Pore-fracture Structure Research Articles

Classification systems of pore-fractures structures and its effects on fracturing fractures propagation in shale reservoir

Marine shales serve as the primary source of shale gas in China, having attained industrial development, whereas transitional shales constitute a significant focus for ongoing exploration and exploitation. Understanding the pore-fracture structures in marine and transitional shales is strategic importance for the advancement of shale gas and oil resources in China. This study focuses on marine and transitional shales, using core samples for physical simulations to classify pore-fracture structures and reveal their impact on fracturing fractures propagation. The pore-fracture structures in shale are categorized into three primary types: pore-pore, pore-fracture, and fracture-fracture structures, with further subdivision into 12 subtypes based on the spatial distribution and types of pores and fractures. The genesis types of pore-fracture structures in different depositional facies were revealed, and characteristic models for the development of pore-fracture structure development were established. In marine shales, dense pore, pores-within-pores and interconnected pore structures are primarily controlled by organic hydrocarbon generation, as well as interconnected fracture structures formed under depositional and stresses. Interconnected fracture structures, being advantageous, are the primary targets for enhancing fracture connectivity and extension. Meanwhile, fracturing fractures preferentially connect with interconnected fracture structures developed between minerals, followed by those between clay and mineral particles. The influence of trending fracture structures on fracturing fractures is location-dependent; structures developed between skeleton mineral particles facilitate fracturing fractures propagation, while the ends of trending fracture structures retain energy, promoting spontaneous connection with surrounding pore-fracture structures, resulting in secondary fractures and aiding in multi-directional fracture propagation, enhancing the effectiveness of fracturing treatments and providing valuable theoretical support for their design.

Investigation on microscopic pore structure optimization and Lattice Boltzmann seepage law in coal modified by N-methylpyrrolidone composite solvents

This study evaluated the impact of composite solvents (1-butyl-3-methylimidazolium tetrafluoroborate [Bmim]BF4, sodium dodecyl sulfate (SDS), and N-methyl pyrrolidone (NMP)) on microscale pore-fracture structures and mesoscopic gas seepage in coal samples; by employing fractal theory and the Lattice Boltzmann method (LBM). Under combined application of three composite solvents: (1) there was a substantial 23.66 % increase in the scanning electron microscopy fractal dimension of the samples, which signifies enhanced complexity and nonhomogeneity of the samples; (2) the percentages of mesopores and macropores in the samples experienced a 10.64 % increase, resulting in a 20.45 % increase in overall porosity; (3) the effective pore fractal dimension (Da) and seepage pore fractal dimension (Ds) exhibited respective decreases of 3.05 % and 0.57 %; and (4) the average gas seepage velocity substantially increased by 53.57 %, with the optimal flow channel development position along the x-direction being closer to the exit (x = 170). These phenomena were attributed to the following: (1) introducing SDS reagents enhanced coal hydrophilicity; (2) NMP and [Bmim]BF4 aqueous solvents could more easily infiltrate the minuscule pores; (3) the synergy of the composite solvents disrupted the pore-fracture structures of the coal matrix, leading to a substantial increase in the aperture and area of the open pores; and (4) this process enhanced the connectivity, consequently increasing the average seepage velocity.

Comprehensive Characterization and Metamorphic Control Analysis of Full Apertures in Different Coal Ranks within Deep Coal Seams

The pore fracture structure of deep coal reservoirs is crucial for evaluating the potential of deep coalbed methane resources, conducting exploration and development, and controlling coal mine gas disasters. Mercury intrusion porosimetry, the liquid nitrogen method, and the low-temperature carbon dioxide adsorption method were used to study the full pore size structure and pore fractal characteristics of different coal grades in deep coal and comprehensively characterize the pore structure of kilometer-level coal mining. The sponge, Frenkel–Halsey–Hill (FHH), and density function models were applied to comprehensively analyze the pore complexity of coal, and the influence of metamorphic degree on pore size structure was evaluated. The distribution relationship of pore volume in different stages of coal samples was macropore→mesopore→micropore, and macropores had the best connectivity. Micropores and mesopores had the largest specific surface area, and the development of micropores and microcracks controlled the deep gas adsorption performance. The micropore volume and specific surface area both revealed a nonlinear decreasing trend with the increase in volatile matter, and coal metamorphism promoted the development of micropores. The pore volume and specific surface area of mesopores and macropores decreased first and then increased in a “U” shape with increasing volatile matter. In contrast, the fractal dimension D1 revealed an inverted U shape with increasing volatile matter, followed by a decrease. The D2 value decreased nonlinearly with increasing volatile matter, whereas the D3 value increased nonlinearly with increasing volatile matter. The degree of metamorphism increased, and the microporous structure became more regular.

Experimental study of coal fines migration characteristics in reservoirs with diverse coal structures: Influence on reservoir behavior

The challenge of coal fines production within tectonic coal reservoirs during coalbed methane (CBM) development in China presents a significant concern. In this study, coal samples with distinct coal structures from Hancheng mining area were selected for experiments on coal fines migration. Our analysis focused on the distinctive characteristics of coal fines generated by various coal structures, the subsequent alterations in sample permeability, and the changes in pore and fracture structures before and after the experiments. By examining the reservoir properties across different structures, we aimed to uncover the migration characteristics of coal fines in these diverse coal reservoirs and understand their influence on reservoir behavior. The results revealed distinct characteristics of coal fines among reservoirs with different structures. Under the same conditions, the average mass concentration of coal fines produced by cataclastic coal (CC) and granulated coal (GC) was observed to be 1.15–35.33 and 2.27–51.74 times higher than that of primary structure coal (PC), respectively. Coal fines generated by reservoirs with varying structures exerted different effects on pore-fracture structure and permeability. The average permeability ranges of the PC, CC and GC samples during the experiment were 0.27–0.66 mD, 0.33–1.58 mD and 8.96–19.38 mD, respectively. The PC and CC being less affected by tectonic deformation and possessing higher strength, exhibited minimal impact on their permeability. Conversely, the GC displayed the highest degree of structural deformation, lower strength, and unstable pore structure, significantly affecting its permeability. These findings offer valuable insights into coal fines production and reservoir behavior in CBM development, particularly in reservoirs featuring diverse coal structures.

A new parameter for characterizing pore-fracture structure heterogeneity: fractal dimension based on the mercury extrusion curve

A new parameter for characterizing pore-fracture structure heterogeneity: fractal dimension based on the mercury extrusion curve

Analysis of shear fracture characteristics and energy evolution of salt rock under real-time coupled thermo-mechanical conditions

Studying the shear fracture behavior of salt rock is of great importance for the identification of precursor information for geological disasters such as underground salt cavern caprock slippage, fault instability displacement, and zonal destruction of the surrounding rock. Despite its undeniable importance, research on the shear fracture characteristics of salt rock under real-time high-temperature and high-pressure triaxial conditions remains scarce. To address this research gap, this study employed a self-developed rock real-time high-temperature and high-pressure multi-field coupled triaxial universal testing machine to perform triaxial shear fracture tests on salt rock punch through shear (PTS) specimens across a wide range of confining pressures (0 to 25 MPa) and real-time temperatures (20 °C to 600 °C). Additionally, the internal pore fracture structures of the salt rock after different coupled thermo-mechanical (TM) treatments were examined using micro-computed tomography (MCT) and metallographic microscopy. The results reveal the complexity of fracture behavior in salt rock. At normal temperature and pressure, salt rock specimens primarily fractured into short rods and hollow cylindrical forms, with wing cracks appearing on the surfaces of the cylinders. Under high-temperature and high-pressure conditions, the salt rock exhibited more intense shear slippage phenomena, although the specimens did not undergo complete fracturing. Notably, the internal pore fractures in the salt rock under real-time coupled high-temperature and high-pressure displayed a competitive interaction between self-healing and thermal damage, leading to a significant nonlinear increase in mode II fracture toughness with temperature. Through the analysis of energy absorption and dissipation, this study further elucidates the shear fracture mechanism of salt rock under coupled TM conditions. Overall, the findings of this paper not only deepen our understanding of the mechanical behavior of salt rock under high-temperature and high-pressure conditions but also provide crucial theoretical support for the design and risk management of underground salt cavern projects.

Applicability of a Fractal Model for Sandstone Pore-Fracture Structure Heterogeneity by Using High-Pressure Mercury Intrusion Tests

Pore structure heterogeneity affects the porosity and permeability variation of tight sandstone, thereby restricting sandstone gas production. In total, 11 sandstone samples were taken as a target in the northwest margin of the Junggar Basin. Then, scanning electron microscope and high-pressure mercury injection tests are used to study the distribution of a pore and fracture system in the target sandstone. On this basis, single and multifractal models are used to quantitatively characterize the heterogeneity of pore structure, and the applicability of the classification model in characterizing the heterogeneity of the pore-fracture structure is explored. The results are as follows. (1) The target samples are divided into two types, with the mercury removal efficiency of type A samples ranging from 44.6 to 51.8%, pore size mainly distributed between 100 and 1000 nm, and pore volume percentage ranging from 43 to 69%. The mercury removal efficiency of type B samples ranges from 14 to 28%, and pore diameter distribution is relatively uniform. (2) Different fractal models represent different physical meanings. The calculation results of sponge and thermodynamic fractal models indicate that the heterogeneity of pore structure distribution in the type B sample is significantly stronger than that in type A, which is inconsistent with the conclusions of the Sierpinski model. This is because the aforementioned two models characterize the complexity of pore surface area, while the Sierpinski model characterizes the roughness of pore volume. The comparison shows that there is a significant correlation between the thermal dimensionality value DT and the volume percentage of macropores and mesopores. Therefore, the thermodynamic model can better quantitatively characterize the heterogeneity of macropore and mesoporous pore distribution. (3) The results indicate that higher pore volume range is mainly influenced by mesopores and macropores. From the relationship curve between mercury removal efficiency and single fractal dimension, it can be seen that mercury removal efficiency is greatly affected by distribution heterogeneity of the lower value area of pore volume, and it has no obvious relationship with distribution heterogeneity in the lower value area of the pore volume.

Imbibition models quantifying interfacial interactions: Based on nuclear magnetic resonance investigation and coupled structural characteristics

An investigation into spontaneous imbibition in porous media is of paramount scientific significance in various projects. However, a precise understanding of the interaction mechanisms between media structural characteristics and imbibition remains elusive, and quantitative analysis of the interfacial interaction is lacking. Therefore, to mitigate the influence of dispersion, this study first investigates cyclic imbibition experiments of coal samples to explore the interaction mechanism between pore-fracture structure (PFS) and imbibition. Nuclear magnetic resonance is used to visualize water transport during imbibition across all scales. Subsequently, the slake durability index is suggested to clarify the coupling relationship between water–coal interactions and imbibition. Two more comprehensive and accurate imbibition models are established, based on pore size and comprehensive seepage parameters, respectively. The results demonstrate that both new models exhibit superior conformity with experimental data compared to traditional models. The memory factor quantifies interface interaction within these models. Sensitivity analysis reveals that strong interface interaction diminishes the effective imbibition ratio, while the structural characteristics of porous media significantly influence the interaction. Furthermore, the fractal dimension quantitatively characterizes the PFS features of coal samples. An exploration of the relationship between fractal dimension and memory factor indicates the influence of porous media heterogeneity on imbibition.

Pore-fracture structures and seepage flow characteristics during spontaneous coal combustion based on CT 3D reconstruction

To study the evolution characteristics of the pore-fracture structures and seepage properties of coal in the process of spontaneous combustion, a high-temperature tube furnace was used to heat the coal samples. The coal samples were scanned using Xray-CT scanning technology, and the CT 3D reconstruction technology was used to extract the 3D pore structure and equivalent pore network model of each group of coal samples. Firstly, the specific surface area and volume of pore cleavage is statistically characterized; the change rules of Ep, Et, Lc, and Cn are quantitatively analyzed. At 200 °C, the coal body produces a large number of pore fractures, the development of coal samples is more significant, and the pore-specific surface area and the number of pore throats reached their maximum value. In addition, the changes of fractal dimension, porosity, connectivity, and permeability of coal with temperature were discussed, and the best permeability of the coal was achieved at 200 °C. The connectivity and permeability were weakened with the further increase of temperature, and the structural changes had a close influence on the gas seepage pressure and seepage flow rate. The results of the study provide important engineering guidance for deepening fire prevention in coalfields.

Quantitative Characterization of Pore–Fracture Structures in Coal Reservoirs by Using Mercury Injection–Removal Curves and Permeability Variation under Their Constraints

Pore and fracture structure heterogeneity is the basis for coalbed methane production capacity. In this paper, high-pressure mercury intrusion test curves of 16 coal samples from the Taiyuan Formation in the Linxing area are studied. Based on the fractal dimension values of mercury intrusion and retreat curves, the correlation between the two different fractal parameters is studied. Then, the permeability variation of different types of coal samples is studied using overlying pressure pore permeability tests. The correlation between the permeability variation of coal samples and dimension values is explored, and the results are as follows. (1) Based on porosity and mercury removal efficiency, all coal samples can be divided into three types, that is, types A, B, and C. Among them, Type A samples are characterized by lower total pore volume, with pore volume percentages ranging from 1000 to 10,000 nm not exceeding 15%. (2) During the mercury injection stage, both the M-model and S-model can reflect the heterogeneity of seepage pore distribution. In the mercury removal stage, the M-model cannot characterize the heterogeneity of pore size distribution in each stage, which is slightly different from the mercury injection stage. (3) The permeability of Type A samples is most sensitive to pressure, with a permeability loss rate of up to 96%. The original pore and fracture structure of this type of coal sample is relatively developed, resulting in a high initial permeability. (4) There is no significant relationship between compressibility and fractal dimension of mercury injection and mercury removal, which may be due to the comprehensive influence of pore structure on the compressibility of the sample.

Thermal fracturing of anthracite under low-energy microwave irradiation: An experimental study

Microwave-assisted coalbed methane (CBM) development is a very promising technology for engineering applications. The mechanism of the macro and micro thermal fracture of coal must be further discussed because of the thermal inhomogeneity of microwave caused by the heterogeneity and structural complexity of coal. In this study, the temperature, weight and P-wave velocity of anthracite were tested under low-energy microwave irradiation. The characteristics of fracture initiation, extension, and connectivity in coal after microwave irradiation were extracted from macroscopic and microscopic observations. Then the mechanisms of microwave thermal fracturing in anthracite were analyzed. The results showed that the temperature of anthracite under low-energy microwave irradiation varies asynchronously. The temperature distributions with high and low temperature partitions exhibit obvious bedding effects. The coal mass loss varies in stages with microwave irradiation time, first increasing slowly and then increasing dramatically above 500 °C. The P-wave velocity presents a decreasing trend with the increase of input microwave energy. Coal generates a complex fracture network at the micro and macro scales, with fractures expanding outwards in a divergent pattern. The nonuniformity of the temperature distribution promotes fracture development. It is related to the asynchronous heating caused by the mineral composition, water content, pore fracture structure, and electromagnetic field in coal. It is of great significance to improve the thermal fracturing efficiency by using the nonuniformity of microwave heat in the application of microwave-assisted CBM development.

Analysis of pore-fracture structure evolution and permeability in tar-rich coal under high-temperature pyrolysis using μCT technology

To study the internal evolution characteristics of tar-rich coal under high-temperature pyrolysis and improve pyrolysis efficiency, three-dimensional reconstruction and analysis of tar-rich coal from northern Shaanxi after high-temperature pyrolysis were conducted using μCT technology. The evolutionary development of pore and fracture structure at different temperatures and the relationship between pore-fractures and permeability was studied and discussed. The results show that when tar-rich coal from 300 to 600 °C, it mainly undergoes two stages: in the first stage, the internal substance structure of the coal mainly undergoes thermal cracking, forming large fracture bands; in the second stage, the coal undergoes intense pyrolysis reactions, resulting in primarily circular or elliptical large pore structures within the coal, with a reduction in the number of fractures. Furthermore, a strong exponential relationship is exhibited between the porosity and permeability of tar-rich coal, and a predictive equation is provided. When the temperature exceeds 500 °C, the coupled effect of pores and fractures contributes more than 20% to permeability, and its impact cannot be ignored.

Visualization of dynamic micro-migration of shale oil and investigation of shale oil movability by NMRI combined oil charging/water flooding experiments: A novel approach

Investigating the micro-migration processes of hydrocarbons within interbedded shale reservoirs, and quantitatively characterizing the movability of shale oil, are highly important for the exploration and development of continental shale oil. However, due to complex pore-fracture structures, the characterization of the micro-migration and movability of shale oil presents significant difficulties, and the lack of suitable technology restricts the understanding of shale oil accumulation mechanisms and the evaluation of movability. This study employs nuclear magnetic resonance imaging (NMRI) technology in conjunction with oil charging and water flooding experiments, to innovatively visualize and quantitatively characterize the dynamic micro-migration features and movability of hydrocarbons within the pore-fracture structures of shale. The results indicate a significant increase in oil saturation within the interbedded shale oil reservoir during the oil charging process, with the oil phase primarily accumulating in larger pores (T2 = 1–100 ms). The micro-migration and accumulation process of interbedded shale oil can be divided into three stages: the initial stage dominated by water phases in the pore spaces due to insufficient oil filling pressure, the intermediate stage marked by a rapid increase in hydrocarbons in the pore spaces, and the final stage where oil fills the entire pore system resulting in high oil saturation. The movability of different types of shale oil during water flooding varies significantly and is mainly influenced by pore-fracture structures. Interbedded shale oil reservoirs with larger pores exhibits a higher movable oil saturation (approximately 36.94%), while matrix-type shale oil reservoirs shows greater heterogeneity and lower fluid movability (approximately 14%). However, the shale oil movability of matrix-type shale oil reservoir with developed microfractures can reach 40%. More specifically, the fluid movability in smaller pore-microfracture structures (T2 < 0.5 ms) is as high as 56.88%, surpassing that in larger pores (T2 > 0.5 ms) (32.78%). Larger pores and microfractures substantially enhance the movability of hydrocarbons in the shale matrix, thus improving shale oil recoverability. In contrast, due to the higher capillary pressure (Pc) and flow resistance (Pv), smaller pores contribute less to the movability of shale oil. Overall, the outcomes of this study not only advance our understanding of the micro-migration and accumulation patterns of interbedded shale oil but also offer new insights for geological and engineering integration research on shale oil.

Experimental Study on Differential Thermal Response and Pore-Fracture Structure Evolution Characteristics of Coals under Microwave Irradiation: A Case Study of Five Different Rank Coals

Experimental Study on Differential Thermal Response and Pore-Fracture Structure Evolution Characteristics of Coals under Microwave Irradiation: A Case Study of Five Different Rank Coals

Research on Pore-Fracture Structure Alteration and Gas Emission Homogenization in an Outburst Coal Seam Induced by CO2 Gas Fracturing

Research on Pore-Fracture Structure Alteration and Gas Emission Homogenization in an Outburst Coal Seam Induced by CO₂ Gas Fracturing

STUDY OF MICROSCALE PORE STRUCTURE AND FRACTURING ON THE EXAMPLE OF CHINA SHALE FIELD

Accurate characterization of pores and fractures in shale reservoirs is the theoretical basis for effective exploration and development of shale oil and gas. Currently, the scientific community has developed methods for determining the characteristics of the pore and fracture structure of shales with different resolutions, and also discussed the mechanisms of the influence of the characteristics of pores and cracks on the filtration of shale oil and gas. In this work, firstly, a three-dimensional model of a variable-scale pore-fracture structure was created. Secondly, on the basis of data obtained using computed tomography, the characteristics of the development of pores and cracks at different geometric sizes (25 and 2 mm) were statistically analyzed. Third, pore and fracture structures of mixed, felsitic and laminated felsitic shale have been relatively studied. The results show that: (a) the fractured porosity of group I felsite shale is 0.36–0.89 %; mixed shale of group I is 0.34–0.47 %; mixed shale of group III is 0.12–0.86 %; mixed shale of group III is 0.13–0.15 %. (b) Compared to mixed shale of group I, fracturing in felsite shale of the same group is more developed. In addition, the average fractured porosity of felsite shale is 0.28 % greater than that of mixed shale. After analyzing group III, it was noticed that the cracks of the mixed dolomite shale are less developed compared to the mixed shale of the same group, while the average porosity of the cracked shale is 0.33 % less than that of the cracks of the mixed shale (c). Various components of shale samples are distinguished on a gray scale. High density components are bright white (e.g. pyrite); medium density components — light gray (for example, quartz, carbonate and clay minerals); low-density components — dark gray (for example, organic matter); cracks — black (d). The volume of matrix components is relatively high and constitutes the bulk of the total volume of shale samples. The distribution of high-density minerals has a certain randomness. High-density ellipsoidal or irregular minerals (mainly pyrite) range in diameter from a few microns to hundreds of microns, and their volume is relatively small (e). Three types of microscale fractures are mainly developed in shale: microscale fractures within mineral particles (intragranular fractures), microscale fractures between mineral particles (intergranular fractures), and shrinkage fractures. Intragranular cracks are mainly microscale cracks formed by rigid particles that collapse in a certain direction under stress.

Full-Scale Pore and Microfracture Characterization of Deep Coal Reservoirs: A Case Study of the Benxi Formation Coal in the Daning–Jixian Block, China

The pore-fracture structure of deep coal reservoirs is highly important for evaluating, exploring, and developing coalbed methane (CBM) resources. This study considers three coal samples from the DJ57 well in the Benxi Formation in the Daning–Jixian block on the eastern margin of the Ordos Basin as the research object. Based on the coal quality parameters of the coal samples, field emission scanning electron microscopy (FE-SEM), gas adsorption experiments, high-pressure mercury intrusion porosimetry (MIP), and microcomputed tomography (micro-CT) scanning were used to quantitatively characterize the nanoscale pores and microscale fractures in deep coal reservoirs and to evaluate the pore-fracture structure at different scales. The results reveal that the pore types in the Benxi Formation coal samples are diverse and include mainly organic matter (OM) pores, inorganic pores (intraparticle and interparticle pores), and microfractures. The organic pores are diverse in shape and mainly exhibit round, oval, and wedge shapes, while the microfractures exhibit slender stripes or serrated curves. The multiscale quantitative characterization of deep coal reservoir pores and fractures is based on a variety of pore characterization methods, and the pore and fracture volume distributions are mainly U-shaped, revealing the coexistence of micropores and microfractures. The volumes of micropores (0.3–2 nm), mesopores (2–50 nm), macropores (50 nm to 10 μm), and microfractures (&gt;10 μm) account for 78.00%, 6.78%, 2.08%, and 13.14%, respectively, of the total pore volume (PV). Based on a full-scale pore-fracture splicing calculation, the total permeability of the Benxi Formation coal samples ranges from 5.77 to 28.22 mD. The observation results indicate that the microfractures are connected to each other, forming a network structure with strong connectivity. The microfractures are mainly associated with pore diameters&gt;100 μm, accounting for approximately 95% of the total permeability. Moreover, micropores in deep coal reservoirs provide a large space for CBM adsorption, and microfractures enhance the seepage capacity of CBM.

Integrated NMR Analysis for Evaluating Pore-Fracture Structures and Permeability in Deep Coals: A One-Stop Approach

Integrated NMR Analysis for Evaluating Pore-Fracture Structures and Permeability in Deep Coals: A One-Stop Approach

Comprehensive Analysis of Connectivity and Permeability of a Pore-Fracture Structure in Low Permeability Seam of Huainan-Huaibei Coalfield.

The connectivity and permeability of the coal seam pore structures control the occurrence and migration of coalbed methane. Coal samples were used from Huainan-Huaibei to reconstruct three-dimensional models of the pores and an equivalent pore network model, Statistical pore structure characteristic parameters. The pore structure of the coal reservoir was analyzed from the direction of multidimensional and multiangle. It shows that based on quantitative analysis, the representative Elementary volume of 500 × 500 × 500 was the most suitable experimental volume. The Y-axis direction of the Renlou sample had poor pore connectivity compared to that of other samples. Large volume connected pores dominated their pore systems. In terms of coal sample pore connectivity, the coal samples from the Liuzhuang and Qidong regions had pore connectivity better than those from the other regions. The pore connectivity of the Liuzhuang coal samples was the best. In terms of coal permeability, the Liuzhuang sample had better permeability than the other three samples, and the permeability was the best in the Y-axis direction. For all the combinations of the different types of throats, the shorter the throat, the greater the equivalent radius and the better the permeability. Conversely, the worse the permeability. During gas injection production, the closer the gas injection area was to the gas injection well, the poorer the connectivity and the lower the permeability over time. Near the production area, where the CO2 did not reach the production area, the fracture porosity and effective connected porosity of the coal reservoir increased over time. When CO2 reached the production area, the change in its connected pore structure was consistent with the change in the connected pores in the gas injection area. With this study, the coal seam pore structure on a microscale was characterized. A comprehensive analysis of the coal reservoir pore connectivity and permeability was completed. The study results are significant for the exploration and development of coalbed methane in the Huainan-Huaibei coalfield.

Microscopic seepage simulation of gas and water in shale pores and slits based on VOF

Abstract The microscopic pore-fracture structure and wettability have a significant influence on the two-phase seepage of shale gas and water. Due to the limitation of experimental conditions, the seepage patterns of gas and water in shale pores and slits under different wetting conditions have not been clarified yet. In this study, the three-dimensional digital rock models of shale inorganic pores, organic pores, and microfractures are established by focused ion beam-scanning electron microscopy scanning, and gas-driven water seepage simulation in shale microscopic pore-fracture structure under different wetting conditions is carried out based on volume of fluid method. The simulation results show that the gas–water relative permeability curves of microfractures are up-concave, and the gas–water relative permeability curves of inorganic and organic pores are up-convex; the gas–water two-phase percolation in microfractures is least affected by the change of wettability, the gas–water two-phase percolation in inorganic pores is most affected by the change of wettability, and the organic pores are in between; the gas–water two-phase percolation zone of microfractures is the largest, and the isotonic saturation is the highest; under the water-wet conditions, the critical gas saturation of microfractures, inorganic pores, and organic pores are 0.13, 0.315, and 0.34, respectively, and the critical gas saturation of organic pores under non-water-wet conditions is 0.525, indicating that under water-bearing conditions, the shale gas flow capacity in water-wet microfractures is the strongest, followed by water-wet inorganic pores, water-wet organic pores, and hydrophobic organic pores, respectively.