Increasing TF concentration yielded a maximum toughness at mid-TF concentration, such that fibrin diameter and number of fibers underlie a complex role in influencing the rupture resistance of blood clots, resulting in a nonmonotonic relationship between TF and toughness. A simple mechanical model, built on our findings from our Fluctuating Spring (FS) computational model, adopted to estimate the fracture toughness (critical energy release rate) as a function of TF predicts trends that are in good agreement with experiments. The differences in mechanical responses point to the importance of studying the structure-function relationships of fibrin networks, which may be predictive of the tendency for embolization. Statement of significanceFibrin, a naturally occurring biomaterial, is the main mechanical and structural scaffold of blood clots that provides the necessary strength and stability to the clot, ensuring effective stemming of bleeding. The rupture of blood clots can result in the blockage of downstream vessels thereby blocking blood flow and oxygen supply. The fibrin network structure has been shown to influence the viscoelastic mechanical properties of clots, but has not been explored for fracture mechanics. Here, we modulate the fibrin network structure by varying the concentration of Tissue Factor (TF). Interestingly, the association between TF concentration and maximum toughness of the clots is non-monotonic. The variations in mechanical responses highlight the importance of studying the structure-function relationships of fibrin networks, as these may predict the tendency for embolization.

Effect of HIP on Creep Properties in the Single Crystal Superalloy

The Rene N5 is a second-generation single crystal superalloy containing 3wt% Re, commonly used in gas turbine blades for power generation at temperatures up to 1600°C due to its excellent creep life. Generally, single crystal (SX) and directionally solidified (DS) blades are not applied to hot isostatic pressing (HIP) because their porosities are lower than conventionally cast (CC) blades, and it causes recrystallization issue. However, in this study, HIP was chosen as a candidate to improve the mechanical properties of the second-generation single crystal superalloy Rene N5. HIP followed by ultra-rapid cooling rate of 660K/minute was applied in an attempt to address this issue. This approach was expected to enhance creep rupture properties through pore reduction and microstructural homogenization. Furthermore, by setting the HIP temperature and time identical to the solution treatment condition, the possibility of replacing solution treatment with HIP was discussed. As results of creep rupture tests, the rupture life was excellent in the order of specimens treated with HIP + solution + aging, solution + aging, and HIP + aging treatments. It is interesting that this is found to be primarily influenced by the size and shape of carbides and γ’ phases, with the effects of crystallographic orientation, shrinkage porosity, and eutectic phase being negligible.

Integration of multiple observations for validation of mechanisms of earthquake-triggered groundwater level Anomalies: 2016 Taiwan Meinong earthquake

This study analyzes multi-depth groundwater level data and integrated observation data to validate the previously proposed mechanisms of hydrological anomalies triggered by the 2016 M6.4 Meinong earthquake in Taiwan. The main influence area was northwest of the epicenter, which may be due to the blind fault rupture, intensity distribution, and hydrogeological properties. The step changes in groundwater level do not fit the concept of epicentral distance, static stress–strain theory, or the focal mechanism. The distribution of step changes in groundwater level have a pattern similar to that of horizontal peak ground velocity. The results imply that these changes may be driven by dynamic stress–strain, instead of static stress–strain. The minimum horizontal peak ground velocity and acceleration of the Meinong earthquake, which induced obvious step changes in groundwater level and soil liquefaction, are provided. The pressure dissipation ability of an aquifer (e.g., transmissivity) may affect the persistence of groundwater responses. Four wells located near the surface rupture area, which has cemented or partial cemented geological material, showed an obvious step decrease in the groundwater level at a deep depth and all wells showed an increase in the groundwater level at a shallow depth. These decreases and increases of the groundwater level at different depths have different mechanisms, which are discussed in this study. The integrated observations made during the Meinong earthquake show that ground motion and the hydraulic properties might be important factors in hydrological anomalies. The results of this study are an important reference for further studies on earthquake hydrology.

Tailoring microstructural stability and stress rupture properties of a solid-solution strengthened Fe-Ni-based superalloy via niobium addition

The influence of niobium (Nb) addition on the microstructural stability and 750 °C/135 MPa stress rupture properties of a solid-solution strengthened Fe-Ni-based superalloy designed for fourth-generation (Gen IV) nuclear reactors was systematically studied. The results showed that the stress rupture life first increased and then decreased with the increase of Nb content. The alloy with the addition of 0.5 wt% Nb exhibited the best stress rupture properties, with a stress rupture life of 164 h. Compared to Nb-free alloy, the stress rupture life has been increased by 382 %. The enhanced creep performance of this alloy was closely related to its excellent high-temperature microstructural stability, which can be explained as follows: homogeneous and optimal grain size distribution, elemental Nb provided good solid-solution strengthening effects, fine granular secondary carbides relieved stress concentration and strengthened grain boundaries (GBs), dynamic precipitation of nano-sized NbC carbides effectively pined dislocations. Dynamic recrystallization (DRX) behavior can be observed in all alloys. The mechanisms related to DRX behavior were discussed, and it was deemed that the smaller average grain size, higher blocky NbC volume fraction, and increased stacking-fault energy (SFE) may be responsible for the facilitated DRX in the alloy with higher Nb content, which greatly caused local softening and consequently, decreasing the creep resistance of the alloy. Important guidance for the further design and development of γ′-free Fe-Ni-based superalloys for Gen IV nuclear reactors with good high-temperature microstructural stability and creep performance could be summarized from the present study.

Effect of Carbon on the Microstructures and Stress Rupture Properties of a Polycrystalline Ni-Based Superalloy

Effect of Carbon on the Microstructures and Stress Rupture Properties of a Polycrystalline Ni-Based Superalloy

Effect of Overheating Treatment on Microstructure and Stress Rupture Properties of a Nickel-Based Single-Crystal Superalloy

Effect of Overheating Treatment on Microstructure and Stress Rupture Properties of a Nickel-Based Single-Crystal Superalloy

Imaging microearthquake rupture processes using a dense array in Oklahoma

Both large and small earthquakes rupture in complex ways. However, microearthquakes are often simplified as point sources and their rupture properties are challenging to resolve. We leverage seismic wavefields recorded by a dense array in Oklahoma to image microearthquake rupture processes. We construct machine-learning enabled catalogs and identify four spatially disconnected seismic clusters. These clusters likely delineate near-vertical strike-slip faults. We develop a new approach to use the maximum absolute SH-wave amplitude distributions (S-wave wavefields) to compare microearthquake rupture processes. We focus on one cluster with earthquakes located beneath the dense array and have a local magnitude range of -1.3 to 2.3. The S-wave wavefields of single earthquakes are generally coherent but differ slightly between the low-frequency (<12 Hz) and high-frequency (>12 Hz) bands. The S-wave wavefields are coherent between different earthquakes at low frequencies with average correlation coefficients greater than 0.95. However, the wavefield coherence decreases with increasing frequency for different earthquakes. This reduced coherence is likely due to the rupture differences among individual earthquakes. Our results suggest that earthquake slip of the microearthquakes dominates the radiated S-wave wavefields at higher frequencies. Our method suggests a new direction in resolving small earthquake source attributes using dense seismic arrays without assuming a rupture model.

High-temperature tensile rupture property of (Nb,W) co-alloying TiAl-based alloys

In order to explore whether (Nb,W) co-alloying TiAl-based alloys with relatively higher W addition have better high-temperature tensile rupture property, Ti-44Al-4Nb-1 W-0.1B alloy is designed and prepared. Ti-44Al-8Nb-0.1B alloy and Ti-44Al-7.2Nb-0.2 W-0.1B alloy are also prepared for comparative study. The rupture property testing is carried out at 800 °C and different tensile stresses. The property data, macro/microstructure evolution, fracture surface, W content, crack failure behaviors are studied. The results show that the (Nb,W) co-alloying alloys have better rupture property than the pure Nb alloying alloy. For the (Nb,W) co-alloying alloys, the higher W contained Ti-44Al-4Nb-1 W-0.1B alloy has the better property under lower tensile stress, and the lower W contained Ti-44Al-7.2Nb-0.2 W-0.1B alloy has the better property under higher tensile stress. The relationships of rupture life t and stress σ for the three alloys are given. All the three alloys have a coupling fracture mode of ductile fracture and brittle fracture. The ductile fracture exhibits the typical dimple characteristics. The brittle fracture exhibits the typical trans-granular cleavage, river-like pattern and trans-lamella fracture characteristics. The higher the stress, the more brittle fracture characteristics there are. After rupture property testing, the (α2 + γ) lamella colony sizes of the three alloys all decrease, indicating that DRX and grain boundary slip occur not only along (α2 + γ) lamella colony boundary, but also inside it. The colony boundary regions have the stress concentration, where the B2 phase produces the better buffering and coordination, and as well as the dislocation tangles, DRX and grain boundary slip can be found by EBSD and TEM. EPMA results show that the more W added in the alloy, the more W content is in the (α2 + γ) lamella matrix, which is beneficial for the rupture property. However, more W addition will also lead to the formation of more B2 phase in the initial as-cast microstructure. So that, under higher tensile stress, when the stress intensity factor K is higher, the crack failure is more likely to occur.

Kinematic Source Properties of the 2023 Mw 7.7 Türkiye Earthquake Inferred from Near-Fault Strong Ground Motions

Abstract The 2023 Mw 7.7 Türkiye earthquake provided densely observed near-fault ground-motion data, which enabled us to investigate their characteristics and generations. This study aimed to obtain an intuitive understanding of the characteristics of near-fault strong ground motions and their relationship with kinematic source properties using a simple source model. Synthetic ground motions were calculated using the discrete wave number method and compared with observed ground motions. The observed strong motions were used after a time correction based on the first P-wave arrival. Results showed that near-fault pulse-like velocities (0.02–0.6 Hz) were generally explained by the simple kinematic source model that assumed a continuous rupture propagation along the faults. Comparisons at individual sites indicate the various rupture properties of the fault segments. Near-fault ground motions along the Narli segment were explained by the fault plane along the surface trace and not by aftershock distribution. A supershear rupture propagation speed is necessary for a part of the Amanos segment. Rupture stops and restarts were implied near the stepover along the Amanos segment. Empirical site factors estimated by generalized inversion techniques did not show peaks around the frequency of observed large velocity pulses, indicating that the velocity pulses were mainly generated by the source. The model bias and uncertainties were also examined to supplement the simplified subsurface structure used in the simulation. Our results will help to associate the qualitative and quantitative aspects of the kinematic source process with near-fault strong ground motions.

Effects of stabilized heat treatment on stress rupture properties of high Si-bearing austenitic stainless steel weld metal

The 15Cr-9Ni-Nb austenitic stainless steel weld metal with a Si content of 3.5 wt% was prepared via gas tungsten arc welding and then held at 900 °C for 3 h for the stabilized heat treatment (SHT). The stress rupture properties of the as-welded (AW) and SHT weld metals at 550 °C were evaluated via the Larson-Miller parameter. The microstructure evolution was discussed during the 550 °C stress rupture process. The coarse σ-phase and relatively fine G-phase formed on the δ-ferrite during aging at 550 °C. In the AW weld metal, the continuous δ-ferrite with a large amount of coarse σ-phase led to the formation and expansion of cracks during the stress rupture process, which accelerated the eventual rupture and damaged the stress rupture properties. The SHT decreased the δ-ferrite content and formed a large amount of nanoscale NbC precipitated in the matrix. The decreased δ-ferrite content avoided the rapid formation and expansion of cracks and the nanoscale NbC blocked the dislocation movement during the stress rupture process, which improved the stress rupture properties.

Creep rupture properties of dissimilar welded joint of ferritic/martensitic P92 steel and Inconel 617 alloy

The dissimilar welded joint (DWJ) comprising P92 steel and Inconel 617 (IN617) is frequently utilized in advanced ultra-supercritical (AUSC) boilers. In present work the creep rupture behaviour, rupture mechanism and microstructure evolution of DWJ of P92 steel and IN617 with Ni-based ERNiCrCoMo-1 filler, were examined at 650 °C under the stress range of 120–200 MPa. The results of the creep test indicated that the location of creep rupture varied across different testing conditions, encompassing areas such as P92 base metal and the fine-grained heat-affected zone (FGHAZ). The creep tested specimens within the stress range of 180–200 MPa exhibited failure originating from P92 base metal, predominantly influenced by plastic deformation. The failure manifested in a transgranular mode, driven by the formation, growth, and eventually coalescence of microvoids. The creep tested specimens within the stress range of 120–150 MPa displayed the characteristic ofType IV failure, primarily attributed to matrix softening and the absence of adequate precipitates to pin the PAGBs. Microstructural characterization unveiled the presence of microvoids along the PAGBs, facilitating microvoid nucleation primarily owing to the existence of the coarse brittle carbide phase. The growth of these microvoids over a period of time during tertiary stage of creep which lead to their coalescence and the formation of microcracks, ultimately resulting in premature intergranular failure. The specimen creep exposed at 650 °C under the lower stress of 120 MPa exhibited higher creep rupture life for 432 h. The SEM/EDS study of the crept sample of 120 MPa is also confirmed the presence of intermetallic laves phases in regions near the fracture tip and in the heat-affected zones (HAZs). Although the creep tested specimens at 150 MPa and 120 MPa exhibited failure in the FGHAZ and their elemental SEM/EDS analysis confirmed the presence of an oxide layer and notch formation near the interface of P92 base metal and ErNiCrCoMo-1 filler weld. The FESEM study revealed the growth of the oxide layer in the notch region, and it also showed the presence of multiple cracks and microvoids in the oxide layer. The formation and propagation of the oxide notch mainly led to the interfacial failure. The crept specimens subjected to 180 MPa and 200 MPa did not exhibit any cracks or microvoids in HAZs. However, specimens that failed under applied stresses of 120 MPa and 150 MPa revealed the presence of a high density of microvoids in the FGHAZ, inter-critical heat-affected zone (ICHAZ), and in the region of the coarse-grained heat-affected zone (CGHAZ) adjacent to the interface attached with an oxide layer.

The Influence of Microstructural Arrangement on the Failure Characteristics of 3D-Printed Polymers: Exploring Damage Behaviour in Acrylonitrile Butadiene Styrene.

This study investigated how printing conditions influence the fracture behaviour of 3D-printed acrylonitrile butadiene styrene (ABS) under tensile loading. Dog-bone-shaped ABS specimens were produced using the fusion filament fabrication technique, with varying printing angles. Tensile tests were conducted on pre-notched specimens with consistent pre-notch lengths but different orientations. Optical and scanning electron microscopies were employed to analyse crack propagation in the pre-notched specimens. In order to support experimental evidence, finite element computation was implemented to study the damage induced by the microstructural rearrangement of the filaments when subject to tensile loading. The findings revealed the simple linear correlation between the failure properties including elongation at break and maximum stress in relation to the printing angle for different pre-notch lengths. A more progressive damage was found to support the ultimate performance of the studied material. This experiment evidence was used to build a damage model of 3D-printed ABS that accounts for the onset, growth, and damage saturation. This damage modelling is able to capture the failure properties as a function of the printing angle using a sigmoid-like damage function and a modulation of the stiffness within the raster. The numerical results demonstrated that damage pattern develops as a result of the filament arrangement and weak adhesion between adjacent filaments and explains the diffuse damage kinetics observed experimentally. This study concludes with a topological law relating the notch size and orientation to the rupture properties of 3D-printed ABS. This study supports the idea of tailoring the microstructural arrangement to control and mitigate the mechanical instabilities that lead to the failure of 3D-printed polymers.

New insights into the stress rupture life enhancement mechanisms of a nickel-based superalloy

In this paper, the effects of hot isostatic pressing (HIP) and heat treatment (HT) on the stress rupture properties of nickel-based superalloy K417G were investigated. Scanning electron microscopy (SEM), electron backscatter diffraction (EBSD) and transmission electron microscopy (TEM) were employed to analyze the microstructure, fracture morphology, determination of crack source and dislocation evolution after stress rupture fracture. The results indicate that, HIP specimens demonstrate a 19.5% reduction in stress rupture life compared to as-cast specimens, whereas HIP + HT specimens exhibit a 41% increase in stress rupture life, reaching a value of 63.04 h. The fracture mechanism of the samples under different heat treatment conditions is different. There are a large number of pores in the as-cast specimen, which leads to the initiation and propagation of cracks and eventually result in fracture. The pores in the HIP specimen are almost eliminated. However, the coarsening and uneven distribution of γ′ phase led to the weakening of the hindrance to dislocation movement. Additionally, the increase in elongated carbides at grain boundaries accelerates crack initiation and propagation. Under HIP and HT, the cubic γ′ phase is uniformly precipitated, which effectively hinders the movement of dislocation lines. Granular M23C6 carbides precipitate at grain boundaries, acting as pinning points to retard grain boundary sliding and crack propagation, thus improving the stress rupture life.

Synergistic Effects of Boron and Rare Earth Elements on the Microstructure and Stress Rupture Properties in a Ni-Based Superalloy.

The synergistic effects of boron (B) and rare earth (RE) elements on the microstructure and stress rupture properties were investigated in a Ni-based superalloy. The stress rupture lifetime at 650 °C/873 MPa significantly increased with the addition of B as a single element. Furthermore, the stress rupture lifetime reached its peak (303 h), with a certain amount of B and RE added together in test alloys. Although the grain size and morphology of the γ' phase varied a little with the change in B and RE addition, they were not considered to be the main reasons for stress rupture performance. The enhancement in stress rupture lifetime was mostly attributed to the segregation of the B and RE elements, which increased the binding force of the grain boundary and improved its strength and plasticity. In addition, the enrichment of B and RE inhabited the precipitation of carbides along grain boundaries. Furthermore, nano-scale RE precipitates containing sulfur (S) and phosphorus (P) were observed to be distributed along the grain boundaries. The purification of grain boundaries by B and RE elements was favorable to further improve the stress rupture properties.

The influence of γ′ morphology and size on stress rupture properties in Ni-base superalloy IN738LC

This study investigates the influence of γ′ precipitate morphology and size on the creep deformation of the cast superalloy IN738LC under conditions of 760–982 °C and 78–674 MPa. Two microstructures were obtained by different heat treatments. The analysis of the experiments show that, according to the applied stress at 760 °C and 871 °C, the S1A material, with a bimodal distribution with large cuboidal γ′ and small spherical γ′, exhibited the longer creep life compared to those with a monomodal distribution with spherical γ′ precipitates. In the creep test at 760 °C, the S1A material exhibited a stacking fault within the primary cuboidal-shaped γ′ phase. The main deformation mechanism observed was isolated stacking fault (ISF) formation. Conversely, for the S2A material, an extended stacking fault (ESF) was observed, where dislocations continuously traversed several γ′ and γ phases. At 871 °C in low-stress creep tests, the S1A alloy displayed a dislocation network resulting from thermal activation, with localized stacking faults. In the S2A alloy, three-dimensional dislocations generated by climb were primarily observed around spherical γ′ precipitates, accompanied by localized stacking faults. At 982 °C, both S1A and S2A alloys exhibited rafting under lower stress, displaying similar lifetimes. The formation of a regular dislocation network at the interface between γ′ and γ matrix and rafting of γ′ precipitate proved beneficial in improved creep resistance of the alloy.

Effect of Pt on Stress Rupture Properties of Pt-Modified Nickel Aluminide Coatings at 1100 °C.

Platinum plays a crucial role in the superior high-temperature oxidation resistance of Pt-modified nickel aluminide (PtAl) coatings. However, PtAl coatings usually serve in thermo-mechanical coupling environments. To investigate whether Pt contributes to the high-temperature mechanical properties of PtAl coating, stress rupture tests under 1100 °C/100 MPa were performed on PtAl coatings with varying Pt contents. The different coatings were obtained by changing the thickness of the electroplated Pt layer, followed by a diffusion heat treatment and the aluminizing process in the present work. The results of the stress rupture tests indicated that an increasing Pt content resulted in a significant decrease in the stress rupture life of PtAl-coated superalloys under 1100 °C/100 MPa. Theoretical calculations and microstructural analysis suggested that an increased coating thickness due to the Pt content is not the main reason for this decline. It was found that the cracks generated close to the substrate in high-Pt-coated superalloys accelerated the fracture failure.

Moment-dependent rupture properties of deep-focus earthquakes in the Izu-Bonin subduction zone

SUMMARY The physical mechanisms controlling deep-focus earthquakes, or those observed at depths greater than 300 km, remain enigmatic. The leading processes by which deep-focus earthquakes are thought to occur include transformational faulting, thermal runaway and dehydration embrittlement, but distinguishing observations in support of one or more prevailing mechanisms are needed. In this study, we use a modified back-projection method, data recorded by the Hi-net array in Japan and a 3-D velocity model to produce source images of 19 deep-focus earthquakes within the Izu-Bonin subduction zone. We find that the rupture properties and fault plane orientations of imaged events separate according to reported moment magnitude, indicating the distinct operation of two moment-dependent causal mechanisms of deep-focus earthquakes in this region. We discuss these results in the context of previous observational, laboratory and numerical studies and emphasize the importance of continued research to validate the dual-mechanism hypothesis both in and outside Izu-Bonin. Such work may not only improve our understanding of the nucleation and propagation of deep-focus earthquakes, but also help clarify slab structure and subduction zone dynamics.

Fractal Spatial Distributions of Initial Shear Stress and Frictional Properties on Faults and Their Impact on Dynamic Earthquake Rupture

ABSTRACT We investigate the influence of the heterogeneous slip-weakening distance (DC) in dynamic rupture simulations, in which DC is proportional to the fault irregularities. Specifically, we compare a heterogeneous fractal DC distribution to a uniform DC over the entire fault when the initial shear stress is also heterogeneous. We find that even small changes in the average value of DC (<1 mm) can lead to significant differences in the rupture evolution; that is, the average DC and the way DC is distributed determines if the rupture is a runaway, self-arrested, or nonpropagating. We find that the self-arrested ruptures differ from runaway ruptures in the amount of area characterized by large slips (asperities). Self-arrested ruptures match the Somerville et al. (1999) asperity criteria in which ∼25% of ruptured area radiate ∼45% of the total seismic moment. This criterion is not satisfied for runaway ruptures. For runaway ruptures, ∼50% of the ruptured area radiates about 70% of the seismic moment, indicating that the ruptured area is not linearly proportional to the seismic moment. Self-arrested ruptures are characterized by dynamic shear stress drops (SDs) in the range ∼2.9–5.5 MPa, whereas for runaway ruptures the dynamic SDs increase to values between ∼12 and 20 MPa. Self-arrested ruptures generated by fractal distributed DC resemble the rupture properties of observed earthquakes. In addition, results show that the conditions for self-arrested ruptures are connected to the decrease of residual energy at rupture boundaries.

High-Temperature Creep and Microstructure Evolution of Alloy 800H Weldments with Inconel 625 and Haynes 230 Filler Materials

Alloy 800H stands as one of the few code-qualified materials for fabricating in-core and out-of-core components operating in high-temperature reactors. Welding is a common practice for assembling these components; however, the selection of a suitable filler material is essential for enhancing the high-temperature creep resistance of Alloy 800H weldments in high-temperature applications. In this study, Inconel 625 and Haynes 230 filler materials were used to weld Alloy 800H plates by employing the gas tungsten arc welding technique. The high-temperature tensile and creep rupture properties, microstructural stability, and evolution of the weldments after high-temperature exposure were investigated and compared with those of Alloy 800H. The results show that both weldments exhibit enhanced tensile and creep behavior at 760 °C. The creep rupture times of the weldments with Inconel 625 filler and Haynes 230 filler materials were about two and three time longer, respectively, than those of Alloy 800H base metal when tested at 80 MPa and 760 °C. Carbides (MC and M23C6) were commonly observed in the microstructures of both the weld and base metals in the two weldments after high-temperature creep tests. However, the Inconel 625 filler weldment displayed detrimental δ and Laves phases in the fusion zone, and these precipitates could be potential sites for initiating cracks following prolonged high-temperature exposure. This study shows that the weldment with Haynes 230 filler material exhibit better phase stability and creep rupture properties than the one with Inconel 625, suggesting its potential for use as a candidate filler material for Alloy 800H for further investigation. This finding also emphasizes the critical consideration of microstructural evolutions and phase stability in evaluating high-temperature materials and their weldments in high-temperature reactor applications.