This study reconstructs the paleoenvironmental and paleoclimate variabilities of the Paleogene-Quaternary River Niger Basin in Nigeria, West Africa, using integrated geochemical (XRF) and palynological proxies, with samples collected from three locations along a downstream gradient: JB (proximal to the Agbaja ironstone formation), AL (midstream), and JL (farthest downstream). Geochemical analysis reveals distinct trends influenced by the proximity to the Agbaja ironstone. JB sediment exhibits high Fe₂O₃ (20.538 wt.%) and MnO (0.425 wt.%) concentrations, reflecting localised ferruginous inputs and tropical weathering associated with the ironstone. Downstream, AL and JL show increasing SiO₂ content (63.546 wt.% in JB to 87.215 wt.% in JL), indicating progressive sediment dilution, greater contributions from quartz-rich sources, and prolonged transport. The palynological analysis identifies diverse microfossils, including Laevigatosporites sp., Retitricolporites irregularis, Diatom frustules, and Botryococcus braunii, providing insights into vegetation dynamics and hydrological fluctuations. Rainforest indicators, such as Sapotaceae and Proxapertites cursus, signify wetter interglacial periods, while grassland taxa like Monoporites annulatus and charred gramineae cuticles denote arid phases. Algal taxa (Pediastrum sp., Diatom frustules) reflect freshwater conditions, whereas mangrove-associated species (Acrostichum aureum, Echiperiporites sp.) highlight episodes of brackish influence during sea-level rises. This bi-proxy approach reveals alternating humid and arid phases influenced by Quaternary climate oscillations. These changes have affected vegetation cover, sediment transport, and depositional settings. The findings enhance our understanding of the paleoenvironmental evolution of West Africa, providing valuable context for regional climate models and sedimentary processes. This study makes a significant contribution to the findings on Quaternary climate variability and its impact on the ecological and geological history of the River Niger basin in Nigeria, West Africa.
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