AbstractWood ash, a byproduct of wood combustion, poses environmental challenges when disposed of in landfills. This study explores a sustainable alternative by investigating the carbonation of wood ash, a process converting CO2 into stable carbonate minerals. With increasing concerns about waste management, this research aims to identify optimal carbonation conditions by varying relative humidity, liquid-to-solid ratio (L/S), and temperature. Results demonstrate that the ideal conditions for wood ash carbonation involve a moderate relative humidity of 55%, room temperature at 25 °C, and a lower L/S ratio. Thermogravimetric analysis (TGA) indicates that extended curing times increase CaCO3 formation. Scanning electron microscopy (SEM) and X-ray diffraction (XRD) confirm the presence of carbonate phases. Mechanical strength tests reveal that samples with lower porosity and higher carbonation products exhibit superior strength. This study contributes to the understanding of wood ash carbonation but also emphasizes its potential practical applications in construction materials as light aggregates in cement concrete. The research explores the implications for sustainable waste management, offering insights into environmentally and economically viable solutions for wood ash recycling.