Surface Roughness Research Articles

Photocatalytically active layered double hydroxide-PVDF composite membranes for effective remediation of dyes contaminated water

In this work, polyvinylidene fluoride (PVDF) intercalated CuFe layered double hydroxides (LDH) membranes were fabricated and investigated for UV-LED/persulfate degradation of methylene blue (MB), crystal violet (CV), methyl orange (MO), and Eriochrome black T (EBT) dyes from water. The PVDF-CuFe membrane exhibited improved heterogeneity, surface functionality (CuO, Fe-O, Cu-O-Fe), surface roughness, and hydrophilicity. The process parameters were optimized by response surface methodology, and maximum MB removal (100%) was achieved within 45.22-178.5 min at MB concentration (29.45-101.93 mg/L), PP concentration (0.5-2.41 g/L) and catalyst dosage (1.84-1.95 g/L). The degradation kinetics was well described by a pseudo-first-order model (R2=0.982) and fast reaction rate (0.029-0.089/min). The MB dye degradation mechanism is associated with HO•/SO4•− reactive species generated by Fe3+/Fe2+ or Cu2+/Cu+ in PVDF-CuFe membrane and PP dissociation. The PVDF-CuFe membrane demonstrated excellent recyclability performance with a 12% reduction after five consecutive cycles. The catalytic membrane showed excellent photocatalytic degradation of crystal violet (100%), methyl orange (79%), and Eriochrome black T (60%). The results showed that UV-LED/persulfate-assisted PVDF-CuFe membranes can be used as a recyclable catalyst for the effective degradation of dye-contaminated water streams.

Novel machine learning-driven multi-objective optimization method for EDM trajectory planning of distorted closed surfaces

Highly distorted closed surfaces pose significant challenges for machining trajectory planning due to their intricate surface constraints and closed structures. Despite these challenges, components with such features are prevalent in industries like aerospace. This paper presents a machine learning-driven multi-objective optimization method for electrical discharge machining (EDM) trajectory planning of highly distorted closed surfaces. The method transforms the structural design of forming electrodes and trajectory planning into a multi-objective decision problem. And a discrete point trajectory planning method, guided by surface average curvature, is employed to determine the optimal position and orientation of the electrode. Additionally, an elite dataset, generated using the Monte Carlo method and Arena's Principle, is utilized to train an artificial neural network (ANN). This network predicts hyperparameters for the nonlinear optimization problem. Based on the proposed method, a multi-objective optimization model is formulated for an integral shrouded blisk, considering minimization of iteration count, axial motion, and maximization of machining surface quality. The Pareto front is utilized to obtain the optimal EDM trajectory. Experimental results demonstrate a 17.38 % reduction in the overall machining cycle duration using this trajectory, and the surface roughness and profile accuracy satisfy the design specifications, which proves the effectiveness of this method.

Spatiotemporal prediction of surface roughness evolution of C/C composites based on recurrent neural network

Carbon/carbon (C/C) composites are widely used in aerospace applications due to their excellent properties. Their surface roughness is an important factor affecting the material properties and ablation resistance, which is essential for the accurate prediction of the material. Images are often used to summarize and characterize microstructural features, which include information such as fiber microstructure and fiber orientations. An ablation shape evolution model based on optimization of attention mechanism, which combines multi-scale convolutional neural network (MSCNN) and long short-term memory (LSTM) methods for the C/C composites, is proposed. MSCNN encodes the microstructural information of the ablation image, which is fed into the LSTM model to extract the spatiotemporal features and long-term dependencies latent in the temporal law. The attention mechanism is used to assign different weights to the extracted features which makes the model focus more on the important time steps in the sequence. The results show that the proposed model achieves excellent effects in predicting the evolution of ablative morphology, with high agreement with the simulated values. The method saves time and cost, while providing an efficient and reliable method for the design and optimization of thermal protection materials.

Investigation of surface finish and fatigue life of laser Powder Bed fused Ti-6Al-4V

In this fact-pacing world of technological advancement, the rise of additive manufacturing (AM) has found immense applications of metallic alloys such as Ti6Al4V to manufacture key components in automotive, aerospace and healthcare sectors. However, fatigue characteristics of such additively manufactured metal alloys is noticeably weak, and as such requires post-processing. In this study, AM Ti6Al4V manufactured by Laser Powder Bed Fusion (L-PBF) was treated by Hydrodynamic Cavitation Abrasive Finishing (HCAF) and Laser Cavitation Peening (LCP) to observe the improvement in surface roughness as well as fatigue performance. Our investigations revealed a substantial improvement in surface quality post-HCAF processing. Notably, the surface roughness of AM Ti6Al4V specimens showed a significant reduction of about 91.2 %, post surface treatment. However, Laser Cavitation Peening (LCP) treated sample demonstrates a significantly enhanced fatigue strength of 393 ± 22 MPa at 107, which was 1.75 times better than that of as-built one, i.e., 224 ± 16 MPa. This difference can be attributed to the distinct surface modification mechanisms of each technique. LCP, utilizing laser-induced shock waves, likely induces large compressive residual stresses, leading to better fatigue resistance.

Fabrication and performance optimization of an advanced pervaporation desalination membrane: A study utilizing PVDF and hydrophilic active layer as composite

Pervaporation emerges as a promising technique for brine treatment. In this investigation, we employed a PVDF substrate layer and applied various coating solutions using a simple spray technique to produce a composite pervaporation membrane. The composite membrane's chemical structure, morphology, hydrophilicity, swelling property, surface roughness, and crosslinking conditions were thoroughly investigated. Notably, the PVDF/PEI/P(SS-MA) composite membrane exhibited outstanding desalination performance, demonstrating high salt rejection and flux of 308.7 ± 13.8 kg m−2 h−1 when subjected to a 3.5 wt% sodium chloride solution. Even at an elevated brine concentration of 20 wt%, the membrane maintained a commendable flux of 88.76 ± 5.4 kg m−2 h−1 at 72 °C. These findings underscore the efficacy of the developed composite membrane for brine desalination applications.

Surface integrity and fatigue performance of Ti6Al4V alloy peened by sinking bead abrasive jet

Exploring a green, low-cost peening process to improve the surface integrity of titanium alloys, increasing fatigue life, and breaking through the limitations in large-scale applications is an urgent need at present. The study presents a novel peening method using sinking beads as the shot, combined with the low dust pollution and water film cushioning advantages of waterjet peening. The impact of the process on the surface integrity of titanium alloys is meticulously discussed to elucidate the microstructural evolution. Constant stress fatigue tests are performed to evaluate the effectiveness of the proposed method. It was found that the jet pressure and feed rate determined the energy density and the number of peening for sinking bead abrasives, which were the key factors affecting the surface material properties of the peening specimen. By optimizing the process parameters, the maximum surface residual compressive stress can reach 875.5 MPa, the microhardness can attain 481.7 HV, and the surface roughness can be reduced to 1.594 μm. The surface of the peened specimen is covered with impact craters, exhibiting a plastic deformation layer with evident grain refinement and lattice distortion. The ductility of the peened specimen decreased, with axial deformation reducing from 0.278 mm to 0.260 mm under constant cyclic stress. Due to the increase in microhardness and the introduction of residual compressive stresses, the fatigue cycles of the specimen were increased from 20692 to 33615, improving the fatigue life by 62.45%.

Hydrogen bonding-mediated interaction underlies the enhanced membrane toxicity of chemically transformed polystyrene microplastics by cadmium

The global attention on microplastic pollution and its implications for human health has grown in recent years. Additionally, the co-existence of heavy metals may significantly alter microplastics’ physicochemical characteristics, potentially amplifying their overall toxicity—a facet that remains less understood. In this study, we focused the membrane toxicity of modified polystyrene microplastics (PS-MPs) following cadmium (Cd) pretreatment. Our findings revealed that Cd-pretreated PS-MPs exacerbated their toxic effects, including diminished membrane integrity and altered phase fluidity in simulated lipid membrane giant unilamellar vesicles (GUVs), as well as heightened membrane permeability, protein damage, and lipid peroxidation in red blood cells and macrophages. Mechanistically, these augmented membrane toxicities can be partially ascribed to modifications in the surface roughness and hydrophilicity of Cd-pretreated PS-MPs, as well as to interactions between PS-MPs and lipid bilayers. Notably, hydrogen bonds emerged as a crucial mechanism underlying the enhanced interaction of PS-MPs with lipid bilayers.

Investigations of the hybrid laser polishing and high-temperature tribological properties of the 316L stainless steel formed by selective laser melting

In this study, the rough surfaces of additive manufactured parts were polished using an innovative combined treatment of continuous wave (CW) laser and inclined femtosecond (fs) laser techniques. The high-temperature friction and wear performances of the initial surface and the polished surface were investigated. The results indicate that the surface roughness was reduced to 0.21 µm and a fine-grained layer of approximately 25 µm was generated through CW-fs laser polishing. The coefficient of friction and wear volume of the CW-fs laser polished surface showed the most significant reductions of 52.2 % and 88.3 %, respectively, compared to those of initial surface under high-temperature conditions.

Mechanical properties and strain rate effect of graphene oxide grafted carbon fiber modified concrete under dynamic impact load

In order to improve the shortcomings of carbon fiber, such as smooth surface, poor bonding with concrete matrix and easy to pull out under dynamic impact load, graphene oxide is grafted onto the surface of carbon fiber by chemical bonds to prepare graphene oxide grafted carbon fiber (CF-GO). The dynamic impact test on CF-GO modified concrete (CF-GOMC) is carried out by the split hopkinson pressure bar (SHPB) test system, and the mechanical properties and strain rate effect of CF-GOMC under dynamic impact loads are studied. The modification mechanism of CF-GO is analyzed by microscopic tests. The results show that compared with carbon fiber, the surface roughness and surface area of CF-GO increase and CF-GO is more suitable for bonding with concrete matrix. CF-GO can improve the mechanical properties of concrete under dynamic impact load and enhance the strain rate effect of dynamic mechanical properties indicators by preventing crack, bridging, filling and promoting hydration. With the increase of CF-GO content, the dynamic mechanical properties and strain rate sensitivity of CF-GOMC increase first and then decrease. The optimal content of CF-GO is 0.3 %. The improvement effect of CF-GO on the dynamic mechanical properties and strain rate effect of concrete is better than that of carbon fiber. The graphene oxide on the surface of CF-GO makes the interface of CF-GO/concrete matrix compact by improving the mechanical bite force of fiber/concrete matrix and promoting the formation of hydration products on the surface of fiber. The addition of CF-GO does not change the composition of cement hydration products, but promotes the crystal growth of hydration products and optimizes the pore structure of concrete.

A robust, durable and eco-friendly UV-cured wood film with self-matting and anti-fingerprint performance via wrinkled structure

With the changes in people's living standards and aesthetic perspectives, the matting films with wrinkled surfaces play a crucial role in fields such as decorative materials, wooden furniture, wood-based panels and industrial coatings. In this paper, the UV-cured polyurethane acrylate (PUA) films with self-matting and anti-fingerprint performance on the wood-based panels was prepared and developed the wrinkled surface by using excimer/mercury dual UV curing. The results showed that the roughness, wavelengths (λ) and amplitudes (A) of wrinkles surface were positively correlated with the excimer irradiation time and negatively correlated with the mercury lamp irradiation time. Furthermore, the increasing irradiation time improved the degree of curing and crosslink density of the cured films, which enhanced the mechanical properties and durability of the cured film. Consequently, the prepared UV-cured PUA film exhibited excellent self-matting with a gloss of 3.4 GU at an incident angle of 60° and maintained the gloss value < 5 GU after 500 times rubs and 1 hour corrosion. Additionally, the self-matting films with wrinkled surface enhanced the hydrophobicity and anti-fingerprint performance of the surface. Besides, the cured film presented high physical performance with hardness of 4 H and adhesion of 0 grade. These results provide a reference for the further application of self-matting films in wood-based panels, furniture and interior decoration fields.

Evaporation of a water droplet on composite materials Cu-SiC, Cu/G and alloy AlMg3: Modeling the wettability of a metal-matrix composite with MDS

Composite materials are widely used in technology. The choice of exact composite material depends on its purpose, functional properties, stability of parameters over time, and specific conditions of use. In this work, the wettability of various materials was studied. The materials used were processed in two ways: polishing and laser texturing with and without craters. The surface wettability using molecular dynamics methods was modeled when changing the concentration of the reinforcing component in the composite. The crystalline grain orientation and surface roughness of the Cu-SiC composite after texturing is different from Cu, which is important to consider when modeling the wettability. The sensitivity of the wettability of various materials to the surface temperature (Δθ0/ΔTw) was studied experimentally. The maximum sensitivity of the contact angle to temperature was found for the superhydrophobic surface. The minimum sensitivity was observed for polished AlMg3 surface. Power-law dependences of the evaporation rate of water droplet on the contact angle were obtained for various materials in the temperature range of 25–90 °С. As the droplet diameter increases, the influence of the wetting diameter on the evaporation rate decreases, while that of convection increases. The data obtained can be useful for the development of composite materials technologies and optimization of their functional properties.

Effect of the conventional shot peening and multiple shot peening on microstructure and residual stress of TC17 titanium alloy

This study examines the residual stress, microstructure, and stress-induced phase transformation of TC17 titanium alloy after different shot peening processes. A comprehensive analysis of the unique impact of shot peening on α-Ti and β-Ti was performed. The results indicate a substantial reduction in the grain size of the deformed layer and the creation of a high density of dislocations. Additionally, increased peening intensity results in decreased grain size, and multiple shot peening promotes further reduction in grain size. Compressive residual stresses were detected in the deformed layer, and multiple shot peening significantly augmented the residual stresses in the surface and near-surface regions. In particular, the highest compressive residual stresses after triple shot peening treatments were measured at −1079 MPa (at a depth of 10 μm for α-Ti) and −792 MPa (at a depth of 50 μm for β-Ti). In addition, multiple shot peening can significantly reduce surface roughness and enhance surface nanocrystallization when approximate surface residual stresses are obtained. Remarkably, the use of single shot peening revealed parallel stacking faults in certain α-Ti samples. However, under multiple shot peening, these stacking faults evolved into face-centered cubic Ti (FCC-Ti) with broader widths and a greater number. The stress-induced phase transition orientation relation was determined to be (0001)HCP//(11¯1)FCC and [21¯1¯0]HCP//[011]FCC, with α-Ti grains being interspersed with FCC-Ti, thus promoting additional grain refinement.

Rare earth oxide nanoparticles for superhydrophobic, antifouling and self-cleaning coatings

The widely used rare earth oxides (REOs) have a limited application in antifouling coatings. Here, coatings composited with REOs-1H,1H,2H,2H-perfluorodecytrimeth-oxysilane (REOs-FAS) based on hydrothermal reaction were prepared for study if REOs can be used in marine antifouling coatings. A network consisting of polydimethylsiloxane (PDMS) and REOs-FAS (REOs-FAS/PDMS) (RE = Ce, Pr, Nd) was created by using the blending method and polymerization reaction. The presence of the REOs-FAS imparts to the polymers an amphiphobic structure and disrupts the cell membrane, resulting in excellent antifouling properties and antibacterial performance. The water, coffee, and soya-bean milk droplet state on the Pr6O11-FAS/Sylgard 184 silicone elastomer with the ratio of 4:1 (PFSR-4) and the ink self-cleaning experiment demonstrated that the PFSR-4 has a perfect self-cleaning property. The most suitable surface roughness of PFSR-4 not only empowered the superhydrophobic (the contact angle of water is as high as 157° ± 2° and the sliding angle of water is as low as 5° ± 2°)-oleophobic characteristic (the contact angle of diiodomethane is as high as 132° ± 3°), but also endowed the coating with the anti-diatom (as high as 97.7 %) and anti-mussel adhesive properties. Moreover, the colored PFSR coatings were prepared to do another barrier for the adhesion of large fouling organisms, especially for the white coatings. The anti-mussel attachment ratio of purely whited PDMS was high to 84.6 %. The antibacterial REOs are appropriate for preparing multi-functional coatings. In general, the designed coating has the potential to be a durable, self-cleaning, antibacterial, and antifouling coating and could serve as a foundation for developing innovative super-amphiphobic coatings.

Visible light-driven Synergetic antimicrobial activity of Cu2O quantum dots and electrospun PAN/PCL nanofiber matrix

This work reported a successful observation of the synergistic rapid antibacterial activity of the Electrospun PAN/PCL Nanofiber (NF) with Cuprous Oxide -based Quantum Dots (QDs). Our findings reveal that the NF-QDs nanostructure exhibits excellent antibacterial activity that eliminated more than 98% of antimicrobial-resistant bacteria in 30 s under visible light. The characterization including X-ray diffraction (XRD), scanning electron microscopy (SEM), Transmission electron microscopy (TEM), UV–Vis spectrophotometer (UV–Vis), Fourier transform infrared spectroscopy (FTIR), atomic force microscopy (AFM), Brunauer-Emmet-Teller (BET) analysis exhibits good physicochemical properties of both synthesized quantum dots and nanofiber. A desired hydrophobic NF with an average surface roughness of 219.40 nm and 243.46 nm for NF–Cu2O and NF–Cu2O/TiO2 was achieved with an average diameter of 502.54 nm and 343.02 nm, respectively. The antibacterial activity was tested against antibiotics-resistance strains, Klebsiella pneumoniae and Methicillin-resistant Staphylococcus aureus, as well as non-resistance strains, Escherichia coli and Staphylococcus aureus. Our results indicate the promising potential of NF-QDs as antibacterial fabric to halt antibiotic resistance infections and mitigate outbreaks in various sectors.

Effect of oxygen doping on cutting performance of CVD diamond coated milling cutters in zirconia ceramics machining

Diamond thin films were deposited on WC-Co tools using the hot-filament chemical vapor deposition (HFCVD) technique at varying pressures and oxygen doping levels. As the oxygen doping content increased, the purity of the diamond phase improved, and the density of the <111> crystal plane on the film's surface increased. The growth rate of diamond films initially increased and then decreased under low pressure, with a corresponding decrease in residual compressive stress. Conversely, at high pressure, increased oxygen doping enhanced the diamond phase purity and growth rate while reducing residual compressive stress. Cutting experiments on pre-sintered zirconia ceramics for milling linear slots and engraving dentures demonstrated that diamond-coated milling cutters exhibited superior cutting performance under consistent oxygen and carbon source concentrations and stable air pressure conditions. The oxygen-doped diamond-coated milling cutter grown at a pressure of 1 KPa exhibited the longest service life, attributed to its reduced surface roughness, lower cutting force, and increased density of the <111> crystal plane orientation. This cutter could machine up to 1300 crowns, making it approximately 80% more durable than non‑oxygen-doped diamond-coated milling cutters and about 20 times more durable than uncoated ones.

Comparison of the efficacy of Er,Cr:YSGG laser on oral biofilm removal from implant surfaces with various application times for the treatment of peri-implantitis defects: ex vivo study

PurposeThe major struggle in peri-implantitis therapy is the availability of successful decontamination of the infected implant surface. The main hypothesis of this study was the Er,Cr: YSGG laser decontamination efficacy investigation on the infected implant surfaces with various peri-implantitis defects. The primary objective of this study was to decide the efficacy of Er,Cr:YSGG laser as a decontamination tool at various peri-implantitis simulating defects. The secondary objective was to compare the efficacy of the Er,Cr: YSGG laser on oral biofilm removal between two protocols the first protocol (4 cycles at 2.5 min) and the second protocol (5 cycles at 5 min) at various peri-implantitis simulating defects.Materials and methodsA total of 3 subjects whose plaque biofilms formed in-vivo on twenty-four tested implants were divided into four tested groups. Two native implants were tested as controls.The in vitro defect model was computer‐aided designed and printed into a 3D-printed model with various anulations in peri-implant infrabony defects, which were 15,30,60,and 90 degrees.ResultsBoth Er, Cr: YSGG decontamination protocols at 50 mJ (1.5 W/30 Hz), 50% air, and 40% water were effective at reducing the total implant surface area/ biofilm ratio (%), but the second protocol had a markedly greater reduction in the duration of application (5 cycles at 5 min) than did the first protocol (4 cycles at 2.5 min).ConclusionThe Er, Cr: YSGG laser is an effective decontamination device in various peri-implantitis defects. The second protocol(5 cycles at 5 min) with greater application time and circles is more effective than the first one. The defect angulation influence the decontamination capability in peri-implantitis therapy.Clinical relevance (Scientific rationale for study)Clinicians anticipate that the exploration of suitable therapeutic modalities for peri-implantitis therapy is limited by the obvious heterogeneity of the available evidence in the literature and need for a pre-clinical theoretical basis setup. The major challenges associated with peri-implantitis therapy include the successful decontamination of the infected implant surface, the absence of any damage to the treated implant surface with adequate surface roughness, and the biocompatibility of the implant surface, which allows osteoblastic cells to grow on the treated surface and is the key for successful re-osseointegration. Therefore, these are the expected empirical triads that need to be respected for successful peri-implantitis therapy. Failure of one of the triads represents a peri-implantitis therapeutic failure. The Er, Cr: YSGG laser is regarded as one of the expected devices for achieving the required triad.Trial registration"Efficacy of Er,Cr YSGG Laser in Treatment of Peri-implantitis". ClinicalTrials.gov ID NCT05137821. First Posted date: 30 -11–2021.

Biomechanical surface roughness analysis of ramie-low melt polyester nonwovens exposed to plasma

Biomechanical surface roughness analysis of ramie-low melt polyester nonwovens exposed to plasma

Physicochemical and bioactive characterization of pink guava pulp microcapsules prepared by freeze-drying using coffee mucilage as a wall material

This study investigated the potential of coffee mucilage (CM), a readily available coffee industry byproduct, as a wall material for the microencapsulation of pink guava pulp via freeze-drying (FD). Microcapsules with varying wall compositions incorporating powdered coffee mucilage, maltodextrin (MD), or a combination of both (FD-CM/MD) were developed and characterized using techniques such as FT-IR spectroscopy, SEM, TGA/DSC, and zeta potential analysis. The retention of bioactive compounds was assessed using total phenolic content, antioxidant capacity and carotenoid analyses. Results revealed that the incorporation of powdered coffee mucilage significantly influenced the physicochemical properties of the microcapsules, resulting in larger particle sizes and less rough surface morphologies compared with maltodextrin-based formulations. Notably, FD-CM microcapsules exhibited a thermal stability (Tg ≈ 50 °C) and retention total polyphenols of 30.19 ± 5.26 mg GAE/g dry weight (DW) and carotenoids of 5.50 ± 0.29 mg β-carotene/100 g DW, which can be attributed to the protective effects and inherent antioxidant capacity of 91.85 ± 9.93 μmol Trolox Equivalents/g DW in the coffee mucilage matrix. While influencing the color attributes, all microcapsule formulations retained a commercially appealing (hab = 79.80 ± 0.06) red-yellow hue. This study demonstrated the potential of powdered coffee mucilage as a sustainable and effective encapsulating wall material for enhancing the stability and bioavailability of bioactive compounds in food products.

HYPREZ Wafering Solutions: A Novel Approach of SiC Wafering Solution

A novel approach for processing SiC wafers has been developed to grind then polish 150 and 200mm SiC wafers without lapping. The purpose of this work was to optimize the processing of SiC wafers sliced from boules to finished epi-ready wafers by grinding and chemical-mechanical polishing (CMP). Diamond vitrified wheels were used for coarse and fine grinding to correct the irregular shape of SiC wafers before reducing surface roughness by CMP. 4H-SiC wafers were sliced by diamond embedded/slurry wire saw and laser split techniques. Incoming wafer condition was seen to affect coarse grinding wheel performance depending on incoming surface roughness and shape. Wheel characteristics, including abrasive size, abrasive concentration, and bond structure, were adjusted to improve grinding efficiency based on incoming conditions. Coarse grinding wheels were able to reduce wafer total thickness variation to 3-5um and average surface roughness to 20-30nm (Ra). Fine grinding wheels were optimized to reduce total thickness variation (TTV) below 2um and surface roughness to 1-2nm Ra and peak-to-valley height of 20-30nm (Rt). Coarse and fine wafering time was less than 30 minutes total to remove 50 microns on both Si and C-face per wafer. Surface damage from grinding was removed after one hour of polishing each wafer by CMP, achieving surface roughness of 0.4nm Ra and 5-7nm Rt. The benefit of optimizing coarse and fine grinding of 150 and 200mm SiC wafers is demonstrated by producing flat wafers, which reduced overall processing time to prepare an epi-ready condition by CMP.

Understanding the Effect of Drilling Parameters on Hole Quality of Fiber-Reinforced Polymer Structures.

Hole quality in composite materials is gaining interest in aerospace, automotive, and marine industries, especially for structural applications. This paper aims to investigate the quality of holes performed without a backup plate, in thin plates of glass fiber-reinforced polymer (GFRP). The samples were manufactured by two different technologies: vacuum bagging and an innovative method named vacuum mold pressing. Three experiments were designed choosing the control factors that affect the maximum cutting force, delamination factor, and surface roughness of drilled holes in composite materials based on twill fabric layers. Quality analysis of the hole features was performed by microscopy investigations. The effects of the main factors on the targets are investigated using the statistical design of experiments, considering control factors, such as support opening width, weight fraction (wf), feed per tooth, and hole area. The results showed that the feed per tooth and hole area had a more significant influence on the delamination factors and surface roughness (Sa). The best quality of the holes drilled in twill-based GFRP was achieved for a lower feed rate of 0.04 mm/tooth and used a support opening width of 55 mm.