Pressure-sensitive Film Research Articles

Characterisation of the Mechanical Properties of Natural Fibre Polypropylene Composites Manufactured with Automated Tape Placement

The integration of natural fibre thermoplastic composites, particularly those combining flax fibres with polypropylene, offers a promising alternative to traditional synthetic composites, emphasising sustainability in composite materials. This study investigates the mechanical properties of flax/polypropylene composites manufactured using flashlamp automated tape placement and press consolidation, individually and in combination. Tensile, compression, three-point bending, and double cantilever beam tests are utilised for comparing these manufacturing processes and the mechanical performance of the resulting composites. The microstructure of the tapes is investigated using cross-sectional microscopy, and the thermophysical behaviour is analysed utilising thermogravimetric analysis and differential scanning calorimetry. The temperature during placement is monitored using an infrared camera, and the pressure is mapped with pressure-sensitive films. The natural fibre tapes show a good aptitude for being manufactured with automated tape placement. The tensile performance of tapes manufactured with automated tape placement is close to that of press consolidated samples. Compression, flexural properties, and the mode I fracture toughness critical energy release rate all benefit from a second consolidation step.

Fractal contact and asperities coalescence of rock joints under normal loading: Insights from pressure-sensitive film measurement

Direct measurement of the real contact area of rock joints under normal loading is crucial for comprehending the subsurface geological processes. However, measuring this phenomenon quantitatively at site-scale or laboratory-scale is challenging. Here, we investigate the evolution mechanism of the real contact area in rock joints by conducting closure tests on artificial and saw-cut sandstone joints under normal stresses up to 50 MPa. Geometrical shapes of contact patches are quantified by the pressure-sensitive film using the adaptive threshold method. An extensive range of contact stress within contact patches is innovatively measured by integrating the results from multi-type pressure-sensitive films. Experimental results demonstrate that the real contact area increases with the increasing normal stress hyperbolically. Such a nonlinear contact evolution behavior can be attributed to the coalescence of adjacent contact patches. The fractal dimension of composite surface governs the geometrical shapes of contact patches and the distribution of contact stress. The relationship between patch areas and bearing loads follows the Hertzian theory when the patches are small, while it gradually becomes linear with the increasing patch size. A power model with exponential cut-off is proposed to predict the size distribution of contact patches. This work can provide new insights for estimating the patch-dependent seismic nucleation length and slip stability of subsurface joints.

Static pressure response model of fluorescent pressure-sensitive film for underwater surface pressure measurement

The fluorescent pressure-sensitive film (FPSF) is a non-contact, deformation-based optical pressure sensor with high spatial resolution. The pressure response principle of FPSF is to convert pressure change into variations in fluorescent intensity through the deformation of fluorescent microspheres embedded within the film. To quantitatively analyze the pressure–deformation–intensity mechanism, a static pressure response model was established in this study. First, a finite element model was developed to predict the deformation of microspheres within the film under pressure. Second, the deformation-induced variation in fluorescent intensity was modeled with consideration of the light path blockage effect. The pressure calibration curve of the FPSF predicted by the proposed model was noted to be consistent with the experimental results of underwater calibration. In addition, the relationship between pressure sensitivity and the structural parameters of the FPSF were investigated using the pressure response model.

Relating Hydro‐Mechanical and Elastodynamic Properties of Dynamically Stressed Tensile‐Fractured Rock in Relation to Applied Normal Stress, Fracture Aperture, and Contact Area

AbstractWe exploit nonlinear elastodynamic properties of fractured rock to probe the micro‐scale mechanics of fractures and understand the relation between fluid transport and fracture aperture under dynamic stressing. Experiments were conducted on rough, tensile‐fractured Westerly granite subject to triaxial stresses. We measure fracture permeability for steady‐state fluid flow with deionized water. Pore pressure oscillations are applied at amplitudes ranging from 0.2 to 1 MPa at 1 Hz frequency. During dynamic stressing we transmit ultrasonic signals through the fracture using an array of piezoelectric transducers (PZTs) to monitor evolution of interface properties. We examine the influence of fracture aperture and contact area by conducting measurements at effective normal stresses of 10–20 MPa. Additionally, the evolution of contact area with stress is characterized using pressure sensitive film. These experiments are conducted separately with the same fracture and map contact area at stresses from 9 to 21 MPa. The measurements are a proxy for “true” contact area for the fracture surface and we relate them to elastic properties using the calculated PZT sensor footprints via numerical modeling of Fresnel zones. We compare the elastodynamic response of the fracture using the stress‐induced changes in ultrasonic wave velocities for transmitter‐receiver pairs to image spatial variations in contact properties. We show that nonlinear elasticity and permeability enhancement decrease with increasing normal stress. Additionally, post‐oscillation wave velocity and permeability exhibit quick recoveries toward pre‐oscillation values. Estimates of fracture contact area (global and local) demonstrate that the elastodynamic and permeability responses are dominated by fracture topology.

Reduced migration of multi-arm structured plasticizer from pressure-sensitive adhesive films

Reduced migration of multi-arm structured plasticizer from pressure-sensitive adhesive films

Effect of the Height of a 3D-Printed Model on the Force Transmission and Thickness of Thermoformed Orthodontic Aligners.

This research aims to investigate the influence of model height employed in the deep drawing of orthodontic aligner sheets on force transmission and aligner thickness. Forty aligner sheets (Zendura FLX) were thermoformed over four models of varying heights (15, 20, 25, and 30 mm). Normal contact force generated on the facial surface of the upper right central incisor (Tooth 11) was measured using pressure-sensitive films. Aligner thickness around Tooth 11 was measured at five points. A digital caliper and a micro-computed tomography (µ-CT) were employed for thickness measurements. The normal contact force exhibited an uneven distribution across the facial surface of Tooth 11. Model 15 displayed the highest force (88.9 ± 23.2 N), while Model 30 exhibited the lowest (45.7 ± 15.8 N). The force distribution was more favorable for bodily movement with Model 15. Thickness measurements revealed substantial thinning of the aligner after thermoforming. This thinning was most pronounced at the incisal edge (50% of the original thickness) and least at the gingivo-facial part (85%). Additionally, there was a progressive reduction in aligner thickness with increasing model height, which was most significant on the facial tooth surfaces. We conclude that the thermoplastic aligner sheets undergo substantial thinning during the thermoforming process, which becomes more pronounced as the height of the model increases. As a result, there is a decrease in both overall and localized force transmission, which could lead to increased tipping by the aligner and a diminished ability to achieve bodily movement.

Effect of thermomechanical ageing on force transmission by orthodontic aligners made of different thermoformed materials: An experimental study.

Investigating the impact of thermal and mechanical loading on the force generation of orthodontic aligners made from various thermoplastic materials and different compositions. Five distinct materials were utilized including, three multi-layer (Zendura FLX, Zendura VIVA, CA Pro) and two single-layer (Zendura A and Duran). A total of 50 thermoformed aligners (n = 10) underwent a 48-hour ageing protocol, which involved mechanical loading resulting from a 0.2 mm facial malalignment of the upper right central incisor (Tooth 11) and thermal ageing through storage in warm distilled water at 37°C. The force exerted on Tooth 11 of a resin model was measured both before and after ageing using pressure-sensitive films and a biomechanical setup. Before ageing, pressure-sensitive films recorded normal contact forces ranging from 83.1 to 149.7 N, while the biomechanical setup measured resultant forces ranging from 0.1 to 0.5 N, with lingual forces exceeding facial forces. Multi-layer materials exhibited lower force magnitudes compared to single-layer materials. After ageing, a significant reduction in force was observed, with some materials experiencing up to a 50% decrease. Notably, multi-layer materials, especially Zendura VIVA, exhibited lower force decay. The force generated by aligners is influenced by both the aligner material and the direction of movement. Multi-layer materials exhibit superior performance compared to single-layer materials, primarily because of their lower initial force, which enhances patient comfort, and their capability to maintain consistent force application even after undergoing ageing.

Effect of material composition and thickness of orthodontic aligners on the transmission and distribution of forces: an in vitro study.

To investigate the effects of material type and thickness on force generation and distribution by aligners. Sixty aligners were divided into six groups (n = 10): one group with a thickness of 0.89mm using Zendura Viva (Multi-layer), four groups with a thickness of 0.75mm using Zendura FLX (Multi-layer), CA Pro (Multi-layer), Zendura (Single-layer), and Duran (Single-layer) sheets, and one group with a thickness of 0.50mm using Duran sheets. Force measurements were conducted using Fuji® pressure-sensitive films. The lowest force values, both active and passive, were recorded for the multi-layered sheets: CA Pro (83.1N, 50.5N), Zendura FLX (88.9N, 60.7N), and Zendura Viva (92.5N, 68.5N). Conversely, the highest values were recorded for the single-layered sheets: Duran (131.9N, 71.8N) and Zendura (149.7N, 89.8N). The highest force was recorded at the middle third of the aligner, followed by the incisal third, and then the cervical third. The net force between the incisal and cervical thirds (FI-FC) showed insignificant difference across different materials. However, when comparing the incisal and middle thirds, the net force (FI-FM) was higher with single-layered materials. Both overall force and net force (FI-FM) were significantly higher with 0.75mm compared to those with a thickness of 0.50mm. Multi-layered aligner materials exert lower forces compared to their single-layered counterparts. Additionally, increased thickness in aligners results in enhanced retention and greater force generation. For effective bodily tooth movement, thicker and single-layered rigid materials are preferred. This research provides valuable insights into the biomechanics of orthodontic aligners, which could have significant clinical implications for orthodontists. Orthodontists might use this information to more effectively tailor aligner treatments, considering the specific tooth movement required for each individual patient. In light of these findings, an exchangeable protocol for aligner treatment is suggested, which however needs to be proven clinically. This protocol proposes alternating between multi-layered and single-layered materials within the same treatment phase. This strategy is suggested to optimize treatment outcomes, particularly when planning for a bodily tooth movement.

Characterization of Contact Pressure Distribution and Bruising Prediction of Apple under Compression Loading

The pressure distribution characteristics of an apple subjected to compressive loading were investigated using the pressure-sensitive film (PSF) technique combined with apple bruise measurements. Pressure was unevenly distributed in the elliptical contact region. The average pressure had no effect on bruising because it changed slightly in the range of 0.26–0.31 MPa with increasing load. Pressures of 0.20–0.40 MPa accounted for 72% of the total pressure area. Comparatively, the area where pressure over 0.50 MPa was distributed could be ignored and showed little contribution to the bruise area. The contact edge subjected to pressure below 0.10 MPa showed that no bruising occurred. As a result, the relationship between the ≥0.10 MPa pressure area strongly correlated with the bruise area according to a linear equation, with a correlation coefficient of ≥0.99. When this relationship was applied to determine the bruise area with FE, satisfactory predicted results were obtained with minor error rates of 0–7.89% for loads of 54–80 N. But larger prediction errors occurred when the load was above 90 N, suggesting that the linear elastic FE model may not be appropriate for accurately predicting apple bruising.

Highly Sensitive Pressure Sensor Based on Elastic Conductive Microspheres.

Elastic pressure sensors play a crucial role in the digital economy, such as in health care systems and human-machine interfacing. However, the low sensitivity of these sensors restricts their further development and wider application prospects. This issue can be resolved by introducing microstructures in flexible pressure-sensitive materials as a common method to improve their sensitivity. However, complex processes limit such strategies. Herein, a cost-effective and simple process was developed for manufacturing surface microstructures of flexible pressure-sensitive films. The strategy involved the combination of MXene-single-walled carbon nanotubes (SWCNT) with mass-produced Polydimethylsiloxane (PDMS) microspheres to form advanced microstructures. Next, the conductive silica gel films with pitted microstructures were obtained through a 3D-printed mold as flexible electrodes, and assembled into flexible resistive pressure sensors. The sensor exhibited a sensitivity reaching 2.6 kPa-1 with a short response time of 56 ms and a detection limit of 5.1 Pa. The sensor also displayed good cyclic stability and time stability, offering promising features for human health monitoring applications.

Analysis and prediction of contact characteristics of rock fracture surfaces under normal loading

The real contact area of rock fractures is smaller than the nominal area, and actual stresses on contacts are significantly higher. Evaluating contact characteristics and predicting potential contact areas are crucial for understanding mechanical and hydraulic properties of geological fractures under compression or shear. We measured the real contact area of mated tensile fractures using pressure-sensitive films and studied their contact characteristics and evolution under different normal stresses through point cloud analysis. It is revealed that the initial aperture of mated tensile fractures determines the contact state. Under conditions of low normal stress, regions exhibiting higher mean curvature are more susceptible to contact formation, particularly when aperture sizes are comparable. This propensity is further influenced by the directional orientation of the normal vector components within these regions. Increasing normal stress leads to faster development of new contacts in regions with smaller initial apertures. Additionally, we predicted contact characteristics and real contact area of tensile fractures using back propagation artificial neural network. Comparison between predictions and laboratory measurements demonstrated accurate prediction of contact distribution and area values by the neural network. Our findings enable the prediction of real stress states, potential failure areas, and hydraulic conductivity of rock fractures in slope and underground rock engineering.

Adhesion and Contact Aging of Acrylic Pressure-Sensitive Adhesives to Swollen Elastomers.

Fluid-infused (or swollen) elastomers are known for their antiadhesive properties. The presence of excess fluid at their surface is the main contributor to limiting contact formation and minimizing adhesion. Despite their potential, the mechanisms for adhesion and contact aging to fluid-infused elastomers are poorly understood beyond contact with a few materials (ice, biofilms, glass). This study reports on adhesion to a model fluid-infused elastomer, poly(dimethylsiloxane) (PDMS), swollen with silicone oil. The effects of oil saturation, contact time, and the opposing surface are investigated. Specifically, adhesion to two different adherents with comparable surface energies but drastically different mechanical properties is investigated: a glass surface and a soft viscoelastic acrylic pressure-sensitive adhesive film (PSA, modulus ∼25 kPa). Adhesion between the PSA and swollen PDMS [with 23% (w/w) silicone oil] retains up to 60% of its value compared to contact with unswollen (dry) PDMS. In contrast, adhesion to glass nearly vanishes in contact with the same swollen elastomer. Adhesion to the PSA also displays stronger contact aging than adhesion to glass. Contact aging with the PSA is comparable for dry and unsaturated PDMS. Moreover, load relaxation when the PSA is in contact with the PDMS does not correlate with contact aging for contact with the dry or unsaturated elastomer, suggesting that contact aging is likely caused by chain interpenetration and polymer reorganization within the contact region. Closer to full saturation of the PDMS with oil, adhesion to the PSA decreases significantly and shows a delay in the onset of contact aging that is weakly correlated to the poroelastic relaxation of the elastomer. Additional confocal imaging suggests that the presence of a layer of fluid trapped at the interface between the two solids could explain the delayed (and limited) contact aging to the oil-saturated PDMS.

Impact of Pressure Distribution and Magnitude on the Performance of Lithium Metal Anodes

Li metal anodes are a critical battery technology due to their ability to substantially increase the energy density of Li-based batteries. It is well known that pressure greatly impacts the performance of a Li-metal anode. However, precisely how the pressure value and distribution of pressure affect performance is unclear. Furthermore, the solid-electrolyte interphase composition that forms under varying pressure distributions remains a key parameter for practical lithium metal anodes. In this work, different pressure distributions were employed by using differently shaped and oriented mechanical springs in the coin cells, resulting in varying contact points. Pressure-sensitive films were used to spatially map the pressure and correlate it to the performance. It was found that higher average pressure does not necessarily have a positive effect on performance. When high pressure is paired with poor pressure uniformity, the performance is in fact worse likely due to the current focusing effect, rendering unsatisfied cycling stability. This work points to the importance of controlling the relationship between average pressure and pressure uniformity.

Thermal and mechanical investigation of proton exchange membrane fuel cells under combined loading conditions

Mechanical performance of PEM fuel cells under combined loadings is one of critical issues in improving cell performance and reliability. In this study, thermal and mechanical performance of the PEM fuel cell under clamping force and temperature load are investigated by experiments and three-dimensional dynamic simulations. In experiments, pressure distributions between gas diffusion layer and flow field are measured by pressure sensitive films. The experimental results show that the local pressure increases with clamping load, and pressure distribution is much uneven in the midstream. Meanwhile, a three-dimensional model of the cell combined transient heat transfer and mechanical response of components is developed, which is validated by experimental data. The modeling results show that under combined loadings, the porosity of gas diffusion layer under the rib decreases, attributed to compressive deformation caused by thermal gradient and clamping pressure, leading to higher effective thermal conductivity and electrical conductivity. When at a higher temperature, the overall stresses of gas diffusion layer decrease and the minimum stress is located under the center rib, forming a concave stress distribution pattern. Distribution and variation patterns of local deformations and stresses for the membrane are similar to those of gas diffusion layer, but the maximum stress and deformation are much lower. A dimensional stress coefficient is proposed to determine the stress distribution uniformity under the rib. With the increase of clamping torque, dimensionless stress coefficients under lower ambient temperature change slightly. As temperature increases, dimensionless stress coefficients increase significantly and decrease with the clamping torque, indicating the decreasing role of temperature load on mechanical response of the cell.

In Vitro Assessment of Compression Patterns Using Different Methods to Achieve Interfragmentary Compression during Tibial Plateau Levelling Osteotomy.

The aim of this study was to evaluate and characterize different methods to achieve interfragmentary compression during tibial plateau levelling osteotomy (TPLO). TPLO was performed in 20 canine tibia models (Sawbones, Vashon, Washington, United States) using 3D-printed guides for standardization. Interfragmentary compression was assessed using pressure-sensitive films (Prescale, Fujifilm, Atherstone, United Kingdom). Seven compression methods were tested: (1) Kern bone holding forceps clamping the craniodistal aspect of the TPLO plate to the caudal aspect of the tibia (K); (2) using the distal TPLO plate dynamic compression hole (P); (3) pointed bone reduction forceps engaging the caudal aspect of the proximal bone fragment and the cranial aspect of the tibial crest (F); (4) K + P; (5) K + F; (6) F + P; and (7) K + F + P. Five measurements were obtained for each method, and each bone model was used for two measurements (single method, ± plate). The interfragmentary surface was digitalized and divided into quadrants for standardization and pixel density calculation: Q1, craniomedial; Q2, craniolateral; Q3, caudomedial; and Q4, caudolateral. One-way analysis of variance (ANOVA) and post hoc tests were used for statistical analysis. Mean pressures per quadrant differed significantly between methods (p < 0.001). Methods K, F, and P produced more craniomedial, craniolateral, and caudal compression, respectively. Method K resulted in loss of caudal compression (p < 0.001). Method F + P provided the most even distribution of high interfragmentary compression forces. The addition of method K to this construct (K + F + P) marginally increased cranial compression (p = 0.189 for Q1; p < 0.001 for Q2), but reduced compression caudally (p < 0.001). Method F + P provided more even interfragmentary compression. If method K were used, then combined use with method F + P would be recommended.

An ovine knee simulator: description and proof of concept.

The ovine stifle is an established model for evaluation of knee treatments, such as meniscus replacement. This study introduces a novel ovine gait simulator for pre-testing of surgical treatments prior to in vivo animal trials. Furthermore, we describe a pilot study that assessed gait kinematics and contact pressures of native ovine stifle joints and those implanted with a novel fiber-matrix reinforced polyvinyl alcohol-polyethylene glycol (PVA-PEG) hydrogel meniscus to illustrate the efficacy of the simulator. The gait simulator controlled femoral flexion-extension and applied a 980N axial contact force to the distal tibia, whose movement was guided by the natural ligaments. Five right ovine stifle joints were implanted with a PVA-PEG total medial meniscus replacement, fixed to the tibia via transosseous tunnels and interference screws. Six intact and five implanted right ovine stifle joints were tested for 500k gait cycles at 1.55Hz. Implanted stifle joint contact pressures and kinematics in the simulator were compared to the intact group. Contact pressures were measured at 55° flexion using pressure sensitive film inserted sub-meniscally. 3D kinematics were measured optically across two 30-s captures. Peak contact pressures in intact stifles were 3.6 ± 1.0MPa and 6.0 ± 2.1MPa in the medial and lateral condyles (p < 0.05) and did not differ significantly from previous studies (p > 0.4). Medial peak implanted pressures were 4.3 ± 2.2MPa (p > 0.4 versus intact), while lateral peak pressures (9.4 ± 0.8MPa) were raised post medial compartment implantation (p < 0.01). The range of motion for intact joints was flexion/extension 37° ± 1°, varus/valgus 1° ± 1°, external/internal rotation 5° ± 3°, lateral/medial translation 2 ± 1mm, anterior/posterior translation 3 ± 1mm and distraction/compression 1 ± 1mm. Ovine joint kinematics in the simulator did not differ significantly from published in vivo data for the intact group, and the intact and implanted groups were comparable (p > 0.01), except for in distraction-compression (p < 0.01). These findings show correspondence of the ovine simulator kinematics with in vivo gait parameters. The efficacy of the simulator to evaluate novel treatments was demonstrated by implanting a PVA-PEG hydrogel medial meniscal replacement, which restored the medial peak contact pressures but not lateral. This novel simulator may enable future work on the development of surgical procedures, derisking subsequent work in live animals.

Association between oral health status and occlusal bite force in young adults

Background/purposeOral health is related to general health and a person’s overall well-being. The aim of the present study was to explore the association between oral health status and bite force among young adults. Materials and methodsMaximum bite force (MBF) was measured using Dental Prescale II in conjunction with a pressure-sensitive film and bite force analyzer in 40 young adults aged 20 to 40. Supragingival dental plaque was collected and cultured. Plaque weight, pH, and colony counts were assessed. The decayed, missing, and filled teeth index (DMFT) and body mass index (BMI) were recorded. ResultsBite force was negatively correlated with the number of missing teeth and the sum of missing and filled teeth. When the filled-to-remaining-teeth ratio (F/R ratio) was less than 8%, the bite force was significantly higher compared to an F/R ratio of 8–25%. Additionally, the amount of total bacteria was positively correlated with total bite force, and the quantity of Streptococcus mutans (S. mutans) along with total bacteria was positively correlated with bite force in the molar region (∗P < 0.05). The molar region predominantly contributed to bite force. ConclusionElevated levels of cariogenic bacteria may increase the risk of tooth loss, subsequently leading to reduced bite force. This reduction in bite force can further impact the efficiency of chewing function and, consequently, the quality of life. An F/R ratio above 8% could be easily calculated clinically and could serve as a guide to identify patients, particularly young adults, at risk of reduced bite force.

Liquid and Pressure-Sensitive Adhesives Based on Cassava Starch and Gelatin Capsule Residue: Green Alternatives for the Packaging Industry

Natural polymer-based adhesives are green alternatives, necessary to reduce the problems impacted by synthetic adhesives. Starch and gelatin have extraordinary potential for the synthesis of biobased adhesives. Citric acid (CA), a natural acid, induces the crosslinking and hydrolyzing of both gelatin and starch. In this sense, this work deals with the use of gelatin capsule residues as a promising material to produce biobased adhesives in combination with cassava starch in the presence of different CA concentrations characterizing their mechanical, physicochemical and microstructural properties. Depending on CA concentration, formulations adjusted to different applications can be obtained such as liquid and pressure-sensitive adhesive films. The inclusion of CA allows us not only to improve the applicability of the system since it modifies the flowability of the adhesives as evidenced by the observed changes in the viscosity (from 158.3 to 90.3 for formulations with 20 and 80% CA, respectively). In addition, mechanical profiles showed that the inclusion of CA increased the adhesive bond strength (from 2230.7 to 2638.7 for formulations with 20 and 80% CA, respectively). Structural modifications induced by CA in adhesive formulations were highlighted by ATR-FTIR analysis.

Influence of clamping pressure on contact pressure uniformity and electrical output performance of proton exchange membrane fuel cell

The contact pressure distributions are initially analyzed by conducting structural simulations on a single cell and a 40-cell stack of proton exchange membrane fuel cell (PEMFC) at various clamping pressures. The corresponding experimental pressure-sensitive film distributions are obtained that shows a good agreement with the simulation results. Then, the experimental and simulation data are compared by transforming images of pressure-sensitive film from experiments into detailed contact pressure data. The contact pressure uniformity of the simulation and experiment are compared by introducing mean pressure error and fluctuating intensity, and the optimal pressure range for best contact pressure uniformity is determined to be between 1.25 MPa and 1.67 MPa. Finally, CFD simulation approach is utilized to assess the electrical output performance. When comparing interface contact resistance (ICR) to porosity, the results indicate a reduction in power density of 5.1% and 1.2% at low clamping pressure compared to the case without taking ICR and porosity into account, while it decreases by 7.5% and 6.3% under high clamping pressure, respectively. It also deduced that there exists an optimal clamping pressure range for the best electrical output performance. The optimal clamping pressure is approximately 1.33 MPa, which is consistent with the previous structural results. In summary, experiments and numerical calculations of structure and fluid are carried out in this study to comprehensively evaluate the influence of clamping pressure on the structural and electrical performance of the PEMFC, the methods of experiments and simulations can offer guidance on the stack assembly process in practical applications.

Fabrication and peeling behavior of thermally conductive pressure-sensitive adhesive films with embedded graphite composite patterns

Thermal interface materials (TIMs) have been widely employed to address the thermal issues arising in electronics. Given that heat generated at heat sources is dissipated into heat sinks through TIMs, the softer they are, the more efficient the heat transfer is. In this paper, a thermally conductive pressure-sensitive adhesive (PSA) film (gr-PSA film) in which graphite composite patterns were embedded was fabricated and its thermal conductivity and peeling behavior were investigated. Because of its low storage modulus (2.4 × 104 Pa), a mixture of soft polyurethane acrylate, butyl acrylate, and 2-ethylhexyl acrylate was used to fabricate a PSA. The in-plane and through-plane thermal conductivity of the gr-PSA film were measured as 1.56 (±0.37) Wm−1K−1 and 0.25 (±0.03) Wm−1K−1, respectively. The peeling behavior of the gr-PSA tape was investigated by a 90° peel test and the results were compared with simulation results obtained by cohesive zone modeling implemented in the finite element method. Both results show that the peel force oscillated when the gr-PSA tape was peeled. Because the gr-PSA tape comprises alternating stiff and compliant segments, more force is needed peeling when bending the stiff segments.