AbstractThe development of gauze ring random packing for laboratory scale fractionating columns is described. The packing consists of small open‐ended cylinders of wire gauze and the column is operated in such a manner that a thin film of liquid is maintained over the entire surface of these cylinders. This Aim is produced by flooding the packing before the start of a fractionation and a method of doing this is described. This packing shows a high fractionating efficiency, a fractionating performance of 84 theoretical plates per foot of height having been obtained with some columns. It has also a low hold‐up per theoretical plate and a low pressure drop. It may be used in place of other packings in existing columns.High efficiency fractionation has been developed in the Billingham laboratories of the Imperial Chemical Industries, Limited, primarily for the analysis of complex hydrocarbon mixtures. Before 1936, the most common random packings were glass and metal beads,1 Lessing rings of metal or ceramic materials,2 metal eyelets, carding teeth,3 and jack chain.4 The fractionating efficiency of these packings was low, being only equivalent to about four theoretical plates per foot of height.Notable increases in efficiency were later obtained by Fenske5 using single turn wire helices, by Stedman6 who used a regular packing in the form of conical wire gauzes and by Lecky and Ewell7 who produced a spiral packing made from wire gauze.It was found in these laboratories that the gauze packings of Stedman and Lecky and Ewell were difficult to construct, needed precision bore glass tubing to ensure high efficiency, and that a uniform flow of reflux over the gauze surface was not obtainable. To improve the liquid distribution copper gauze cylinders in the form of Lessing rings 1/8 in. × 1/8 in. were introduced into the empty spaces around the cones of the Stedman packing and a great improvement in efficiency was obtained. A further improvement was obtained by removing the gauze cones completely and replacing them with more gauze rings. Since this cylindrical packing was comparatively easy to manufacture and use, the development work on other packings was abandoned and from 1941 to 1943 a study was made of the variables affecting the performance of this packing. The results of this work are summarized in this paper. A mixture of 20% normal heptane and 80% methyl cyclohexane was used throughout for the determination of fractionating efficiency.