Pull-out Tests Research Articles

Mechanical properties of sisal fiber-reinforced fly ash cement mortar activated by sodium sulfate

The substantial use of fly ash as cement replacement to reduce carbon emissions is identified as the primary goal, 50 % of the cement was substituted with fly ash and in order to avoid the low early stage mechanical properties of the composite, varying doses of sodium sulfate were used as an activator of fly ash. Additionally, sisal fibers were chosen to enhance the flexural strength. The results indicate that sodium sulfate significantly enhances the early stage mechanical performance of the cementitious composites and the matrix exhibits the optimal mechanical performance at 4 wt% sodium sulfate dosage (4SS). The addition of sisal fibers resulted in an enhancement of the flexural performance of the material. The collaboration between sodium sulfate and sisal fibers results in an improvement in the initial flexural performance of the material while preserving its compressive strength. The single-fiber pullout test further confirmed that adding sodium sulfate enhances the fiber-matrix interface and bonding. Microstructural investigations by XRD, TGA, MIP, and SEM-EDS revealed accelerated hydration and early formation of a large amount of ettringite due to the addition of sodium sulfate. Ettringite acts as a gel nucleation seed, promoting the formation of a dense gel structure and effectively improving the early mechanical properties of the composite. Furthermore, with curing age, sodium sulfate also effectively improves the pore structure of the matrix in the late hydration stage.

Elevating mechanical performance of cementitious composites with surface-modified 3D-Printed polymeric reinforcements

3D printed polymeric reinforcement has been found able to improve the ductility of cementitious materials. However, due to the hydrophobic nature of commonly used 3D printing polymers, the bonding strength between the 3D printed polymers and cementitious matrix is extremely weak, which potentially hinders the mechanical performance of the reinforced composites. This work aims to improve the bonding properties by applying surface modifications on the 3D printed reinforcement, and eventually enhance the mechanical performance of the reinforced cementitious composites. Three types of surface coatings ingredients: epoxy resin (EP), sand sprinkled epoxy (SA) and short steel fibers sprinkled epoxy (SF) were used. Pull-out experiments are performed to study the bonding properties of the 3D printed reinforcement with different coatings. Then, uniaxial tensile and four-point-bending experiments are used to investigate the mechanical performance of the reinforced cementitious composites. A lattice type numerical model is applied to simulate the pull-out and tensile tests. The pull-out experiments indicate that the SA and SF reinforcement achieved approximately two times higher bonding strength than the uncoated and EP reinforcement. The tensile and flexural results suggest that the cementitious composites with SA and SF reinforcement achieved significantly better ductility (manifested by strain-hardening and deflection-hardening behavior) than the composites with uncoated and EP reinforcement. The numerical simulation results highly agree with the experimental findings, and further confirmed that the improved reinforcement-mortar bonding strength is the determinative factor that enhanced the composites mechanical performance. The findings of this work suggest that the sand and steel fiber surface coatings can effectively enhance the ductility of cementitious composites reinforced by 3D printed polymers.

Prediction model for the bond behaviour of low-corrosion reinforced concrete considering corrosion time variability

Corrosion greatly affects the bond behaviour of reinforced concrete. In the case of reinforcing low-corrosion reinforced concrete, the bond strength of steel bars and concrete is at an enhanced stage. Accurate prediction of bond behaviour at this stage is crucial for the rational reinforcement. This study designed ten groups, totalling 30 pull-out specimens, were accelerated corroded with various current densities and electrification times. Through 3D scanning and image analysis technology, we observed that increasing the current density yielded less homogeneous corrosion, creating pit-like rust marks. Meanwhile, we developed a model for predicting the corrosion level. The model is applicable to the corrosion level design of accelerated corrosion. Pull-out tests showed that as corrosion increased, the specimen failure mode changed from pull-out to splitting and back to pull-out, with the bond strength first increasing and then decreasing. A bond-slip prediction model for corroded reinforced concrete was also established, considering the effects of corrosion on bond strength in different stages, especially the enhancement stage. The model performs well in predicting the bond behaviour of low-corrosion reinforced concrete and can be used in conjunction with corrosion prediction models and provides guidance for reinforcement.

Multi-scale experimental investigation on the structural behaviour of novel nanocomposite/natural textile-reinforced mortars

Natural fibre composites present a very appealing area of research for the structural strengthening of masonry structures. Natural fibres possess several drawbacks, such as low initial stiffness and poor interfacial bond behaviour with inorganic matrices that hinder their functions. Such challenges were overcome by applying an innovative nanocomposite-based impregnation system that was pre-engineered and presented by the authors previously. In this paper, a full experimental study involving pullout, tensile tests and large-scale testing via diagonal compression test was carried out to evaluate the structural efficiency of the developed system. Remarkable improvement at yarn-to-matrix level upon nanocomposite coating was observed. At a medium bond length, yarn rupture was observed, highlighting the great anchorage provided by the nanocomposite coating within the matrix. Coupons cast with the developed system demonstrated outstanding composite behaviour and multicracking under tensile loading. Finally, wallets strengthened with the developed system displayed multiple cracks and maintained high shear capacity (40–60 % of τmax) at remarkably large displacements developed at later stages of the test. Such ductility is crucial for retrofitting masonry structures, especially in seismic areas.

Effect of fit and self-etching adhesive on fiber post retention in endodontically treated teeth.

Fiber post (FP) reinforced restoration was widespread in endodontically treated teeth, of which the retention was closely related to fit and operation process. However, the question whether the fit and self-etching adhesive (SED) affect the success of FP restoration still remained unclear. This research aimed to assess how the fit and self-etching adhesive (SED) impact the pull-out bond strength (BS) of glass fiber-reinforced composite posts from the root canal dentin. Eighty lower first premolars underwent simulated endodontic treatment, after which their canals were shaped to accommodate a size three RelyX fiber post (FP) (diameter 1.9 mm). They were then divided into 4 equal groups [Unfit post and no SEA (Group UN), Fit post and no SEA (Group FN), Unfit post with SEA (Group UA) and Fit post with SEA (Group FA)] using two different sized FPs and SEA. Cement thickness was acquired by histological analysis and stereomicroscopy. Each sample was tested for pull-out strength through a universal testing machine. Based on the pull-out test, the failure types were observed and scored by visualizing through a stereomicroscope. Group FA demonstrated significantly greater BS compared to Group UN and Group UA, with Group UN showing a statistically significant difference at p< 0.01 and Group UA at p< 0.05. Main failure types in Group FA were Type II, which illustrated that the cement detachment mainly occurred from the post-cement interface. Therefore, Group FA possessed the STRONGEST BS and was most suitable for FP-reinforced crown restorations. Both the fit and SEA enhanced the pull-out BS. The SEA was critical for BS promotion when the mechanical retention was inadequate.

Modelling the ultimate pullout resistance of geogrids

This paper provides a review of the modelling of geogrid ultimate pullout resistance. Several analytical models were found to disregard the effect of the geogrid stiffness as well as the particle size distribution of the soil. A sensitivity analysis was done on 289 pullout tests to evaluate the significance of these omitted variables as well as other key variables contributing to pullout resistance. It was found that ultimate pullout resistance was the most sensitive to normal stress followed by geogrid length, geogrid stiffness and the friction angle of the soil. By considering geogrid geometry, stiffness and soil grading descriptors, in addition to the standard variables of length, stress and friction angle, regression models of ultimate pullout capacity improved by 15%. In addition, an alternative model to the simplified linear models of FHWA and EBGEO which maintains dimensional consistency while incorporating geogrid stiffness and non-linearity in the model, was proposed. This alternative model performed 32% better than the simplified linear models.

A Revised Abaqus® Procedure for Fracture Path Simulation Based on the Material Effort Criterion.

This paper presents the results of computer simulations of fracture in three laboratory tests: the three-point bending of a notched beam cut from sandstone, the pull-out test of a self-undercutting anchor fixed in sandstone, and the pull-out test of a bar embedded in concrete. Five material failure criteria were used: Rankine, Coulomb-Mohr, Drucker-Prager, Ottosen-Podgórski, and Hoek-Brown. These criteria were implemented in the Abaqus® FEA system to work with the crack propagation modeling method-extended finite element method (X-FEM). All criteria yielded similar force-displacement relationships and similar crack path shapes. The improved procedure gives significantly better, close-to-real crack propagation paths than can be obtained using the standard subroutines built into the Abaqus® system.

Improving clay-geogrid interaction: Enhancing pullout resistance with recycled concrete aggregate encapsulation

In this study, Recycled Concrete Aggregate (RCA) was employed as a sandwich technique around the geogrid to enhance the pullout resistance of the geogrid in clayey backfills. Large-scale pullout tests were conducted on three configurations: geogrid-reinforced clay, geogrid-reinforced RCA, and geogrid sandwiched between layers of RCA, aimed at investigating pullout resistance and deformation. The experiments encompassed two different geogrid types (designated as G1 and G2), varying normal pressures ranging from 10 to 50 kPa, and RCA layers with thicknesses of 40, 80, 160, and 320 mm. Results from the experiments revealed that the inclusion of RCA layers around the geogrid substantially enhanced pullout resistance, with improvements ranging from 1.5 to 3 times compared to clay specimens. Optimal RCA thicknesses were determined in order to enhance soil-geogrid bonding and pullout resistance. For G1 geogrid, a thickness of 160 mm (equivalent to replacing 25% of clay volume with RCA) was identified as optimal, while for G2 geogrid, an 80 mm thickness (equivalent to replacing 15% of clay volume with RCA) was found to be sufficient. These thicknesses were established to achieve over 80% of the pullout force compared to full RCA specimens.

Structural, mechanical and in vitro studies on pulsed laser deposition of hydroxyapatite on additive manufactured polyamide substrate

Additive manufacturing (AM) is an emerging field that merges engineering and life sciences to produce components that can effectively act as a replacement in the human body. This AM encompasses biofabrication using cells, biological or biomaterials as building blocks to fabricate biological and bio-application oriented substance, device and therapeutic products through a broad range of engineering and biological processes. Furthermore, bioactive coating on BAM surface facilitates biological fixation between the prosthesis and the hard tissue which increases the long term stability and integrity of the implant. In this paper, hydroxyapatite (HA) powder was coated over AM polyamide substrate using pulsed laser deposition. Coating morphology was characterised using scanning electron microscope (SEM) analysis and observed that the coating was dominated by the presence of particle droplet with different sizes. Compounds like tricalcium phosphate and a few amorphous calcium phosphates were found along with HA which was confirmed by X-ray diffraction (XRD) analysis. Fourier transform infrared spectroscopy (FTIR) techniques shows the presence of phosphate and carbonate groups in the HA structure. Nano-indentation and pull-out test reveals that the layer was strong enough and withstands higher load before it peels off. In vitro analysis was evaluated with human osteosarcoma MG-63 cells with respect to the cell viability and results shows that the good viability was observed on coated surface due to combinational effect of Ca2+ and PO4 3&amp;minus; ions. The multitude of characterisation conducted on the coating has established that coating polyamide with HA results in a positive combination for an implant.

Upper and Lower Bounds to Pull-Out Loading of Inclined Hooked End Steel Fibres Embedded in Concrete

Steel fibre-reinforced concrete (SFRC) consists of short, hooked steel fibres that are randomly distributed and oriented within the cementitious matrix. This paper presents a new analytical load-bounding approach that captures the tensile response of misaligned fibres embedded in the matrix. The contribution of fibres in bridging cracks to provide the required stress transfer relies on the orientation of the fibres in the concrete. Bridging fibres aligned with a crack are less effective than those inclined to it. Therefore, understanding the pull-out behaviour of misaligned fibres is a key factor in quantifying and optimising the design of SFRC in structural applications. In the laboratory, a single-oriented fibre embedded in a solid cylinder of concrete was subjected to a pull-out test, where the axis of the tensile force is aligned with the axis of the cylinder. Based on the observed behaviour, this paper presents a new analytical bounding approach to capture the pull-out response of misaligned hooked-end steel fibres embedded in a concrete matrix. The analysis was based on a transversely isotropic failure criterion assumed for the plasticity that occurs in the cold-drawn fibre. Lower and upper bounds to the loading failure were derived from fibre pull-out and fibre fracture, respectively. The division between bounds depended upon the fibre orientation, fibre diameter and the combined strengths of the steel and concrete. Bounding predictions were drawn from ratios between a fibre’s shear strength and its transverse and axial uniaxial strengths, as found from a novel testing proposal. The two bounds were compared with new data and other experimental results published in the literature. The results showed that the region between the bounds captured the failure loads of embedded fibres with effective load-bearing orientations. A critical orientation was observed at maximum strength. The present interpretation of the plasticity occurring within off-axis, hooked-end steel fibres suggests that it is possible to optimise the strength of concrete using this method of reinforcement.

Predicting axial-bearing capacity of fully grouted rock bolting systems by applying an ensemble system

In this paper, the potential of the five latest artificial intelligence (AI) predictive techniques, namely multiple linear regression (MLR), multi-layer perceptron neural network (MLPNN), Bayesian regularized neural network (BRNN), generalized feed-forward neural networks (GFFNN), extreme gradient boosting (XGBoost), and their ensemble soft computing models were evaluated to predict of the maximum peak load (PL) and displacement (DP) values resulting from pull-out tests. For this, 34 samples of the fully cementitious grouted rock bolts were prepared and cast. After conducting pull-out tests and building a dataset, twenty-four tests were randomly considered as a training dataset, and the remaining measurements were chosen to test the models’ performance. The input parameters were water-to-grout ratio (%) and curing time (day), while peak loads and displacement values were the outputs. The results revealed that the ensemble XGBoost model was superior to the other models. It was because having higher values of R2 (0.989, 0.979) and VAF (99.473, 98.658) and lower values of RMSE (0.0201, 0.0435) were achieved for testing the dataset of PL and DP’ values, respectively. Besides, sensitivity analysis proved that curing time was the most influential parameter in estimating values of peak loads and displacements. Also, the results confirmed that the ensemble XGBoost method was positioned to predict the axial-bearing capacity of the fully cementitious grouted rock bolting system with extreme performance and accuracy. Eventually, the results of the ensemble XGBoost modeling technique suggested that this novel model was more economical, less time-consuming, and less complicated than laboratory activities.

Pullout behavior of polyethylene fiber from cement matrix: Effect of embedment length, matrix strength, and inclination angle

Engineered cementitious composites reinforced with polyethylene fibers (PE-ECC) exhibit the potential for high strength and toughness. To optimize the performance and tailor the properties of PE-ECC, this study focuses on analyzing the pullout behavior of polyethylene (PE) fibers from matrices through single fiber pullout tests and scanning electron microscopy analysis. One fiber type was used throughout the experiment, while three embedment lengths and three inclination angles were considered to investigate the pullout behavior from high-strength matrices. Furthermore, the pullout response from matrices with middle and low strength was examined, considering two embedment lengths. The results indicate that fibers with shorter embedment lengths exhibit lower pullout loads but higher energy absorption capacities. High matrix strength enhances adhesion and friction at the fiber-matrix interface, resulting in plumper pullout load versus slip curves. Owing to snubbing and matrix spalling effects, as the inclination angle increases, both the peak load and slip at the peak load of the inclined fibers exhibit an exponential increasing trend. Additionally, following the peak load, the pullout load of inclined fibers decreases more gradually than that of aligned fibers, and the energy absorption capacity of inclined fibers is significantly improved. Ultimately, general equations are derived for the calculation of pullout work and equivalent bond strength.

Comparative Analysis of Internal Tapered Implant-Abutment Connections: Evaluating the Morse Effect.

The purpose of the present study was to evaluate the Morse effect of different internal tapered implant-abutment connections (ITCs) using a pullout test. Implants with different ITCs were selected: Short (Bicon, USA), G1; Novo Colosso (Medens, Brazil), G2; Epkut (SIN, Brazil), G3; Strong SW (SIN, Brazil), G4; Flash (Conexão, Brazil), G5 and Bone Level (Straumann, Switzerland), G6. The respective computer-aided design (CAD) files were loaded into the analysis software to measure each ITC's taper angle and implant-abutment contact area. Six implants from each group were embedded in acrylic resin blocks, and the respective universal abutments were fixed using a mallet (G1) or by applying 20 Ncm of torque (G2 to G6). After 10 minutes, each abutment's retention screw was removed, and the force necessary for abutment rupture was recorded using a universal testing machine at a crosshead speed of 0.5 mm/min. The groups were compared using a one-way analysis of variance and Tukey's test. Spearman's correlation was used to check the correlation of the taper angle and contacting area with the pullout strength. G1, a no-screw abutment with a 3° taper, and G2, a 10° tapered abutment tightened by 20 Ncm, presented the highest pullout strength (P < .05). The increased taper angle of G4, compared to G3, reduced the Morse effect despite their similar implant-abutment contacting areas (P < .05). The G5 and G6 abutments loosened after screw removal and did not exhibit pullout resistance. The closer the tapered angle (r = -.958) and the higher the implant-abutment contact area (r = .880), the higher the pullout strength (P < .001). Within the limits of this study, the Morse effect is different among tapered implant-abutment connections. The closer the tapered angle and the higher the interface area, the higher the Morse effect between the abutment and the implant.

Effect of repeated steam sterilizations on insertional torque, torque to failure, and axial pullout strength of 3.5-mm and 2.0-mm cortical bone screws.

The objective of this study was to determine the effects of repeated steam sterilization cycles on the biomechanical properties of surgical screws. 42 3.5-mm and 42 2.0-mm self-tapping, cortical screws were divided into 3 groups per size and underwent autoclave sterilization for 1 (G1), 50 (G50), or 100 (G100) cycles and testing from August 2018 through June 2021. Sixty screws were then inserted into canine cadaver femurs, and biomechanical properties were measured, including peak insertional torque, torque to failure, and pullout strength, each normalized to cortical thickness. Scanning electron micrographs were taken from 24 screws, and images were blindly analyzed by 5 trained examiners. The mean normalized insertion torque for 3.5-mm screws was significantly different between G1 and both G50 and G100. The mean normalized torque to failure for 3.5-mm screws was significantly different between G1 and both G50 and G100. Axial pullout testing was found to be significantly different for 2.0-mm screws between G1 and G100. Scanning electron micrographs surface scoring identified a significant difference in 3.5-mm screws at the screw tip. The results indicate that biomechanical changes occur with repeated steam sterilizations. Specifically, peak insertional torque and torque to failure are decreased with increased sterilizations for 3.5-mm screws, whereas 2.0-mm screws were altered in pullout testing after 100 sterilizations. It is suspected that numerous sterilizations negatively alter the physical-mechanical properties of certain screw sizes. The biomechanical properties of the bone-implant interface could negatively be affected by multiple steam sterilizations during clinical setting.

Impact of screw tip design on screw anchorage: mechanical testing and numerical simulation

BackgroundScrew loosening is a commonly reported issue following spinal screw fixation and can lead to various complications. The initial cause of screw loosening is biomechanical deterioration. Previous studies have demonstrated that modifications in screw design can impact the local biomechanical environment, specifically the stress distribution on bone-screw interfaces. There are several different designs of screw tips available for clinically used pedicle screws; however, it remains unclear whether these variations affect the local stress distribution and subsequent screw anchorage ability.MethodsThis study conducted comprehensive biomechanical research using polyurethane foam mechanical tests and corresponding numerical simulations to investigate this topic. Models of pedicle screw-fixed osteoporotic polyurethane foam were created with two different clinically used screw tip designs (flat and steep) featuring varying tip lengths, taper angles, and diameters, as well as identical flank overlap areas and thread designs. The anchorage ability of the different models was assessed through toggle and pull-out test. Additionally, numerical mechanical models were utilized to compute the stress distributions at the screw and bone-screw interfaces in the different models.ResultsMechanical tests revealed superior anchorage ability in models utilizing flat-tipped screws. Furthermore, numerical modeling indicated improved anchorage ability and reduced stress concentration tendency in these models.ConclusionChanges in screw tip design can significantly impact the biomechanical anchoring capability of screws. Specifically, flatter tip pedicle screws may mitigate the risk of screw loosening by alleviating stress concentration on bone-screw interfaces.

A stacking machine learning model for predicting pullout capacity of small ground anchors

Small ground anchors are widely used to fix securing tents in disaster relief efforts. Given the urgent nature of rescue operations, it is crucial to obtain prompt and accurate estimations of their pullout capacity. In this study, a stacking machine learning (ML) model is developed for the rapid estimation of pullout capacity offered by small ground anchors used for temporary tents, leveraging cone penetration data. The proposed stacking model incorporates three ML algorithms as the base regression models: K-nearest neighbors (KNN), support vector regression (SVR), and extreme gradient boosting (XGBoost). A dataset comprising 119 in-situ anchor pullout tests, where the cone penetration data were measured, is utilized to train and assess the stacking model performance. Three metrics, i.e., coefficient of determination (R2), mean absolute error (MAE), and root mean square error (RMSE), are employed to evaluate the predictive accuracy of the proposed model and compare its performance against four popular ML models and an empirical formula to highlight the advantages of the proposed stacking approach. The results affirm that the proposed stacking model outperforms other ML models and the empirical approach as achieving higher R2 and lower MAE and RMSE and more predicted data points falling within 20% error line. Thus, the proposed stacking model holds promising potential as a solution for efficiently predicting the pullout capacity of small ground anchors.

Photon-Induced Photo-Acoustic Streaming vs. Shock Wave-Enhanced Emission Photo-Acoustic Streaming-The Effect of Three Final Irrigation Protocols on the Bond Strength of an Individually Formed Fiber Post.

(1) Background: This study aimed to evaluate how laser-activated irrigation (LAI) influences the retention of a fiber post when used before an endodontic filling, as well as after post space preparation. (2) Materials and Methods: Sixty freshly extracted human incisors were selected. The teeth were randomly assigned to three groups-CONVENTIONAL (CONV), PIPS or SWEEPS-and treated endodontically. Each group received irrigation with 1 × 5 mL EDTA (17%) and 3 × 5 mL NaOCl (5.25%). In the first group, the irrigants were not activated, while in the second and third group, LAI was adopted using PIPS and SWEEPS protocols (Lightwalker from Fotona, Ljubliana, Slovenia). After post space preparation, each group received the same irrigation protocol initially established. Sticky posts (everStick Post, GC AUSTRIA GmbH Swiss) were individually adapted to the corresponding post spaces and cemented using dual cure resin cement (Gradia Core, GC Austria GmbH Swiss). All specimens were vertically embedded into self-curing acrylate (Duracryl plus, Spofa Dent, Europe), and each was sectioned into three segments of type A and type B samples for debonding through push-out and pull-out tests. The results were statistically analyzed. (3) Results: The pull-out test showed the superiority of the SWEEPS group, with a mean fracture force of 133.0 ± 50.7 N, followed by the PIPS group, with 102 N, with a lower standard deviation of ± 34.5 N. The CONV group registered the lowest fracture force. Concerning the push-out test, the SWEEPS group showed superior shear stress in comparison to the other two groups (13.45 ± 4.29 MPa); the CONV group was inferior, with shear tension values of 8.31 ± 4.67 MPa. (4) Conclusions: It can be stated that the SWEEPS and PIPS protocols resulted in considerably higher fiber post retention than the conventional method, whereas the SWEEPS protocol was superior to the PIPS protocol.

Transient mode-III problem of the elastic matrix with a line inclusion

The method of pull-out test has been used to identify the mechanical performance of hybrid and fiber-reinforced composite materials. This paper investigates the elastic phase preceding the pull-out of a rigid line inclusion from the polymer matrix with fixed top and bottom surfaces. The mode-III problem is investigated such that the pull-out force is applied from the out-of-plane direction and it can be either transient or static. By applying the singular integral equation technique, the semi-analytical elastic field expressions are obtained. Under the static pull-out force, the stress intensity factor (SIF) near the inclusion tip shows a monotonic increase as the length and height of the matrix increase, whereas for the transient pull-out force, the SIF displays an initial increasing and followed by a decline. The maximum SIF is obtained for (1) the matrix length is 2 to 2.5 times of the inclusion length, and (2) the matrix height is 1 to 2 times of the inclusion length. Moreover, this paper provides a solution approach that incorporates the elasticity of the inclusion, showing that there is an optimal shear stiffness that minimizes the stress singularity of system. The conclusions of this study hold significance for the design and performance evaluation of fiber-reinforced composite materials.

Functional post-processing of extrusion-based 3D printed parts: polyaniline (PAni) as a coating for thermoplastics components

PurposeThis study aims to evaluate in situ oxidative polymerization of aniline (Ani) as a post-processing method to promote extrusion-based 3D printed parts, made from insulating polymers, to components with functional properties, including electrical conductivity and chemical sensitivity.Design/methodology/approachExtrusion-based 3D printed parts of polyethylene terephthalate modified with glycol (PETG) and polypropylene (PP) were coated in an aqueous acid solution via in situ oxidative polymerization of Ani. First, the feedstocks were characterized. Densely printed samples were then used to assess the adhesion of polyaniline (PAni) and electrical conductivity on printed parts. The best feedstock candidate for PAni coating was selected for further analysis. Last, a Taguchi methodology was used to evaluate the influence of printing parameters on the coating of porous samples. Analysis of variance and Tukey post hoc test were used to identify the best levels for each parameter.FindingsColorimetry measurements showed significant color shifts in PP samples and no shifts in PETG samples upon pullout testing. The incorporation of PAni content and electrical conductivity were, respectively, 41% and 571% higher for PETG in comparison to PP. Upon coating, the surface energy of both materials decreased. Additionally, the dynamic mechanical analysis test showed minimal influence of PAni over the dynamic mechanical properties of PETG. The parametric study indicated that only layer thickness and infill pattern had a significant influence on PAni incorporation and electrical conductivity of coated porous samples.Originality/valueCurrent literature reports difficulties in incorporating PAni without affecting dimensional precision and feedstock stability. In situ, oxidative polymerization of Ani could overcome these limitations. However, its use as a functional post-processing of extrusion-based printed parts is a novelty.

Bond Behavior of High-Strength Steel Rebar in Ultra-High-Performance Manufactured Sand Concrete: Experiment and Modelling

Manufactured sand (MS), due to its wide availability and cost-effectiveness, is used as an alternative aggregate for quartz sand (QS) in ultra-high-performance concrete (UHPC) to prepare ultra-high-performance manufactured sand concrete (UHPMC). This study aims to assess the bond behavior of 600 MPa-grade, high-strength, hot-rolled ribbed bars (HRB 600) in UHPMC. Thirty specimens were designed for the pull-out tests, taking into account several feature parameters, including MS replacement ratio (0%, 50%, 100%), water–binder ratio (0.17, 0.19, 0.21), steel fiber content (0%, 1%, 2%), and anchorage length (2d, 3d, 4d, 5d). The effects of the feature parameters on the failure mode, bond stress–slip curves, bond strength, bond-slip mechanism, and constitutive model were analyzed and illustrated. The results reveal that the pull-out specimen of UHPMC exhibits three distinct failure modes: rebar pull-out failure, UHPMC splitting failure, and splitting-pull-out failure. The bond strength increases from 46.57 MPa to 56.92 MPa when the steel fiber content increases from 0% to 2%. Additionally, a decrease in anchoring length is beneficial for improving the bond strength; as the anchoring length increases from 2d to 5d, the bonding strength decreases by 35.84%. The bond strength increases with an increase in the MS replacement ratio. As for the water–binder ratio, the bond strength presents the highest value when the water­–binder ratio is 0.17. In addition, a new bond-slip constitutive model applicable to UHPMC and HRB 600 rebar, considering the MS replacement ratio, the water–binder ratio, etc., is proposed, which presents favorable prediction accuracy.